BRPI0516831A - processo para a purificação de 1,4- butanodiol - Google Patents

processo para a purificação de 1,4- butanodiol

Info

Publication number
BRPI0516831A
BRPI0516831A BRPI0516831-7A BRPI0516831A BRPI0516831A BR PI0516831 A BRPI0516831 A BR PI0516831A BR PI0516831 A BRPI0516831 A BR PI0516831A BR PI0516831 A BRPI0516831 A BR PI0516831A
Authority
BR
Brazil
Prior art keywords
butanediol
stream
feed
purification
hydroxybutoxy
Prior art date
Application number
BRPI0516831-7A
Other languages
English (en)
Inventor
Michael Anthony Wood
Robert Wild
Simon Wayne Jackson
Original Assignee
Davy Process Techn Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Davy Process Techn Ltd filed Critical Davy Process Techn Ltd
Publication of BRPI0516831A publication Critical patent/BRPI0516831A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/26—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D307/30—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/32—Oxygen atoms
    • C07D307/33—Oxygen atoms in position 2, the oxygen atom being in its keto or unsubstituted enol form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C07C29/90—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound using hydrogen only
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/04—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D307/06—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
    • C07D307/08—Preparation of tetrahydrofuran
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/04—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D307/18—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/20—Oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PROCESSO PARA A PURIFICAçãO DE 1,4-BUTANODIOL. Um processo para a purificação de uma corrente de alimentação líquida bruta, compreendendo 1,4-butanodiol e uma pequena quantidade de 2-(4-hidroxibutóxi)- tetraidrofurano e/ou seus precursores, em que o processo compreende passar a alimentação bruta na presença de hidrogênio numa zona reacional sobre um catalisador heterogêneo de cobre tolerante a líquido na fase líquida em condições de hidrogenação e recuperando uma corrente purificada de 1,4-butanodiol com uma pequena quantidade de 2-(4-hidroxibutóxi) - tetraidrofurano do que a corrente de alimentação líquida bruta.
BRPI0516831-7A 2004-10-01 2005-09-29 processo para a purificação de 1,4- butanodiol BRPI0516831A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB0421928.3A GB0421928D0 (en) 2004-10-01 2004-10-01 Process
PCT/GB2005/003741 WO2006037957A1 (en) 2004-10-01 2005-09-29 Process for the purification of 1, 4-butanediol

Publications (1)

Publication Number Publication Date
BRPI0516831A true BRPI0516831A (pt) 2008-09-23

Family

ID=33427974

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0516831-7A BRPI0516831A (pt) 2004-10-01 2005-09-29 processo para a purificação de 1,4- butanodiol

Country Status (16)

Country Link
US (1) US8129548B2 (pt)
EP (1) EP1794109B1 (pt)
JP (1) JP5526335B2 (pt)
KR (1) KR101223949B1 (pt)
CN (1) CN101052607B (pt)
AR (1) AR051378A1 (pt)
AU (1) AU2005291129B2 (pt)
BR (1) BRPI0516831A (pt)
CA (1) CA2581539C (pt)
EA (1) EA013753B1 (pt)
GB (1) GB0421928D0 (pt)
MX (1) MX2007003969A (pt)
NO (1) NO20072248L (pt)
TW (1) TWI353350B (pt)
WO (1) WO2006037957A1 (pt)
ZA (1) ZA200702523B (pt)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0803663D0 (en) * 2008-02-28 2008-04-09 Davy Process Techn Ltd Process
CN102649688B (zh) * 2011-02-25 2014-08-13 中国石油化工股份有限公司 乙二醇产品纯化的方法
CN102649692B (zh) * 2011-02-25 2015-10-21 中国石油化工股份有限公司 提高乙二醇质量的方法
CN102649687B (zh) * 2011-02-25 2014-11-26 中国石油化工股份有限公司 提高乙二醇产品质量的方法
TWI535711B (zh) * 2011-07-04 2016-06-01 三菱化學股份有限公司 四氫呋喃之製造方法
WO2013005748A1 (ja) * 2011-07-04 2013-01-10 三菱化学株式会社 １，４－ブタンジオールの製造方法
CN103635469B (zh) 2011-07-04 2015-05-06 三菱化学株式会社 四氢呋喃的制造方法
WO2013012048A1 (ja) * 2011-07-20 2013-01-24 三菱化学株式会社 １，４－ブタンジオールの製造方法
GB201115617D0 (en) * 2011-09-09 2011-10-26 Davy Process Techn Ltd Proacess
CN103044197B (zh) * 2011-10-17 2015-07-22 中国石油化工股份有限公司 一种1,4-丁二醇纯化并联产γ-丁内酯的工艺方法
EP2782893B1 (en) 2011-11-25 2017-08-23 Conser SPA Process for producing 1,4-butanediol, gamma-butyrolactone and tetrahydrofuran by hydrogenating dialkyl maleate in mixed liquid/vapor phase
US20130296585A1 (en) 2012-03-30 2013-11-07 Basf Corporation Catalyst For Tetrahydrofuran Synthesis
US20220135729A1 (en) * 2019-03-05 2022-05-05 Asahi Kasei Kabushiki Kaisha Polycarbonate diols
CN114436778B (zh) * 2020-10-31 2024-08-06 中国石油化工股份有限公司 一种缩醛加氢精制1,4-丁二醇的方法
IT202000031979A1 (it) * 2020-12-22 2022-06-22 Novamont Spa Processo di purificazione di una miscela comprendente dioli e acetali
US20240287011A1 (en) * 2021-06-25 2024-08-29 Cj Cheiljedang Corporation Method for producing tetrahydrofuran, gamma-butyrolactone, or 1,4-butanediol
KR102604948B1 (ko) * 2021-06-25 2023-11-23 씨제이제일제당(주) 테트라하이드로퓨란, 감마부티로락톤 또는 1,4-부탄디올의 제조 방법
CN113731442B (zh) * 2021-08-20 2024-02-02 河南省生物基材料产业研究院有限公司 一种马来酸二甲酯加氢反应催化剂及其制备方法和应用
GB202203264D0 (en) 2022-03-09 2022-04-20 Johnson Matthey Davy Technologies Ltd Process for producing a refined 1,4-butanediol stream
CN114874074B (zh) * 2022-05-27 2023-06-13 辽宁石油化工大学 一种1,4-丁二醇的分离纯化工艺与系统
CN115716778A (zh) * 2022-10-10 2023-02-28 新疆蓝山屯河能源有限公司 低温纯化结晶提升bdo纯度的方法及装置
CN118561661A (zh) * 2024-05-06 2024-08-30 内蒙古东景生物环保科技有限公司 一种1,4-丁二醇的提纯方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE366084A (pt) 1928-12-15
GB8331793D0 (en) * 1983-11-29 1984-01-04 Davy Mckee Ltd Process
GB8514002D0 (en) * 1985-06-04 1985-07-10 Davy Mckee Ltd Process
GB8618888D0 (en) * 1986-08-01 1986-09-10 Davy Mckee Ltd Process
WO1988000937A1 (en) 1986-08-01 1988-02-11 Davy Mckee (London) Limited Process for the co-production of butane-1,4-diol and gamma-butyrolactone
DE69027304T2 (de) 1989-01-17 1997-01-23 Davy Process Technology Ltd., London Kontinuierliches Verfahren zur Herstellung von Carbonsäureestern
DE3909485A1 (de) * 1989-03-22 1990-09-27 Basf Ag Verfahren zur herstellung von butandiol-1,4 und tetrahydrofuran
JP3175360B2 (ja) * 1992-12-10 2001-06-11 三菱化学株式会社 １，４−ブタンジオールの精製方法
TW366335B (en) 1996-03-29 1999-08-11 Kvaerner Process Tech Ltd Process for the purification of butane-1,4-diol
KR100500858B1 (ko) * 1996-03-29 2005-11-08 데이비 프로세스 테크놀로지 리미티드 부탄-1,4-디올의정제방법
ZA973972B (en) 1996-05-14 1998-03-23 Kvaerner Process Tech Ltd A process for the production of at least one C4 compound selected from butane-1,4-diol, gamma-butyrolactone and tetrahydrofuran.
ZA973971B (en) 1996-05-15 1998-03-23 Kvaerner Process Tech Ltd A process for the production of at least one C4 compound selected from butane-1,4-diol, gamma-butyrolactone and tetrahydrofuran.
SG65043A1 (en) * 1997-01-23 1999-05-25 Mitsubishi Chem Corp Process for purifying crude 1,4-butanediol
US5981810A (en) 1997-06-16 1999-11-09 Mitsubishi Chemical Corporation Process for preparing 1,4-butanediol
GB9724004D0 (en) 1997-11-13 1998-10-21 Kvaerner Process Tech Ltd Process
GB9724195D0 (en) 1997-11-14 1998-01-14 Kvaerner Process Tech Ltd Process
DE19809493A1 (de) * 1998-03-05 1999-09-09 Basf Ag Verfahren zur Destillation Butandiol-haltiger Gemische
EP0962438B1 (en) 1998-03-23 2001-06-06 Basf Aktiengesellschaft Process for the preparation of 1,4-butanediol, butyrolactone and tetrahydrofuran.
MY139259A (en) 1999-10-12 2009-09-30 Kvaerner Process Tech Ltd Process
EP1108702A1 (en) * 1999-12-13 2001-06-20 Kvaerner Process Technology Limited Process for the co-production of aliphatic diols and cyclic ethers
GB0117090D0 (en) 2001-07-12 2001-09-05 Kvaerner Process Tech Ltd Process
JP3998440B2 (ja) * 2001-07-17 2007-10-24 三菱化学株式会社 １，４−ブタンジオールの製造方法
GB0325526D0 (en) 2003-10-31 2003-12-03 Davy Process Techn Ltd Process
GB0325530D0 (en) 2003-10-31 2003-12-03 Davy Process Techn Ltd Process
GB0329152D0 (en) 2003-12-16 2004-01-21 Davy Process Techn Ltd Process

Also Published As

Publication number Publication date
AU2005291129A1 (en) 2006-04-13
KR20070059116A (ko) 2007-06-11
CA2581539A1 (en) 2006-04-13
MX2007003969A (es) 2007-05-11
TW200621688A (en) 2006-07-01
US20070260073A1 (en) 2007-11-08
TWI353350B (en) 2011-12-01
EA013753B1 (ru) 2010-06-30
JP5526335B2 (ja) 2014-06-18
NO20072248L (no) 2007-04-30
ZA200702523B (en) 2009-01-28
CN101052607A (zh) 2007-10-10
KR101223949B1 (ko) 2013-01-18
EP1794109B1 (en) 2016-02-03
EA200700713A1 (ru) 2007-08-31
WO2006037957A1 (en) 2006-04-13
AR051378A1 (es) 2007-01-10
AU2005291129B2 (en) 2011-09-22
US8129548B2 (en) 2012-03-06
CA2581539C (en) 2013-06-18
EP1794109A1 (en) 2007-06-13
CN101052607B (zh) 2012-06-20
GB0421928D0 (en) 2004-11-03
JP2008514684A (ja) 2008-05-08

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Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: INDEFIRO O PEDIDO DE ACORDO COM O(S) ARTIGO(S) 8O E 13 DA LPI.

B12B Appeal: appeal against refusal [chapter 12.2 patent gazette]
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]
B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]