BRPI0910801A2 - processo e dispositivo para a recuperação de etilenoglicol na preparação de poli (tereftalato de etileno ) - Google Patents

processo e dispositivo para a recuperação de etilenoglicol na preparação de poli (tereftalato de etileno )

Info

Publication number: BRPI0910801A2
Authority: BR; Brazil
Prior art keywords: ethylene glycol; waste water; process waste; collecting tank; rectification column
Prior art date: 2008-08-18

Application number

BRPI0910801A

Other languages

English (en)

Inventor

Randolf Reimann

Rolf Ambrassat

Original Assignee

Lurgi Zimmer Gmbh

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2008-08-18

Filing date

2009-06-05

Publication date

2015-10-06

2009-06-05 Application filed by Lurgi Zimmer Gmbh filed Critical Lurgi Zimmer Gmbh

2015-10-06 Publication of BRPI0910801A2 publication Critical patent/BRPI0910801A2/pt

2019-07-02 Publication of BRPI0910801B1 publication Critical patent/BRPI0910801B1/pt

Links

LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title abstract 42
238000000034 method Methods 0.000 title abstract 16
-1 polyethylene terephthalate Polymers 0.000 title abstract 4
229920000139 polyethylene terephthalate Polymers 0.000 title abstract 4
239000005020 polyethylene terephthalate Substances 0.000 title abstract 4
238000011084 recovery Methods 0.000 title 1
239000002351 wastewater Substances 0.000 abstract 13
HTWIZMNMTWYQRN-UHFFFAOYSA-N 2-methyl-1,3-dioxolane Chemical compound CC1OCCO1 HTWIZMNMTWYQRN-UHFFFAOYSA-N 0.000 abstract 11
KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 abstract 6
239000012530 fluid Substances 0.000 abstract 5
LLLVZDVNHNWSDS-UHFFFAOYSA-N 4-methylidene-3,5-dioxabicyclo[5.2.2]undeca-1(9),7,10-triene-2,6-dione Chemical compound C1(C2=CC=C(C(=O)OC(=C)O1)C=C2)=O LLLVZDVNHNWSDS-UHFFFAOYSA-N 0.000 abstract 4
238000005886 esterification reaction Methods 0.000 abstract 4
239000000356 contaminant Substances 0.000 abstract 3
239000000203 mixture Substances 0.000 abstract 3
IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 abstract 2
238000003776 cleavage reaction Methods 0.000 abstract 2
230000032050 esterification Effects 0.000 abstract 2
230000003301 hydrolyzing effect Effects 0.000 abstract 2
238000004519 manufacturing process Methods 0.000 abstract 2
230000007017 scission Effects 0.000 abstract 2
238000000926 separation method Methods 0.000 abstract 2
238000005809 transesterification reaction Methods 0.000 abstract 2
238000011144 upstream manufacturing Methods 0.000 abstract 2
IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 abstract 1
DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 abstract 1
125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 abstract 1
230000005465 channeling Effects 0.000 abstract 1
238000006243 chemical reaction Methods 0.000 abstract 1
238000006068 polycondensation reaction Methods 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
- C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
- C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
- C02F2103/38—Polymers

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Environmental & Geological Engineering (AREA)
Life Sciences & Earth Sciences (AREA)
Hydrology & Water Resources (AREA)
Engineering & Computer Science (AREA)
Water Supply & Treatment (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Health & Medical Sciences (AREA)
Separation Using Semi-Permeable Membranes (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)

BRPI0910801-7A 2008-08-18 2009-06-05 Processo e dispositivo para a recuperação de etilenoglicol na preparação de poli (tereftalato de etileno ) BRPI0910801B1 (pt)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
DE102008044440A DE102008044440B4 (de)	2008-08-18	2008-08-18	Verfahren und Vorrichtung zur Rückgewinnung von Ethylenglykol bei der Polyethylenterephthalatherstellung
DE102008044440.5		2008-08-18
PCT/EP2009/056948 WO2010020442A1 (de)	2008-08-18	2009-06-05	Verfahren und vorrichtung zur rückgewinnung von ethylenglykol bei der polyethylenterephthalatherstellung

Publications (2)

Publication Number	Publication Date
BRPI0910801A2 true BRPI0910801A2 (pt)	2015-10-06
BRPI0910801B1 BRPI0910801B1 (pt)	2019-07-02

Family

ID=40957905

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
BRPI0910801-7A BRPI0910801B1 (pt)	2008-08-18	2009-06-05	Processo e dispositivo para a recuperação de etilenoglicol na preparação de poli (tereftalato de etileno )

Country Status (11)

Country	Link
US (2)	US7951980B2 (pt)
EP (1)	EP2157115B1 (pt)
KR (1)	KR20110043550A (pt)
CN (1)	CN102037054B (pt)
AT (1)	ATE526354T1 (pt)
BR (1)	BRPI0910801B1 (pt)
DE (1)	DE102008044440B4 (pt)
EA (1)	EA014966B1 (pt)
ES (1)	ES2374488T3 (pt)
UA (1)	UA97599C2 (pt)
WO (1)	WO2010020442A1 (pt)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE102008044440B4 (de) *	2008-08-18	2011-03-03	Lurgi Zimmer Gmbh	Verfahren und Vorrichtung zur Rückgewinnung von Ethylenglykol bei der Polyethylenterephthalatherstellung
US9018424B2 (en) *	2011-03-30	2015-04-28	Toray Industries, Inc.	Method of producing diol or triol
DE102011082769A1 (de) *	2011-09-15	2013-03-21	Lindauer Dornier Gesellschaft Mit Beschränkter Haftung	Verfahren und Vorrichtung zum Entgasen einer PET - Kunststoffschmelze in einer Extrusionsanlage
US20140005352A1 (en) *	2012-06-29	2014-01-02	Invista North America S.A R.L.	Gas scrubber and related processes
US9145345B2 (en) *	2012-08-30	2015-09-29	Glyeco, Inc.	Method and apparatus for processing glycol
CN103212424B (zh) *	2013-03-08	2015-02-11	上海聚友化工有限公司	一种聚酯废水中回收乙二醇和乙醛的方法
WO2015095879A1 (en)	2013-12-18	2015-06-25	Invista Technologies S.A.R.L.	Method of manufacturing 2-methyl-1, 3-dioxolane in a solid state polycondensation process
US9976490B2 (en) *	2014-07-01	2018-05-22	United Technologies Corporation	Geared gas turbine engine with oil deaerator
CN104497281A (zh) *	2014-11-12	2015-04-08	新疆蓝山屯河聚酯有限公司	高白度聚酯pet瓶片的制备方法
US11555209B2 (en)	2017-12-19	2023-01-17	Lanzatech, Inc.	Microorganisms and methods for the biological production of ethylene glycol
EP4110510A1 (en) *	2020-02-28	2023-01-04	The Procter & Gamble Company	Method to remove chemical contaminants
CN114262257B (zh) *	2020-09-16	2023-07-14	万华化学集团股份有限公司	一种通过柠檬醛工艺废液加氢回收异戊醇的方法
CN112724388B (zh) *	2020-12-28	2023-06-23	扬州普立特科技发展有限公司	一种回收聚酯再生为可降解材料pbat的生产装置
CN113024355B (zh) *	2021-03-18	2022-07-26	湖北山特莱新材料有限公司	一种pta法中乙二醇的回收方法
TW202307202A (zh)	2021-08-06	2023-02-16	美商朗澤科技有限公司	用於改良乙二醇之生物產生的微生物及方法
CN116002881B (zh) *	2021-10-20	2025-12-12	中国石油化工股份有限公司	一种提高cod装置乙醛回收率的装置及其操作方法
KR102766336B1 (ko) *	2021-11-25	2025-02-12	롯데케미칼 주식회사	화학적 재활용 pet의 제조 방법
AU2023286621A1 (en)	2022-06-21	2025-01-09	Lanzatech, Inc.	Microorganisms and methods for the continuous co-production of tandem repeat proteins and chemical products from c1-substrates
CN119403929A (zh)	2022-06-21	2025-02-07	朗泽科技有限公司	用于由c1底物连续共产生高价值专用蛋白和化学产物的微生物和方法
CN118666448A (zh) *	2024-06-19	2024-09-20	上海泓济环保科技股份有限公司	资源化利用含乙酸废水处理系统及其处理方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS53106794A (en) *	1977-03-01	1978-09-18	Mitsubishi Rayon Co Ltd	Treatment of polyester by-product
US4146729A (en) *	1977-04-07	1979-03-27	E. I. Du Pont De Nemours And Company	Process for preparing poly(ethylene terephthalate)
US5236558A (en) *	1982-09-23	1993-08-17	Allied-Signal Inc.	Method to recycle spent ethylene glycol
ATE41668T1 (de) *	1986-04-29	1989-04-15	Fischer Karl Ind Gmbh	Verfahren und vorrichtung zur herstellung hochmolekularer polyester.
US5294305A (en) *	1993-05-06	1994-03-15	Mobile Process Technology, Inc.	Ethylene glycol recovery process
DE19516886A1 (de) *	1995-05-09	1996-11-14	Brown John Deutsche Eng Gmbh	Verfahren und Anlage zum Rückgewinnen von Ethylen-Glykol in einem Polyethylenterephthalat-Polykondensationsprozeß
US5932105A (en) *	1997-10-01	1999-08-03	Mobile Process Technology, Co.	Method of polyester manufacturing using crossflow membrane filtration
DE60112885T2 (de) *	2000-04-27	2006-06-01	Teijin Ltd.	Verfahren zur kontinuierlichen herstellung von polyester
DE10125678B4 (de) *	2001-05-25	2011-04-14	Lurgi Zimmer Gmbh	Verfahren und Vorrichtung zur Herstellung von Polyethylenterephthalat
DE10219671A1 (de) *	2002-05-02	2003-11-20	Zimmer Ag	Verfahren und Vorrichtung zur Herstellung von Polyestern, Copolyestern und Polycarbonaten
CN100462345C (zh) *	2006-12-07	2009-02-18	浙江大学	从聚酯废水中回收乙二醇和乙醛的方法
DE102008044440B4 (de) *	2008-08-18	2011-03-03	Lurgi Zimmer Gmbh	Verfahren und Vorrichtung zur Rückgewinnung von Ethylenglykol bei der Polyethylenterephthalatherstellung

2008
- 2008-08-18 DE DE102008044440A patent/DE102008044440B4/de not_active Expired - Fee Related
2009
- 2009-06-05 UA UAA201101871A patent/UA97599C2/ru unknown
- 2009-06-05 CN CN200980117992.3A patent/CN102037054B/zh active Active
- 2009-06-05 WO PCT/EP2009/056948 patent/WO2010020442A1/de not_active Ceased
- 2009-06-05 EP EP09162048A patent/EP2157115B1/de active Active
- 2009-06-05 ES ES09162048T patent/ES2374488T3/es active Active
- 2009-06-05 KR KR1020107029812A patent/KR20110043550A/ko not_active Abandoned
- 2009-06-05 AT AT09162048T patent/ATE526354T1/de active
- 2009-06-05 BR BRPI0910801-7A patent/BRPI0910801B1/pt active IP Right Grant
- 2009-08-05 US US12/535,732 patent/US7951980B2/en active Active
- 2009-08-17 EA EA200900999A patent/EA014966B1/ru not_active IP Right Cessation
2011
- 2011-01-06 US US12/985,444 patent/US8080222B2/en active Active

Also Published As

Publication number	Publication date
US20110097243A1 (en)	2011-04-28
BRPI0910801B1 (pt)	2019-07-02
US7951980B2 (en)	2011-05-31
EA200900999A1 (ru)	2010-02-26
ES2374488T3 (es)	2012-02-17
EA014966B1 (ru)	2011-04-29
WO2010020442A1 (de)	2010-02-25
ATE526354T1 (de)	2011-10-15
DE102008044440B4 (de)	2011-03-03
KR20110043550A (ko)	2011-04-27
CN102037054A (zh)	2011-04-27
UA97599C2 (ru)	2012-02-27
DE102008044440A1 (de)	2010-02-25
CN102037054B (zh)	2013-03-20
EP2157115B1 (de)	2011-09-28
US20100041925A1 (en)	2010-02-18
US8080222B2 (en)	2011-12-20
EP2157115A1 (de)	2010-02-24

Legal Events

Date	Code	Title	Description
2018-04-17	B06F	Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
2018-10-30	B07A	Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
2019-04-09	B09A	Decision: intention to grant [chapter 9.1 patent gazette]
2019-07-02	B16A	Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]	Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 02/07/2019, OBSERVADAS AS CONDICOES LEGAIS. (CO) 10 (DEZ) ANOS CONTADOS A PARTIR DE 02/07/2019, OBSERVADAS AS CONDICOES LEGAIS

Publication	Publication Date	Title
BRPI0910801A2 (pt)	2015-10-06	processo e dispositivo para a recuperação de etilenoglicol na preparação de poli (tereftalato de etileno )
AR071051A1 (es)	2010-05-26	Metodo y aparato para producir acido acetico con productividad mejorada
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ATE437847T1 (de)	2009-08-15	Verfahren zur abtrennung und rückgewinnung von dimethylterephthalat und ethylenglykol aus polyesterabfällen
CZ294890B6 (cs)	2005-04-13	Způsob přípravy dichlorpropanolů z glycerinu
AR071059A1 (es)	2010-05-26	Eliminacion de acetaldehido del acetato de metilo mediante destilacion a presion elevada y proceso de produccion de acido acetico
BR112015014628B8 (pt)	2021-03-30	processo para produzir ácido acético, e, método para separar ou remover acetaldeído
MX2013003528A (es)	2013-05-30	Purificacion de oxido de propileno.
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EP1816129A4 (en)	2008-01-02	PROCESS FOR PURIFYING PROPYLENE OXIDE
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AR086136A1 (es)	2013-11-20	Reduccion del acido dentro de la columna por medio de la esterificacion durante la produccion de alcoholes
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