BRPI0509703A - processo para a produção de pré-polìmeros de poliuretano - Google Patents
processo para a produção de pré-polìmeros de poliuretanoInfo
- Publication number
- BRPI0509703A BRPI0509703A BRPI0509703-7A BRPI0509703A BRPI0509703A BR PI0509703 A BRPI0509703 A BR PI0509703A BR PI0509703 A BRPI0509703 A BR PI0509703A BR PI0509703 A BRPI0509703 A BR PI0509703A
- Authority
- BR
- Brazil
- Prior art keywords
- polyol
- range
- component
- polyurethane prepolymers
- groups
- Prior art date
Links
- 229920001730 Moisture cure polyurethane Polymers 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 229920005862 polyol Polymers 0.000 abstract 5
- 150000003077 polyols Chemical class 0.000 abstract 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 3
- 239000005056 polyisocyanate Substances 0.000 abstract 3
- 229920001228 polyisocyanate Polymers 0.000 abstract 3
- 239000000853 adhesive Substances 0.000 abstract 2
- 230000001070 adhesive effect Effects 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 abstract 2
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 239000012948 isocyanate Substances 0.000 abstract 1
- 150000002513 isocyanates Chemical group 0.000 abstract 1
- 239000000178 monomer Substances 0.000 abstract 1
- 229920000642 polymer Polymers 0.000 abstract 1
- 229920002635 polyurethane Polymers 0.000 abstract 1
- 239000004814 polyurethane Substances 0.000 abstract 1
- 239000003566 sealing material Substances 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
- C08G18/797—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing carbodiimide and/or uretone-imine groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
- C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6603—Compounds of groups C08G18/42, C08G18/48, or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
- C08G18/6607—Compounds of groups C08G18/42, C08G18/48, or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
PROCESSO PARA A PRODUçãO DE PRé-POLìMEROS DE POLIURETANO. A presente invenção refere-se a um processo para a produção de pré-polímeros de poliuretano com grupos isocianato em posição terminal, no qual reagem-se pol´isocianatos com polióis, sendo que (1) em um primeiro estágio de síntese se produz um componente (A), em que a) se utiliza como poliisocianato (X) pelo menos um pol´isocianato assimétrico, preferentemente do grupo: toluilenodisocianato (TDI) com um teor>igual 99% em peso, de 2,4-TDI,2,4'-difenilmetanodiisocianato com uma fração de 2,4'-isómeros de pelo menos 95% em peso, preferentemente pelo menos 97% em peso, b) como poliol pelo menos um poliol com um peso molecular médio (M~ n~) de 60 até 3000 g/mol, c) a proporção de grupos hidroxila para grupos isocianato é ajustada para < 1, preferentemente na faixa entre 0,4: 1 até 0,8: 1, de modo especialmente preferido, na faixa entre 0,45: 1 até 0,6: 1, d) eventualmente se acescenta um catalisador e após a reação de todos os grupos hidroxila (II) em um segundo estágio de síntese se acrescenta um outro poliol ao componente (A), sendo que se ajusta a proporção de reação dos grupos hidroxila do outro poliol para grupos isocianato do componente A na faixa de 1,1 :1 até 2,0 :11 preferentemente de 1,3 :1 até 1,8:1 e de modo especialmente preferido, na faixa de 1,45 :1 até 1,75 :1. Pré-polímeros de poliuretano produzidos dessa maneira prestam-se para a fabricação de adesivos e materiais de vedação de um e dois componentes, especialmente de adesivos de revestimento, Os pré-polimeros de poliuretano produzidos de acordo com a invenção, são pouco viscosos e pobres em monómeros.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102004018048A DE102004018048A1 (de) | 2004-04-08 | 2004-04-08 | Verfahren zur Herstellung von Polyurethan-Prepolymeren |
| PCT/EP2005/002205 WO2005097861A1 (de) | 2004-04-08 | 2005-03-03 | Verfahren zur herstellung von polyurethan-prepolymeren |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0509703A true BRPI0509703A (pt) | 2007-09-18 |
Family
ID=34962691
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0509703-7A BRPI0509703A (pt) | 2004-04-08 | 2005-03-03 | processo para a produção de pré-polìmeros de poliuretano |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20070129525A1 (pt) |
| EP (1) | EP1732966A1 (pt) |
| CN (1) | CN1938353B (pt) |
| BR (1) | BRPI0509703A (pt) |
| DE (1) | DE102004018048A1 (pt) |
| WO (1) | WO2005097861A1 (pt) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006059464A1 (de) * | 2006-12-14 | 2008-06-19 | Henkel Kgaa | Polyurethan-Kaschierklebstoff |
| DE102008009407A1 (de) * | 2008-02-15 | 2009-08-20 | Bayer Materialscience Ag | Klebstoff |
| DE102008035947B4 (de) | 2008-07-31 | 2015-03-26 | Kraussmaffei Technologies Gmbh | Verfahren zur Herstellung eines Produktes aus reaktiven Ausgangsstoffen |
| DE102008060885A1 (de) * | 2008-12-09 | 2010-06-10 | Henkel Ag & Co. Kgaa | PU-Klebstoffen für sterilisierbare Verbundfolien |
| WO2011123492A2 (en) * | 2010-04-01 | 2011-10-06 | Henkel Corporation | Methods for making aqueous polyurethane dispersions of aromatic polyisocyanate mixtures and compositions thereof |
| DE102010030437A1 (de) | 2010-06-23 | 2011-12-29 | Henkel Ag & Co. Kgaa | TPU-Kaschierklebstoff |
| PL2588312T3 (pl) | 2010-06-29 | 2021-01-25 | Ashland Licensing And Intellectual Property Llc | Bezrozpuszczalnikowe spoiwo laminacyjne do laminowania elastycznych opakowań i struktury laminowane wytworzone ze spoiwem |
| CN102140243B (zh) * | 2010-11-26 | 2012-07-25 | 山东东大一诺威聚氨酯有限公司 | 硅烷改性单组份湿固化聚氨酯球场用塑胶浆料及其制备方法 |
| WO2012142148A1 (en) * | 2011-04-15 | 2012-10-18 | H.B. Fuller Company | Modified diphenylmethane diisocyanate-based adhesives |
| CN102432991B (zh) * | 2011-08-16 | 2013-08-07 | 江阴市文明体育塑胶有限公司 | 塑胶地垫加强层 |
| CN102286245B (zh) * | 2011-08-16 | 2013-10-09 | 江阴市文明体育塑胶有限公司 | 塑胶地板弹性层 |
| DE102011089783A1 (de) * | 2011-12-23 | 2013-06-27 | Bayer Materialscience Aktiengesellschaft | Niedrigviskose reaktive Polyurethan-Zusammensetzungen |
| JP6171467B2 (ja) * | 2013-03-27 | 2017-08-02 | Dic株式会社 | ラミネート用２液混合接着剤組成物 |
| FR3021659B1 (fr) | 2014-05-28 | 2017-11-17 | Bostik Sa | Composition de polyurethane a terminaisons nco a base de 2,4-tdi non thermofusible et a faible teneur en monomere tdi, comprenant au moins un compose isocyanate de volume molaire particulier. |
| FR3021658B1 (fr) * | 2014-05-28 | 2017-12-08 | Bostik Sa | Composition de polyurethane a terminaisons nco a base mdi non thermofusible et a faible teneur en monomere mdi, comprenant au moins un compose isocyanate de volume molaire particulier. |
| DE102014212999A1 (de) | 2014-07-04 | 2016-01-07 | Henkel Ag & Co. Kgaa | Polyurethan-Kaschierklebstoff enthaltend Füllstoffe |
| RU2696496C2 (ru) | 2015-02-03 | 2019-08-02 | Хенкель Аг Унд Ко. Кгаа | Полиуретановые клеящие составы для склеивания пленок с низкой поверхностной энергией |
| EP3067377B1 (en) | 2015-03-12 | 2023-01-18 | Henkel AG & Co. KGaA | Ultralow monomer polyurethanes |
| US11198803B2 (en) | 2015-07-31 | 2021-12-14 | Dow Global Technologies Llc | Aminobenzoate-terminated materials for laminated adhesives |
| FR3045616B1 (fr) * | 2015-12-21 | 2020-07-10 | Bostik Sa | Mastics polyurethane superelastiques |
| JP2019508529A (ja) | 2016-01-13 | 2019-03-28 | ヘンケル・アクチェンゲゼルシャフト・ウント・コムパニー・コマンディットゲゼルシャフト・アウフ・アクチェンＨｅｎｋｅｌ ＡＧ ＆ Ｃｏ． ＫＧａＡ | 充填剤を含有する反応性ポリウレタンホットメルト接着剤 |
| WO2018033551A1 (en) | 2016-08-19 | 2018-02-22 | Henkel Ag & Co. Kgaa | Method for preparing a hydrophobically modified clay |
| PL3327056T3 (pl) | 2016-11-25 | 2022-07-18 | Henkel Ag & Co. Kgaa | Szybko utwardzalna kompozycja kleju do laminowania o niskiej lepkości |
| PL3327057T3 (pl) | 2016-11-25 | 2025-07-21 | Henkel Ag & Co. Kgaa | Niezawierająca poliestru kompozycja kleju do kaszerowania |
| CN114921215A (zh) | 2016-11-25 | 2022-08-19 | 汉高股份有限及两合公司 | 不含聚酯的层合粘合剂组合物 |
| KR101937697B1 (ko) * | 2017-11-23 | 2019-01-14 | 태광산업주식회사 | 유색 폴리우레탄우레아 탄성섬유 제조 방법 |
| KR101943894B1 (ko) * | 2017-11-23 | 2019-01-30 | 태광산업주식회사 | 항염소성 흑색 폴리우레탄우레아 탄성섬유 제조방법 |
| EP3670576B8 (de) | 2018-12-19 | 2020-12-09 | Ems-Chemie Ag | Polyamid-formmassen für glasverbunde |
| ES2924345T3 (es) | 2019-05-20 | 2022-10-06 | Henkel Ag & Co Kgaa | Método para preparar una arcilla exfoliada por lo menos parcialmente utilizando un agente exfoliante que comprende un éster parcial de (meta)acrilato de poli(óxido de alquileno), un carbonato cíclico y agua |
| JP2021004343A (ja) * | 2019-06-27 | 2021-01-14 | ヘンケルジャパン株式会社 | ラミネート用接着剤 |
| US11732083B2 (en) | 2020-11-19 | 2023-08-22 | Covestro Llc | Polyisocyanate resins |
| JP2024501314A (ja) * | 2020-12-23 | 2024-01-11 | ピーターズ サージカル | Ｎｃｏ末端ウレタンプレプロポリマーを含む止血性の組織接着剤組成物 |
| WO2022179772A1 (en) | 2021-02-26 | 2022-09-01 | Henkel Ag & Co. Kgaa | Flame-retardant adhesive composition for structural wood bonding |
| CN116836362B (zh) * | 2023-08-02 | 2025-08-29 | 南京玖星旭能新材料有限责任公司 | 一种含多金属-氧簇的聚合物及其制备方法和应用 |
| BE1032688B1 (nl) * | 2024-06-11 | 2026-01-22 | Soudal | Reactieve polyurethaan formuleringen met een laag monomeer gehalte |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3839491A (en) * | 1972-12-14 | 1974-10-01 | Peritech Int Corp | Low volatility polyurethane prepolymer |
| DE2606419A1 (de) * | 1976-02-18 | 1977-08-25 | Basf Ag | Lagerbestaendige, fluessige carbodiimidgruppen aufweisende polyisocyanate und verfahren zu ihrer herstellung |
| JPS5742782A (en) * | 1980-08-28 | 1982-03-10 | Asahi Chem Ind Co Ltd | Preparation of organic polyisocyanate composition |
| DE3306559A1 (de) * | 1983-02-25 | 1984-08-30 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung von polyurethan-praepolymeren mit endstaendigen isocyanatgruppen und vermindertem restmonomergehalt |
| DE3401129A1 (de) * | 1984-01-14 | 1985-07-18 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung gemischter polyurethan-prepolymerer |
| US4952621A (en) * | 1988-06-06 | 1990-08-28 | The B. F. Goodrich Company | Urethane sealants or coating admixtures having improved shelf stability |
| DE4136490C2 (de) * | 1991-11-06 | 2003-04-30 | Bayer Ag | Lösungsmittelfreie Beschichtungssysteme |
| DE4232015A1 (de) * | 1992-09-24 | 1994-03-31 | Bayer Ag | Lösungsmittelfreie Zweikomponentenpolyurethanklebstoffsysteme |
| MX9701338A (es) * | 1994-08-22 | 1997-05-31 | Henkel Kgaa | Composiciones de poliuretano con bajo contenido endiisocianatos monomeros. |
| DE19645659A1 (de) * | 1996-11-06 | 1998-05-07 | Bayer Ag | Verfahren zur Isomerentrennung von Isocyanaten |
| DE19700014A1 (de) * | 1997-01-02 | 1998-07-09 | Henkel Kgaa | Monomerenarmes PU-Prepolymer |
| US5925781A (en) * | 1997-11-03 | 1999-07-20 | Bayer Corporation | Prepolymers with low monomeric TDI content |
| US6784242B2 (en) * | 1997-11-11 | 2004-08-31 | Henkel Kommanditgesellschaft Auf Aktien | Polyurethane binding agents having a low content of highly volatile monomers |
| DE10157488A1 (de) * | 2000-12-15 | 2002-06-20 | Henkel Kgaa | Polyurethan-Prepolymere mit NCO-Gruppen und niedrigem Gehalt an monomeren Polyisocyanat |
| DE10229519A1 (de) * | 2001-07-10 | 2003-01-30 | Henkel Kgaa | Reaktive Polyurethane mit einem geringen Gehalt an monomeren Diisocyanaten |
| DE10150722A1 (de) * | 2001-10-13 | 2003-04-30 | Henkel Kgaa | Reaktive Polyurethan-Zusammensetzungen mit niedrigem Restmonomergehalt |
| CA2471252A1 (en) * | 2001-12-18 | 2003-06-26 | Henkel Kommanditgesellschaft Auf Aktien | Method for producing polyurethane prepolymers having a low content of monomers |
| DE10163857A1 (de) * | 2001-12-22 | 2003-07-10 | Henkel Kgaa | Reaktive Polyurethane mit einem geringen Gehalt an monomeren Diisocyanaten |
| DE10206112A1 (de) * | 2002-02-13 | 2003-08-21 | Basf Ag | Wässrige Dispersionen, aufgebaut aus Polycarbodiimiden |
| DE10358932A1 (de) * | 2002-12-17 | 2005-07-28 | Henkel Kgaa | Verfahren zur Herstellung von Polyurethan-Prepolymeren in Gegenwart eines Katalysators |
-
2004
- 2004-04-08 DE DE102004018048A patent/DE102004018048A1/de not_active Ceased
-
2005
- 2005-03-03 WO PCT/EP2005/002205 patent/WO2005097861A1/de not_active Ceased
- 2005-03-03 CN CN2005800107277A patent/CN1938353B/zh not_active Expired - Fee Related
- 2005-03-03 EP EP05728218A patent/EP1732966A1/de not_active Withdrawn
- 2005-03-03 BR BRPI0509703-7A patent/BRPI0509703A/pt not_active IP Right Cessation
-
2006
- 2006-10-09 US US11/539,728 patent/US20070129525A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| WO2005097861A1 (de) | 2005-10-20 |
| CN1938353B (zh) | 2011-04-27 |
| US20070129525A1 (en) | 2007-06-07 |
| CN1938353A (zh) | 2007-03-28 |
| EP1732966A1 (de) | 2006-12-20 |
| DE102004018048A1 (de) | 2005-11-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B25D | Requested change of name of applicant approved |
Owner name: HENKEL AG AND CO. KGAA (DE) Free format text: NOME ALTERADO DE: HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN |
|
| B08F | Application fees: application dismissed [chapter 8.6 patent gazette] |
Free format text: REFERENTE AS ANUIDADES |
|
| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2311 DE 22-04-2015 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |