BRPI0715691B8 - método para a produção de ácido acético - Google Patents
método para a produção de ácido acéticoInfo
- Publication number
- BRPI0715691B8 BRPI0715691B8 BRPI0715691A BRPI0715691A BRPI0715691B8 BR PI0715691 B8 BRPI0715691 B8 BR PI0715691B8 BR PI0715691 A BRPI0715691 A BR PI0715691A BR PI0715691 A BRPI0715691 A BR PI0715691A BR PI0715691 B8 BRPI0715691 B8 BR PI0715691B8
- Authority
- BR
- Brazil
- Prior art keywords
- acetic acid
- production
- impurities
- acetals
- column
- Prior art date
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title abstract 12
- 238000000034 method Methods 0.000 title abstract 3
- 239000012535 impurity Substances 0.000 abstract 3
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 abstract 2
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 1
- -1 hydroxyl compound Chemical class 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 238000000197 pyrolysis Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
patente de invenção: "purificação de ácido acético". a presente invenção refere-se a um método para remoção de impurezas de aldeído de uma corrente de ácido acético. o método compreende a reação de impurezas de aldeído com um composto hidroxila em uma coluna de destilação a seco ou em uma coluna combinada para formar acetais correspondentes. os acetais são subsequentemente removidos como impurezas pesadas de ácido acético por destilação.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/508,109 | 2006-08-22 | ||
| US11/508,109 US7485749B2 (en) | 2006-08-22 | 2006-08-22 | Preparation of acetic acid |
| PCT/US2007/017562 WO2008024198A1 (en) | 2006-08-22 | 2007-08-07 | Purification of acetic acid |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| BRPI0715691A2 BRPI0715691A2 (pt) | 2013-08-06 |
| BRPI0715691B1 BRPI0715691B1 (pt) | 2017-01-31 |
| BRPI0715691B8 true BRPI0715691B8 (pt) | 2017-09-26 |
Family
ID=38802349
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0715691A BRPI0715691B8 (pt) | 2006-08-22 | 2007-08-07 | método para a produção de ácido acético |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US7485749B2 (pt) |
| EP (1) | EP2069281B1 (pt) |
| CN (1) | CN101506137B (pt) |
| BR (1) | BRPI0715691B8 (pt) |
| WO (1) | WO2008024198A1 (pt) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7485749B2 (en) | 2006-08-22 | 2009-02-03 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
| DE102006043587A1 (de) * | 2006-09-16 | 2008-03-27 | Symrise Gmbh & Co. Kg | 2-Methyl-2-alkenyl-substituierte 1,3-Dioxane als Riechstoffe |
| US7619113B2 (en) * | 2007-09-27 | 2009-11-17 | Celanese International Corporation | Method and apparatus for making acetic acid with improved purification |
| US7812191B2 (en) | 2008-05-07 | 2010-10-12 | Lyondell Chemical Technology, L.P. | Removing hydrocarbon impurities from acetic acid by ionic liquid extraction |
| US8076512B2 (en) | 2009-08-27 | 2011-12-13 | Equistar Chemicals, L.P. | Preparation of acetic acid |
| US8431740B2 (en) | 2010-07-21 | 2013-04-30 | Equistar Chemicals, Lp | Controlling decanter phase separation of acetic acid production process |
| US9102612B2 (en) * | 2012-06-25 | 2015-08-11 | Lyondellbasell Acetyls, Llc | Process for the production of acetic acid |
| US8969613B2 (en) | 2012-10-31 | 2015-03-03 | Lyondellbasell Acetyls, Llc | Removal of aldehydes in acetic acid production |
| KR102281510B1 (ko) * | 2017-03-22 | 2021-07-26 | 주식회사 다이셀 | 아세트산의 제조 방법 |
| MY189357A (en) * | 2017-03-28 | 2022-02-07 | Daicel Corp | Method for producing acetic acid |
| US10584087B2 (en) | 2018-03-23 | 2020-03-10 | Lyondellbasell Acetyls, Llc | Removal of permanganate reducing compounds from intermediate GAA process streams |
| CN111918857A (zh) * | 2018-03-23 | 2020-11-10 | 利安德巴塞尔乙酰有限责任公司 | 冰乙酸(gaa)纯化的改进方法 |
| CN111822050B (zh) * | 2020-07-16 | 2022-07-12 | 万华化学集团股份有限公司 | 一种羰基化反应催化剂组合物及制备新戊二醇的方法 |
| US20230265036A1 (en) * | 2022-02-18 | 2023-08-24 | Lyondellbasell Acetyls, Llc | Removal of aldehydes in acetic acid production |
| CN117942722A (zh) * | 2024-03-27 | 2024-04-30 | 河北建滔能源发展有限公司 | 一种用于去除醋酸中醛类杂质的脱醛塔 |
| CN118287080B (zh) | 2024-06-06 | 2024-09-17 | 北京化工大学 | 一种生物基己二酸的制备方法 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3769329A (en) | 1970-03-12 | 1973-10-30 | Monsanto Co | Production of carboxylic acids and esters |
| US4358347A (en) | 1982-01-26 | 1982-11-09 | The Dow Chemical Company | Removal of trace aldehydes from carboxylic acids |
| US5202481A (en) | 1987-12-23 | 1993-04-13 | Hoechst Celanese Corporation | Purification of acetic acid produced by the low water carbonylation of methanol by treatment with ozone |
| US5155265A (en) | 1987-12-23 | 1992-10-13 | Hoechst Celanese Corporation | Purification of acetic acid with ozone followed by treatment with activated carbon and/or an ion-exchange resin |
| CA1313676C (en) | 1987-12-23 | 1993-02-16 | Mark Owen Scates | Purification of acetic acid with ozone |
| US5155266A (en) | 1987-12-23 | 1992-10-13 | Hoechst Celanese Corporation | Purification of acetic acid with ozone in the presence of an oxidation catalyst |
| GB9100216D0 (en) * | 1991-01-05 | 1991-02-20 | Bp Chem Int Ltd | Process |
| AU639630B2 (en) * | 1991-01-28 | 1993-07-29 | Celanese International Corporation | Removal of carbonyl impurities from carbonylation process stream |
| GB9211671D0 (en) * | 1992-06-02 | 1992-07-15 | Bp Chem Int Ltd | Process |
| DE4327011A1 (de) * | 1993-08-12 | 1995-02-16 | Hoechst Ag | Verfahren zur Entfernung von Aldehyden und Acetalen aus technisch hergestellter Essigsäure |
| SG44317A1 (en) * | 1994-06-15 | 1997-12-19 | Daicel Chem | Process for producing high purity acetic acid |
| US5783731A (en) * | 1995-09-11 | 1998-07-21 | Hoechst Celanese Corporation | Removal of carbonyl impurities from a carbonylation process stream |
| US5817869A (en) * | 1995-10-03 | 1998-10-06 | Quantum Chemical Corporation | Use of pentavalent Group VA oxides in acetic acid processing |
| US6339171B1 (en) * | 1996-10-18 | 2002-01-15 | Celanese International Corporation | Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream |
| GB9625335D0 (en) * | 1996-12-05 | 1997-01-22 | Bp Chem Int Ltd | Process |
| EP0952141B1 (en) * | 1998-04-25 | 2002-06-05 | BP Chemicals Limited | Purification process |
| CN1113845C (zh) * | 1998-05-27 | 2003-07-09 | 千年石油化工公司 | 五价va族氧化物在乙酸制备方法中的应用 |
| US6323364B1 (en) * | 1999-08-31 | 2001-11-27 | Celanese International Corporation | Rhodium/inorganic iodide catalyst system for methanol carbonylation process with improved impurity profile |
| US6667418B2 (en) * | 2002-04-16 | 2003-12-23 | Celanese International Corporation | Oxidation treatment of a recycle stream in production of acetic acid by methanol carbonylation |
| US7485749B2 (en) | 2006-08-22 | 2009-02-03 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
-
2006
- 2006-08-22 US US11/508,109 patent/US7485749B2/en not_active Expired - Fee Related
-
2007
- 2007-08-07 BR BRPI0715691A patent/BRPI0715691B8/pt not_active IP Right Cessation
- 2007-08-07 CN CN200780030995.4A patent/CN101506137B/zh not_active Expired - Fee Related
- 2007-08-07 EP EP07811151.5A patent/EP2069281B1/en not_active Not-in-force
- 2007-08-07 WO PCT/US2007/017562 patent/WO2008024198A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| BRPI0715691A2 (pt) | 2013-08-06 |
| CN101506137A (zh) | 2009-08-12 |
| CN101506137B (zh) | 2013-05-15 |
| WO2008024198A1 (en) | 2008-02-28 |
| EP2069281B1 (en) | 2018-10-03 |
| EP2069281A1 (en) | 2009-06-17 |
| US7485749B2 (en) | 2009-02-03 |
| US20080051601A1 (en) | 2008-02-28 |
| BRPI0715691B1 (pt) | 2017-01-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B09X | Republication of the decision to grant [chapter 9.1.3 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] | ||
| B16C | Correction of notification of the grant [chapter 16.3 patent gazette] | ||
| B25A | Requested transfer of rights approved | ||
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 14A ANUIDADE. |
|
| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2631 DE 08-06-2021 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |