BRPI0504143A - processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada pureza - Google Patents

processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada pureza

Info

Publication number
BRPI0504143A
BRPI0504143A BRPI0504143-0A BRPI0504143A BRPI0504143A BR PI0504143 A BRPI0504143 A BR PI0504143A BR PI0504143 A BRPI0504143 A BR PI0504143A BR PI0504143 A BRPI0504143 A BR PI0504143A
Authority
BR
Brazil
Prior art keywords
fatty acid
high purity
alcohol
alkyl esters
effluent
Prior art date
Application number
BRPI0504143-0A
Other languages
English (en)
Inventor
Laurent Bournay
Arnaud Baudot
Original Assignee
Inst Francais Du Petrole
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inst Francais Du Petrole filed Critical Inst Francais Du Petrole
Publication of BRPI0504143A publication Critical patent/BRPI0504143A/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/128Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis
    • C07C29/1285Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by alcoholysis of esters of organic acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/03Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/56Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Catalysts (AREA)

Abstract

"PROCESSO DE PRODUçãO DE éSTERES ALQUìLICOS DE áCIDO GRAXO E DE GLICEROL DE ELEVADA PUREZA". A presente invenção refere-se a um processo de produção de ésteres alquílicos de ácido graxo e de glicerol, compreendendo: - pelo menos uma etapa reacional na qual se coloca em contato uma carga que comporta um óleo vegetal e/ou animal e um álcool, em presença de um catalisador heterogêneo, de maneira a se obter um efluente que comporta pelo menos ésteres alquílicos, glicerol ou álcool; e pelo menos uma etapa de separação, quando na qual se faz uma separação de pelo menos uma parte do efluente, de maneira a separar um efluente rico em álcool e um efluente rico em ésteres alquílicos, pelo menos urna etapa de separação consiste em uma separação membranária que utiliza pelo menos uma membrana permeável ao álcool.
BRPI0504143-0A 2004-07-12 2005-07-12 processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada pureza BRPI0504143A (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0407777A FR2872812B1 (fr) 2004-07-12 2004-07-12 Procede de production d'esters alkyliques d'acides gras et de glycerine de haute purete

Publications (1)

Publication Number Publication Date
BRPI0504143A true BRPI0504143A (pt) 2006-02-21

Family

ID=34942442

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0504143-0A BRPI0504143A (pt) 2004-07-12 2005-07-12 processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada pureza

Country Status (4)

Country Link
US (2) US7138536B2 (pt)
EP (1) EP1616853A1 (pt)
BR (1) BRPI0504143A (pt)
FR (1) FR2872812B1 (pt)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7563915B2 (en) * 2006-05-30 2009-07-21 The Penn State Research Foundation Green biodiesel
US7901469B2 (en) * 2006-07-26 2011-03-08 Alternative Fuels Group Inc. Alternative organic fuel formulations including vegetable oil
US7897798B2 (en) 2006-08-04 2011-03-01 Mcneff Research Consultants, Inc. Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same
US8445709B2 (en) * 2006-08-04 2013-05-21 Mcneff Research Consultants, Inc. Systems and methods for refining alkyl ester compositions
US7905931B2 (en) 2007-02-09 2011-03-15 Primafuel, Inc. Biodiesel production method and apparatus
US8017796B2 (en) * 2007-02-13 2011-09-13 Mcneff Research Consultants, Inc. Systems for selective removal of contaminants from a composition and methods of regenerating the same
CA2678519A1 (en) * 2007-02-13 2008-08-21 Mcneff Research Consultants, Inc. Devices and methods for selective removal of contaminants from a composition
WO2008156612A1 (en) * 2007-06-15 2008-12-24 Cargill, Incorporated Process for the purification of crude glycerol compositions
FR2918059B1 (fr) 2007-06-29 2010-10-29 Inst Francais Du Petrole Amelioration de la decantation dans un procede de production d'esters alkyliques a partir d'huile vegetale ou animale et d'un monoalcool aliphatique.
AR067384A1 (es) * 2007-06-29 2009-10-07 Archer Daniels Midland Co Proceso para desalar soluciones de glicerol y recuperacion de sustancias quimicas
US20090005583A1 (en) * 2007-06-29 2009-01-01 Benecke Herman P Preparation of Propylene Glycol Fatty Acid Ester or Other Glycol or Polyol Fatty Acid Esters
DE102007034621A1 (de) * 2007-07-25 2009-01-29 Lanxess Deutschland Gmbh Polyolreinigung
US8591605B2 (en) 2007-07-26 2013-11-26 Board Of Regents Of The Nevada System Of Higher Education, On Behalf Of The University Of Nevada, Reno Methods, systems, and apparatus for obtaining biofuel from coffee and fuels produced therefrom
US7943791B2 (en) * 2007-09-28 2011-05-17 Mcneff Research Consultants, Inc. Methods and compositions for refining lipid feed stocks
US7718833B2 (en) 2007-11-02 2010-05-18 Johann Haltermann, Ltd. Purification of glycerin obtained as a bioproduct from the transesterification of triglycerides in the synthesis of biofuel
PH12010501172A1 (en) * 2007-12-19 2009-06-25 Bayer Technology Services Gmbh Method for producing fatty acid alkyl esters
WO2009099804A2 (en) * 2008-02-01 2009-08-13 Lanxess Sybron Chemicals Inc. A process for the purification of crude glycerin utilizing ion exclusion chromatorgraphy and glycerin concentration
KR100877384B1 (ko) * 2008-06-30 2009-01-07 바이오원 (주) 필터링 기술을 이용한 조 글리세린의 정제방법
US8137527B1 (en) 2008-07-28 2012-03-20 Primafuel, Inc. Carbon dioxide isolation and generation
US8361174B2 (en) * 2008-10-07 2013-01-29 Sartec Corporation Catalysts, systems, and methods for producing fuels and fuel additives from polyols
US9102877B2 (en) * 2008-11-12 2015-08-11 Sartec Corporation Systems and methods for producing fuels from biomass
FR2940280B1 (fr) 2008-12-23 2011-02-25 Inst Francais Du Petrole Procede de fabrication d'esters a partir d'huile vegetale ou animale et d'un monoalcool aliphatique utilisant une separation membranaire
US20110021807A1 (en) * 2009-07-25 2011-01-27 Soil Net Llc Enhanced biodiesel process
US8907113B2 (en) 2009-07-25 2014-12-09 Aicardo Roa-Espinosa Enhanced biodiesel process
US20110092725A1 (en) * 2009-10-19 2011-04-21 Lurgi Psi, Inc. Catalysis Of Fats And Oils To Alkyl Esters Using Hydrolysis As Pretreatment
FR2966457B1 (fr) 2010-10-21 2012-10-19 IFP Energies Nouvelles Procede de production d'esters alkyliques a partir d'huile vegetale ou animale et d'un monoalcool aliphatique avec integration thermique.
US8962873B2 (en) * 2011-03-09 2015-02-24 Benefuel, Inc. Systems and methods for making bioproducts
EP3010877B1 (en) * 2013-06-19 2019-12-18 FPInnovations Method for producing bio-methanol at pulp mills
US9328054B1 (en) 2013-09-27 2016-05-03 Travis Danner Method of alcoholisis of fatty acids and fatty acid gyicerides
US10144883B2 (en) 2013-11-14 2018-12-04 Uop Llc Apparatuses and methods for desulfurization of naphtha
US9765267B2 (en) 2014-12-17 2017-09-19 Exxonmobil Chemical Patents Inc. Methods and systems for treating a hydrocarbon feed
WO2017119007A1 (en) 2016-01-07 2017-07-13 Institute Of Chemical Technology Process for purification and refining of glycerol
RU2665041C2 (ru) * 2016-12-30 2018-08-27 Федеральное государственное бюджетное образовательное учреждение высшего образования "Российский государственный университет нефти и газа (национальный исследовательский университет) имени И.М. Губкина" Способ получения биодизельного топлива
US10239812B2 (en) 2017-04-27 2019-03-26 Sartec Corporation Systems and methods for synthesis of phenolics and ketones
US10696923B2 (en) 2018-02-07 2020-06-30 Sartec Corporation Methods and apparatus for producing alkyl esters from lipid feed stocks, alcohol feedstocks, and acids
US10544381B2 (en) 2018-02-07 2020-01-28 Sartec Corporation Methods and apparatus for producing alkyl esters from a reaction mixture containing acidified soap stock, alcohol feedstock, and acid

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2003916B (en) * 1977-09-02 1982-05-19 Hitachi Ltd Process for hydrodesulphurizing hydrocarbon oil
NZ504648A (en) * 1997-11-24 2002-02-01 Energea Umwelttechnologie Gmbh Method and equipment for producing fatty acid methyl ester to produce diesel fuel where the fatty acids are transesterified to fatty acid methyl ester
US20030168383A1 (en) * 2002-03-06 2003-09-11 Hoekstra George R. Distillate desulfurization process
US6893554B2 (en) * 2002-03-13 2005-05-17 Exxonmobil Research And Engineering Company Naphtha desulfurization with selectively suppressed hydrogenation
FR2838433B1 (fr) * 2002-04-11 2005-08-19 Inst Francais Du Petrole Procede de production d'esters alkyliques a partir d'une huile vegetale ou animale et d'un monoalcool aliphatique
JP2006508148A (ja) * 2002-11-27 2006-03-09 バイオディーゼル オーストラリア リミテッド アルキルエステルの生産方法

Also Published As

Publication number Publication date
FR2872812A1 (fr) 2006-01-13
US20060014974A1 (en) 2006-01-19
US20060076271A1 (en) 2006-04-13
EP1616853A1 (fr) 2006-01-18
FR2872812B1 (fr) 2006-09-08
US7138536B2 (en) 2006-11-21

Similar Documents

Publication Publication Date Title
BRPI0504143A (pt) processo de produção de ésteres alquìlicos de ácido graxo e de glicerol de elevada pureza
NO20054347D0 (no) Drivstoffproduksjon
BR0112436A (pt) Processo para produzir um alquil éster de um ácido carboxìlico
DE60312446D1 (de) Vefahren zur Herstellung einer Kohlenwasserstoffkomponente biologischer Herkunft
BR0300931A (pt) Processo de produção de ésteres alquìlicos a partir de um óleo vegetal ou animal e de um monoálcool alifático
BRPI0705727A2 (pt) processo para produzir biodiesel de glicerìdeos e processo para produção de biodiesel purificado de glicerìdeos
BRPI0718997A2 (pt) Processo para preparar ésteres de alquila de ácidos graxos e acroleína a partir de triglicerídeos.
BR9713206A (pt) Método para produção de ésteres de ácidos graxos
CO6280548A2 (es) Procedimiento para la preparacion de esteres alquilicos de acidos grasos
WO2007062158A3 (en) Adducts of levulinic derivatives with epoxidized fatty acid esters and uses thereof
AR074019A1 (es) Produccion enzimatica de esteres etilicos de acidos grasos
ATE355350T1 (de) Fettsuurezusammensetzung, herstellung und verwendung davon
ATE525344T1 (de) Verfahren zur herstellung von biodiesel
BR9909312A (pt) Processos para separar ácido acrìlico, e para preparar um acrilato, ou uma mistura de dois ou mais do mesmo
CO6531505A2 (es) Proceso para purificacióbn de glicerol alcalino crudo
EP1966387A4 (en) PROCESS FOR PREPARING DIACYLGLYCERINE
ATE420196T1 (de) Enzymatische herstellung von degummierten fettsäurealkylestern
BRPI0407689A (pt) processo para a obtenção de ésteres de alquila dos ácidos graxos, ácidos de rosina e esteróis a partir de óleo de "tall" em bruto
BRPI0500333A (pt) processo catalìtico para esterificação de ácidos graxos
WO2008099882A1 (ja) 2-メチル-3-(3,4-メチレンジオキシフェニル)プロパナール及びその製造方法
AR033029A1 (es) Metodos para recuperar acidos grasos
KR970015556A (ko) 알칸올을 사용한 (메트) 아크릴산의 에스테르화 방법
WO2007052162A3 (en) Concentration of fatty acid alkyl esters by enzymatic reactions with glycerol
DE602008000299D1 (de) Verfahren zur Herstellung von Aminobenzoatestern
FR3002937B1 (fr) Utilisation d'acide sulfonique pour la recuperation de glycerol issu de la reaction de trans-esterification de triglycerides

Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

Free format text: REFERENTE A 10A ANUIDADE.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2314 DE 12-05-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.