BRPI0607725A2 - agente de absorção de água, artigo para absorção de àgua e método para a produção de um agente de absorção de àgua - Google Patents
agente de absorção de água, artigo para absorção de àgua e método para a produção de um agente de absorção de àguaInfo
- Publication number
- BRPI0607725A2 BRPI0607725A2 BRPI0607725-0A BRPI0607725A BRPI0607725A2 BR PI0607725 A2 BRPI0607725 A2 BR PI0607725A2 BR PI0607725 A BRPI0607725 A BR PI0607725A BR PI0607725 A2 BRPI0607725 A2 BR PI0607725A2
- Authority
- BR
- Brazil
- Prior art keywords
- water
- agent
- water absorbing
- particle size
- producing
- Prior art date
Links
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/60—Liquid-swellable gel-forming materials, e.g. super-absorbents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
- B01J20/26—Synthetic macromolecular compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
- B01J20/26—Synthetic macromolecular compounds
- B01J20/264—Synthetic macromolecular compounds derived from different types of monomers, e.g. linear or branched copolymers, block copolymers, graft copolymers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
- B01J20/26—Synthetic macromolecular compounds
- B01J20/265—Synthetic macromolecular compounds modified or post-treated polymers
- B01J20/267—Cross-linked polymers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
- B01J20/28004—Sorbent size or size distribution, e.g. particle size
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
- B01J20/2803—Sorbents comprising a binder, e.g. for forming aggregated, agglomerated or granulated products
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
- B01J20/28047—Gels
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3028—Granulating, agglomerating or aggregating
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
- C08J3/245—Differential crosslinking of one polymer with one crosslinking type, e.g. surface crosslinking
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
- B01J2220/68—Superabsorbents
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2300/00—Characterised by the use of unspecified polymers
- C08J2300/14—Water soluble or water swellable polymers, e.g. aqueous gels
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2991—Coated
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2991—Coated
- Y10T428/2998—Coated including synthetic resin or polymer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Materials Engineering (AREA)
- Epidemiology (AREA)
- Hematology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Veterinary Medicine (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Absorbent Articles And Supports Therefor (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
AGENTE DE ABSORçãO DE AGUA, ARTIGO PARA ABSORçãO DE áGUA E MéTODO PARA A PRODUçãO DE UM AGENTE DE ABSORçãO DE áGUA. Um objeto da presente invenção compreende proporcionar um agente de absorção de água que possui uma pequena quantidade de monâmero residual, uma pequena varlância da quantidade de monómero residual entre as faixas de distribuição de tamanho de partícula e propriedades de absorção favoráveis e de características sanitárias; um artigo absorvente; e um método para a produção de um agente de absorção de água. O agente de absorção de água da presente invenção possui uma quantidade de monómero residual que não é superior a 500ppm, e um índice de monómero residual que não é maior do que 0,30. O método para produção inclui uma primeira etapa de obtenção do polímero hidrogel para polimerização de uma solução aquosa de um monómero que inclui um ácido carboxílico insaturado e/ou um sal do referido ácido na presença de um agente de reticulação; uma segunda etapa de obtenção de um precursor de uma resina de absorção de água que está na forma de pó e inclui partículas que possuem um tamanho de partícula de 300 a 850 <sym>m e partículas que possuem um tamanho de partícula menor do que 300<sym>m como componentes principais por meio de secagem do polimero hidrogel seguida de pulverização e classificação para ajustar a distribuição de tamanho de partícula, uma terceira etapa para obtenção de uma resina de absorção de água por meio de aquecimento de uma mistura do precursor da resina de absorção de água e um agente reticulador de superfície que pode formar uma ligação éster ao redor da superfície do precursor da resina de absorção de água, uma quarta etapa em que é su}netida a mistura da resina de absorção de água e a solução aquosa a um tratamento térmico sob um fluxo de ar não inferior a 40°C, mas não superior a 120°C.
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2005-038123 | 2005-02-15 | ||
| JP2005038123 | 2005-02-15 | ||
| JP2005-089307 | 2005-03-25 | ||
| JP2005089307 | 2005-03-25 | ||
| PCT/JP2006/302782 WO2006088115A1 (en) | 2005-02-15 | 2006-02-10 | Water absorbing agent, water absorbing article and method for production of water absorbing agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BRPI0607725A2 true BRPI0607725A2 (pt) | 2009-10-06 |
| BRPI0607725B1 BRPI0607725B1 (pt) | 2017-07-04 |
Family
ID=36407948
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0607725-0A BRPI0607725B1 (pt) | 2005-02-15 | 2006-02-10 | Water absorption agent, water absorption article and method for the production of an agent for water absorption |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US8182916B2 (pt) |
| EP (2) | EP1690887B1 (pt) |
| JP (3) | JP5625003B2 (pt) |
| KR (1) | KR20070104663A (pt) |
| CN (1) | CN104086938B (pt) |
| AU (1) | AU2006216015A1 (pt) |
| BR (1) | BRPI0607725B1 (pt) |
| DE (1) | DE602006001215D1 (pt) |
| RU (1) | RU2364611C2 (pt) |
| SG (1) | SG159540A1 (pt) |
| TW (1) | TWI406883B (pt) |
| WO (1) | WO2006088115A1 (pt) |
Families Citing this family (74)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PT1793187E (pt) * | 2004-09-21 | 2012-03-05 | Joan Vives Iglesias | Processo e máquina destinados à sinterização e/ou secagem de materiais em pó utilizando uma radiação infravermelha |
| TW200712114A (en) * | 2005-09-30 | 2007-04-01 | Nippon Catalytic Chem Ind | Method for manufacturing particulate water-absorbing agent and particulate water-absorbing agent |
| EP2013251B1 (en) | 2006-03-27 | 2011-09-14 | Nippon Shokubai Co.,Ltd. | Water absorbing resin with improved internal structure and manufacturing method therefor |
| US9593212B2 (en) | 2006-09-29 | 2017-03-14 | Nippon Shokubai Co., Ltd. | Method for producing water absorbent resin particle |
| US20080127996A1 (en) * | 2006-12-04 | 2008-06-05 | Weinhold Dennis G | Method and apparatus to remediate an acid and/or liquid spill |
| EP2115014B1 (de) * | 2007-02-06 | 2019-01-16 | Basf Se | Verfahren zur herstellung wasserabsorbierender polymerpartikel durch polymerisation von tropfen einer monomerlösung |
| CN101605818B (zh) * | 2007-02-06 | 2012-10-03 | 巴斯夫欧洲公司 | 通过聚合单体溶液的液滴生产吸水性聚合物颗粒的方法 |
| WO2009041727A1 (en) * | 2007-09-28 | 2009-04-02 | Nippon Shokubai Co., Ltd. | Water absorbing agent and production method thereof |
| ES2398736T3 (es) * | 2007-10-24 | 2013-03-21 | Sumitomo Seika Chemicals Co. Ltd. | Procedimiento para la produccion de resinas hidro-absorbentes y las resinas hidro-absorbentes obtenidas |
| CN102066431B (zh) | 2008-06-19 | 2012-10-03 | 巴斯夫欧洲公司 | 连续制备吸水性聚合物颗粒的方法 |
| JP5290413B2 (ja) † | 2008-07-15 | 2013-09-18 | ビーエーエスエフ ソシエタス・ヨーロピア | 吸水性ポリマー粒子の製造方法 |
| EP2471847B2 (en) | 2009-08-28 | 2018-01-03 | Nippon Shokubai Co., Ltd. | Process for production of water-absorbable resin |
| CN102498134B (zh) * | 2009-09-16 | 2013-10-30 | 株式会社日本触媒 | 吸水性树脂粉末的制造方法 |
| JP5731390B2 (ja) | 2009-09-30 | 2015-06-10 | 株式会社日本触媒 | ポリアクリル酸(塩)系吸水性樹脂およびその製造方法 |
| WO2011040530A1 (ja) | 2009-09-30 | 2011-04-07 | 株式会社日本触媒 | 粒子状吸水剤及びその製造方法 |
| WO2011042468A2 (de) | 2009-10-09 | 2011-04-14 | Basf Se | Verfahren zur nachbefeuchtung oberflächennachvernetzter wasserabsorbierender polymerpartikel |
| CN102666670B (zh) | 2009-10-09 | 2014-02-19 | 巴斯夫欧洲公司 | 再润湿表面后交联的吸水性聚合物颗粒的方法 |
| KR101895624B1 (ko) | 2009-12-24 | 2018-09-05 | 가부시키가이샤 닛폰 쇼쿠바이 | 폴리아크릴산계 흡수성 수지분말 및 그 제조방법 |
| US8623994B2 (en) | 2010-01-20 | 2014-01-07 | Nippon Shokubai, Co., Ltd. | Method for producing water absorbent resin |
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| WO2011099586A1 (ja) | 2010-02-10 | 2011-08-18 | 株式会社日本触媒 | 吸水性樹脂粉末の製造方法 |
| JP5658229B2 (ja) | 2010-03-08 | 2015-01-21 | 株式会社日本触媒 | 粒子状含水ゲル状架橋重合体の乾燥方法 |
| JP5632906B2 (ja) | 2010-03-12 | 2014-11-26 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| US9453091B2 (en) | 2010-03-17 | 2016-09-27 | Nippon Shokubai Co., Ltd. | Method of producing water absorbent resin |
| BR112012027406B1 (pt) | 2010-04-26 | 2021-02-09 | Nippon Shokubai Co., Ltd. | resina absorvedora de água tipo ácido poliacrílico (sal), material sanitário e método para produzir a referida resina |
| BR112012027407B1 (pt) | 2010-04-26 | 2020-04-07 | Nippon Shokubai Co., Ltd. | resina absorvedora de água tipo ácido poliacrílico (sal), material sanitário contendo a mesma, método para produzir e identificar a mesma e método para produzir ácido poliacrílico (sal) |
| EP2565219B1 (en) | 2010-04-27 | 2018-06-27 | Nippon Shokubai Co., Ltd. | Method for producing polyacrylic acid (salt)-based water absorbent resin powder |
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| US8507620B2 (en) * | 2010-06-08 | 2013-08-13 | Lg Display Co., Ltd. | Process for preparing water absorbent resin with high performance |
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-
2006
- 2006-02-10 KR KR1020077021214A patent/KR20070104663A/ko not_active Ceased
- 2006-02-10 RU RU2007134385/04A patent/RU2364611C2/ru not_active IP Right Cessation
- 2006-02-10 EP EP06002737A patent/EP1690887B1/en not_active Expired - Lifetime
- 2006-02-10 DE DE602006001215T patent/DE602006001215D1/de not_active Expired - Lifetime
- 2006-02-10 EP EP06713923.8A patent/EP1848758B2/en not_active Expired - Lifetime
- 2006-02-10 TW TW095104551A patent/TWI406883B/zh active
- 2006-02-10 BR BRPI0607725-0A patent/BRPI0607725B1/pt active IP Right Grant
- 2006-02-10 SG SG201000922-3A patent/SG159540A1/en unknown
- 2006-02-10 CN CN201410264575.4A patent/CN104086938B/zh not_active Expired - Lifetime
- 2006-02-10 WO PCT/JP2006/302782 patent/WO2006088115A1/en not_active Ceased
- 2006-02-10 US US11/816,200 patent/US8182916B2/en active Active
- 2006-02-10 AU AU2006216015A patent/AU2006216015A1/en not_active Abandoned
- 2006-02-14 US US11/353,238 patent/US20060183828A1/en not_active Abandoned
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2012
- 2012-01-06 JP JP2012001296A patent/JP5625003B2/ja not_active Expired - Lifetime
-
2013
- 2013-09-27 JP JP2013202582A patent/JP5903086B2/ja not_active Expired - Lifetime
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- 2015-11-13 JP JP2015223284A patent/JP6025953B2/ja not_active Expired - Lifetime
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| WO2006088115A1 (en) | 2006-08-24 |
| US20060183828A1 (en) | 2006-08-17 |
| JP2014039927A (ja) | 2014-03-06 |
| TWI406883B (zh) | 2013-09-01 |
| JP6025953B2 (ja) | 2016-11-16 |
| EP1848758B2 (en) | 2021-02-17 |
| RU2007134385A (ru) | 2009-03-27 |
| JP5625003B2 (ja) | 2014-11-12 |
| EP1848758A1 (en) | 2007-10-31 |
| EP1690887A1 (en) | 2006-08-16 |
| JP5903086B2 (ja) | 2016-04-13 |
| US20100062252A1 (en) | 2010-03-11 |
| AU2006216015A1 (en) | 2006-08-24 |
| EP1848758B1 (en) | 2012-11-07 |
| KR20070104663A (ko) | 2007-10-26 |
| JP2012086221A (ja) | 2012-05-10 |
| CN104086938B (zh) | 2017-09-19 |
| BRPI0607725B1 (pt) | 2017-07-04 |
| US8182916B2 (en) | 2012-05-22 |
| TW200706566A (en) | 2007-02-16 |
| CN104086938A (zh) | 2014-10-08 |
| SG159540A1 (en) | 2010-03-30 |
| EP1848758A4 (en) | 2011-11-30 |
| DE602006001215D1 (de) | 2008-07-03 |
| EP1690887B1 (en) | 2008-05-21 |
| RU2364611C2 (ru) | 2009-08-20 |
| JP2016033224A (ja) | 2016-03-10 |
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