BRPI0504143A - processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada pureza - Google Patents
processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada purezaInfo
- Publication number
- BRPI0504143A BRPI0504143A BRPI0504143-0A BRPI0504143A BRPI0504143A BR PI0504143 A BRPI0504143 A BR PI0504143A BR PI0504143 A BRPI0504143 A BR PI0504143A BR PI0504143 A BRPI0504143 A BR PI0504143A
- Authority
- BR
- Brazil
- Prior art keywords
- fatty acid
- high purity
- alcohol
- alkyl esters
- effluent
- Prior art date
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title abstract 7
- 235000014113 dietary fatty acids Nutrition 0.000 title abstract 2
- 229930195729 fatty acid Natural products 0.000 title abstract 2
- 239000000194 fatty acid Substances 0.000 title abstract 2
- 150000004665 fatty acids Chemical class 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 4
- 238000000926 separation method Methods 0.000 abstract 3
- -1 Glycerol Esters Chemical class 0.000 abstract 2
- 125000005907 alkyl ester group Chemical group 0.000 abstract 2
- 239000012528 membrane Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 239000010775 animal oil Substances 0.000 abstract 1
- 150000002314 glycerols Chemical class 0.000 abstract 1
- 239000002638 heterogeneous catalyst Substances 0.000 abstract 1
- 239000008158 vegetable oil Substances 0.000 abstract 1
- 235000013311 vegetables Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/128—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis
- C07C29/1285—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis of esters of organic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Catalysts (AREA)
Abstract
"PROCESSO DE PRODUçãO DE éSTERES ALQUìLICOS DE áCIDO GRAXO E DE GLICEROL DE ELEVADA PUREZA". A presente invenção refere-se a um processo de produção de ésteres alquílicos de ácido graxo e de glicerol, compreendendo: - pelo menos uma etapa reacional na qual se coloca em contato uma carga que comporta um óleo vegetal e/ou animal e um álcool, em presença de um catalisador heterogêneo, de maneira a se obter um efluente que comporta pelo menos ésteres alquílicos, glicerol ou álcool; e pelo menos uma etapa de separação, quando na qual se faz uma separação de pelo menos uma parte do efluente, de maneira a separar um efluente rico em álcool e um efluente rico em ésteres alquílicos, pelo menos urna etapa de separação consiste em uma separação membranária que utiliza pelo menos uma membrana permeável ao álcool.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0407777A FR2872812B1 (fr) | 2004-07-12 | 2004-07-12 | Procede de production d'esters alkyliques d'acides gras et de glycerine de haute purete |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0504143A true BRPI0504143A (pt) | 2006-02-21 |
Family
ID=34942442
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0504143-0A BRPI0504143A (pt) | 2004-07-12 | 2005-07-12 | processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada pureza |
Country Status (4)
| Country | Link |
|---|---|
| US (2) | US7138536B2 (pt) |
| EP (1) | EP1616853A1 (pt) |
| BR (1) | BRPI0504143A (pt) |
| FR (1) | FR2872812B1 (pt) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7563915B2 (en) * | 2006-05-30 | 2009-07-21 | The Penn State Research Foundation | Green biodiesel |
| US7901469B2 (en) * | 2006-07-26 | 2011-03-08 | Alternative Fuels Group Inc. | Alternative organic fuel formulations including vegetable oil |
| US7897798B2 (en) | 2006-08-04 | 2011-03-01 | Mcneff Research Consultants, Inc. | Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same |
| US8445709B2 (en) * | 2006-08-04 | 2013-05-21 | Mcneff Research Consultants, Inc. | Systems and methods for refining alkyl ester compositions |
| US7905931B2 (en) | 2007-02-09 | 2011-03-15 | Primafuel, Inc. | Biodiesel production method and apparatus |
| US8017796B2 (en) * | 2007-02-13 | 2011-09-13 | Mcneff Research Consultants, Inc. | Systems for selective removal of contaminants from a composition and methods of regenerating the same |
| CA2678519A1 (en) * | 2007-02-13 | 2008-08-21 | Mcneff Research Consultants, Inc. | Devices and methods for selective removal of contaminants from a composition |
| WO2008156612A1 (en) * | 2007-06-15 | 2008-12-24 | Cargill, Incorporated | Process for the purification of crude glycerol compositions |
| FR2918059B1 (fr) | 2007-06-29 | 2010-10-29 | Inst Francais Du Petrole | Amelioration de la decantation dans un procede de production d'esters alkyliques a partir d'huile vegetale ou animale et d'un monoalcool aliphatique. |
| AR067384A1 (es) * | 2007-06-29 | 2009-10-07 | Archer Daniels Midland Co | Proceso para desalar soluciones de glicerol y recuperacion de sustancias quimicas |
| US20090005583A1 (en) * | 2007-06-29 | 2009-01-01 | Benecke Herman P | Preparation of Propylene Glycol Fatty Acid Ester or Other Glycol or Polyol Fatty Acid Esters |
| DE102007034621A1 (de) * | 2007-07-25 | 2009-01-29 | Lanxess Deutschland Gmbh | Polyolreinigung |
| US8591605B2 (en) | 2007-07-26 | 2013-11-26 | Board Of Regents Of The Nevada System Of Higher Education, On Behalf Of The University Of Nevada, Reno | Methods, systems, and apparatus for obtaining biofuel from coffee and fuels produced therefrom |
| US7943791B2 (en) * | 2007-09-28 | 2011-05-17 | Mcneff Research Consultants, Inc. | Methods and compositions for refining lipid feed stocks |
| US7718833B2 (en) | 2007-11-02 | 2010-05-18 | Johann Haltermann, Ltd. | Purification of glycerin obtained as a bioproduct from the transesterification of triglycerides in the synthesis of biofuel |
| PH12010501172A1 (en) * | 2007-12-19 | 2009-06-25 | Bayer Technology Services Gmbh | Method for producing fatty acid alkyl esters |
| WO2009099804A2 (en) * | 2008-02-01 | 2009-08-13 | Lanxess Sybron Chemicals Inc. | A process for the purification of crude glycerin utilizing ion exclusion chromatorgraphy and glycerin concentration |
| KR100877384B1 (ko) * | 2008-06-30 | 2009-01-07 | 바이오원 (주) | 필터링 기술을 이용한 조 글리세린의 정제방법 |
| US8137527B1 (en) | 2008-07-28 | 2012-03-20 | Primafuel, Inc. | Carbon dioxide isolation and generation |
| US8361174B2 (en) * | 2008-10-07 | 2013-01-29 | Sartec Corporation | Catalysts, systems, and methods for producing fuels and fuel additives from polyols |
| US9102877B2 (en) * | 2008-11-12 | 2015-08-11 | Sartec Corporation | Systems and methods for producing fuels from biomass |
| FR2940280B1 (fr) | 2008-12-23 | 2011-02-25 | Inst Francais Du Petrole | Procede de fabrication d'esters a partir d'huile vegetale ou animale et d'un monoalcool aliphatique utilisant une separation membranaire |
| US20110021807A1 (en) * | 2009-07-25 | 2011-01-27 | Soil Net Llc | Enhanced biodiesel process |
| US8907113B2 (en) | 2009-07-25 | 2014-12-09 | Aicardo Roa-Espinosa | Enhanced biodiesel process |
| US20110092725A1 (en) * | 2009-10-19 | 2011-04-21 | Lurgi Psi, Inc. | Catalysis Of Fats And Oils To Alkyl Esters Using Hydrolysis As Pretreatment |
| FR2966457B1 (fr) | 2010-10-21 | 2012-10-19 | IFP Energies Nouvelles | Procede de production d'esters alkyliques a partir d'huile vegetale ou animale et d'un monoalcool aliphatique avec integration thermique. |
| US8962873B2 (en) * | 2011-03-09 | 2015-02-24 | Benefuel, Inc. | Systems and methods for making bioproducts |
| EP3010877B1 (en) * | 2013-06-19 | 2019-12-18 | FPInnovations | Method for producing bio-methanol at pulp mills |
| US9328054B1 (en) | 2013-09-27 | 2016-05-03 | Travis Danner | Method of alcoholisis of fatty acids and fatty acid gyicerides |
| US10144883B2 (en) | 2013-11-14 | 2018-12-04 | Uop Llc | Apparatuses and methods for desulfurization of naphtha |
| US9765267B2 (en) | 2014-12-17 | 2017-09-19 | Exxonmobil Chemical Patents Inc. | Methods and systems for treating a hydrocarbon feed |
| WO2017119007A1 (en) | 2016-01-07 | 2017-07-13 | Institute Of Chemical Technology | Process for purification and refining of glycerol |
| RU2665041C2 (ru) * | 2016-12-30 | 2018-08-27 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Российский государственный университет нефти и газа (национальный исследовательский университет) имени И.М. Губкина" | Способ получения биодизельного топлива |
| US10239812B2 (en) | 2017-04-27 | 2019-03-26 | Sartec Corporation | Systems and methods for synthesis of phenolics and ketones |
| US10696923B2 (en) | 2018-02-07 | 2020-06-30 | Sartec Corporation | Methods and apparatus for producing alkyl esters from lipid feed stocks, alcohol feedstocks, and acids |
| US10544381B2 (en) | 2018-02-07 | 2020-01-28 | Sartec Corporation | Methods and apparatus for producing alkyl esters from a reaction mixture containing acidified soap stock, alcohol feedstock, and acid |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2003916B (en) * | 1977-09-02 | 1982-05-19 | Hitachi Ltd | Process for hydrodesulphurizing hydrocarbon oil |
| NZ504648A (en) * | 1997-11-24 | 2002-02-01 | Energea Umwelttechnologie Gmbh | Method and equipment for producing fatty acid methyl ester to produce diesel fuel where the fatty acids are transesterified to fatty acid methyl ester |
| US20030168383A1 (en) * | 2002-03-06 | 2003-09-11 | Hoekstra George R. | Distillate desulfurization process |
| US6893554B2 (en) * | 2002-03-13 | 2005-05-17 | Exxonmobil Research And Engineering Company | Naphtha desulfurization with selectively suppressed hydrogenation |
| FR2838433B1 (fr) * | 2002-04-11 | 2005-08-19 | Inst Francais Du Petrole | Procede de production d'esters alkyliques a partir d'une huile vegetale ou animale et d'un monoalcool aliphatique |
| JP2006508148A (ja) * | 2002-11-27 | 2006-03-09 | バイオディーゼル オーストラリア リミテッド | アルキルエステルの生産方法 |
-
2004
- 2004-07-12 FR FR0407777A patent/FR2872812B1/fr not_active Expired - Fee Related
-
2005
- 2005-06-23 EP EP05291347A patent/EP1616853A1/fr not_active Withdrawn
- 2005-07-12 BR BRPI0504143-0A patent/BRPI0504143A/pt not_active IP Right Cessation
- 2005-07-12 US US11/178,605 patent/US7138536B2/en not_active Expired - Fee Related
- 2005-09-28 US US11/236,792 patent/US20060076271A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| FR2872812A1 (fr) | 2006-01-13 |
| US20060014974A1 (en) | 2006-01-19 |
| US20060076271A1 (en) | 2006-04-13 |
| EP1616853A1 (fr) | 2006-01-18 |
| FR2872812B1 (fr) | 2006-09-08 |
| US7138536B2 (en) | 2006-11-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 10A ANUIDADE. |
|
| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2314 DE 12-05-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |