CA1054801A - Extraction de gallium dans les liqueurs d'aluminate de sodium - Google Patents

Extraction de gallium dans les liqueurs d'aluminate de sodium

Info

Publication number: CA1054801A
Authority: CA; Canada
Prior art keywords: gallium; liquor; aluminum; sodium; liquors
Prior art date: 1975-09-30
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA236,675A

Other languages

English (en)

Other versions

CA236675S (en

Inventor

Turar B. Tursunbaev

Elizaveta I. Ponomareva

Askar M. Kunaev

Tatyana D. Ostapenko

Galina A. Ivanova

Evgeny N. Bespalov

Igor V. Prokopov

Viktor N. Vasiliev

Salavat I. Turakbaev

Viktor D. Ponomarev

Gennady A. Romanov

Boris A. Smirnov

Boris S. Povazhny

Elena L. Shalavina

Arkady I. Zazubin

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

INSTITUT METALLURGII I OBOGASCHENIA AKADEMII NAUK KAZAKHSKOI SSR

PAVLODARSKY ALJUMINIEVY ZAVOD IMENI 50-LETIA SSSR

Original Assignee

INSTITUT METALLURGII I OBOGASCHENIA AKADEMII NAUK KAZAKHSKOI SSR

PAVLODARSKY ALJUMINIEVY ZAVOD IMENI 50-LETIA SSSR

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-09-30

Filing date

1975-09-30

Publication date

1979-05-22

1975-09-30 Application filed by INSTITUT METALLURGII I OBOGASCHENIA AKADEMII NAUK KAZAKHSKOI SSR, PAVLODARSKY ALJUMINIEVY ZAVOD IMENI 50-LETIA SSSR filed Critical INSTITUT METALLURGII I OBOGASCHENIA AKADEMII NAUK KAZAKHSKOI SSR

1975-09-30 Priority to CA236,675A priority Critical patent/CA1054801A/fr

1979-05-22 Application granted granted Critical

1979-05-22 Publication of CA1054801A publication Critical patent/CA1054801A/fr

Status Expired legal-status Critical Current

Links

229910052733 gallium Inorganic materials 0.000 title claims abstract description 310
GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 title claims abstract description 304
238000000034 method Methods 0.000 title claims abstract description 117
230000008569 process Effects 0.000 title claims abstract description 66
238000000605 extraction Methods 0.000 title claims abstract description 44
239000011734 sodium Substances 0.000 title claims description 11
229910052708 sodium Inorganic materials 0.000 title claims description 10
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 title claims description 8
ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 claims abstract description 115
229910001388 sodium aluminate Inorganic materials 0.000 claims abstract description 115
239000007788 liquid Substances 0.000 claims abstract description 63
229910000838 Al alloy Inorganic materials 0.000 claims abstract description 55
229910052720 vanadium Inorganic materials 0.000 claims abstract description 31
LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims abstract description 29
239000002244 precipitate Substances 0.000 claims abstract description 28
238000004131 Bayer process Methods 0.000 claims abstract description 25
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 17
150000003682 vanadium compounds Chemical class 0.000 claims abstract description 17
150000004645 aluminates Chemical class 0.000 claims abstract description 12
230000000717 retained effect Effects 0.000 claims abstract description 4
229910052782 aluminium Inorganic materials 0.000 claims description 117
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 115
238000003756 stirring Methods 0.000 claims description 16
230000002829 reductive effect Effects 0.000 claims description 9
238000001556 precipitation Methods 0.000 claims description 3
DNEHKUCSURWDGO-UHFFFAOYSA-N aluminum sodium Chemical compound [Na].[Al] DNEHKUCSURWDGO-UHFFFAOYSA-N 0.000 claims 2
239000012535 impurity Substances 0.000 abstract description 23
230000009977 dual effect Effects 0.000 abstract 1
235000010210 aluminium Nutrition 0.000 description 104
GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 42
KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 36
229910001948 sodium oxide Inorganic materials 0.000 description 34
239000010802 sludge Substances 0.000 description 26
229940045605 vanadium Drugs 0.000 description 26
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 24
229910045601 alloy Inorganic materials 0.000 description 21
239000000956 alloy Substances 0.000 description 21
-1 gallium ions Chemical class 0.000 description 19
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 17
229910052753 mercury Inorganic materials 0.000 description 17
239000000243 solution Substances 0.000 description 16
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 15
238000005868 electrolysis reaction Methods 0.000 description 15
229910052731 fluorine Inorganic materials 0.000 description 15
239000011737 fluorine Substances 0.000 description 15
239000000126 substance Substances 0.000 description 15
238000011084 recovery Methods 0.000 description 13
229910052785 arsenic Inorganic materials 0.000 description 12
229940091658 arsenic Drugs 0.000 description 12
238000002425 crystallisation Methods 0.000 description 12
230000008025 crystallization Effects 0.000 description 12
239000012452 mother liquor Substances 0.000 description 12
RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 11
239000000203 mixture Substances 0.000 description 11
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 10
239000000047 product Substances 0.000 description 9
235000011121 sodium hydroxide Nutrition 0.000 description 9
150000001875 compounds Chemical class 0.000 description 8
150000002506 iron compounds Chemical class 0.000 description 8
238000012545 processing Methods 0.000 description 8
PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 8
230000000694 effects Effects 0.000 description 7
238000004519 manufacturing process Methods 0.000 description 6
229940083608 sodium hydroxide Drugs 0.000 description 6
239000007787 solid Substances 0.000 description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 5
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
COHDHYZHOPQOFD-UHFFFAOYSA-N arsenic pentoxide Inorganic materials O=[As](=O)O[As](=O)=O COHDHYZHOPQOFD-UHFFFAOYSA-N 0.000 description 5
238000001816 cooling Methods 0.000 description 5
229910052802 copper Inorganic materials 0.000 description 5
239000010949 copper Substances 0.000 description 5
238000009792 diffusion process Methods 0.000 description 5
229910052739 hydrogen Inorganic materials 0.000 description 5
239000001257 hydrogen Substances 0.000 description 5
229910052759 nickel Inorganic materials 0.000 description 5
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 5
DLYUQMMRRRQYAE-UHFFFAOYSA-N phosphorus pentoxide Inorganic materials O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 5
238000000746 purification Methods 0.000 description 5
238000005245 sintering Methods 0.000 description 5
IHIXIJGXTJIKRB-UHFFFAOYSA-N trisodium vanadate Chemical compound [Na+].[Na+].[Na+].[O-][V]([O-])([O-])=O IHIXIJGXTJIKRB-UHFFFAOYSA-N 0.000 description 5
229910000497 Amalgam Inorganic materials 0.000 description 4
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 4
229910001570 bauxite Inorganic materials 0.000 description 4
150000002500 ions Chemical class 0.000 description 4
229910052698 phosphorus Inorganic materials 0.000 description 4
239000011574 phosphorus Substances 0.000 description 4
235000014786 phosphorus Nutrition 0.000 description 4
238000000926 separation method Methods 0.000 description 4
239000011775 sodium fluoride Substances 0.000 description 4
235000013024 sodium fluoride Nutrition 0.000 description 4
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
238000013019 agitation Methods 0.000 description 3
150000001495 arsenic compounds Chemical class 0.000 description 3
239000002585 base Substances 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
239000003795 chemical substances by application Substances 0.000 description 3
238000000975 co-precipitation Methods 0.000 description 3
239000000470 constituent Substances 0.000 description 3
239000013078 crystal Substances 0.000 description 3
238000000354 decomposition reaction Methods 0.000 description 3
YWEUIGNSBFLMFL-UHFFFAOYSA-N diphosphonate Chemical compound O=P(=O)OP(=O)=O YWEUIGNSBFLMFL-UHFFFAOYSA-N 0.000 description 3
238000001914 filtration Methods 0.000 description 3
CKHJYUSOUQDYEN-UHFFFAOYSA-N gallium(3+) Chemical compound [Ga+3] CKHJYUSOUQDYEN-UHFFFAOYSA-N 0.000 description 3
239000011777 magnesium Substances 0.000 description 3
229910052749 magnesium Inorganic materials 0.000 description 3
235000001055 magnesium Nutrition 0.000 description 3
229940091250 magnesium supplement Drugs 0.000 description 3
230000000737 periodic effect Effects 0.000 description 3
229910052710 silicon Inorganic materials 0.000 description 3
239000010703 silicon Substances 0.000 description 3
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
229910000831 Steel Inorganic materials 0.000 description 2
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical compound [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 2
230000008901 benefit Effects 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
QDOXWKRWXJOMAK-UHFFFAOYSA-N chromium(III) oxide Inorganic materials O=[Cr]O[Cr]=O QDOXWKRWXJOMAK-UHFFFAOYSA-N 0.000 description 2
230000002860 competitive effect Effects 0.000 description 2
239000012141 concentrate Substances 0.000 description 2
238000011109 contamination Methods 0.000 description 2
150000004673 fluoride salts Chemical class 0.000 description 2
150000002222 fluorine compounds Chemical class 0.000 description 2
LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 2
229940093920 gynecological arsenic compound Drugs 0.000 description 2
229910052742 iron Inorganic materials 0.000 description 2
239000000463 material Substances 0.000 description 2
MJGFBOZCAJSGQW-UHFFFAOYSA-N mercury sodium Chemical compound [Na].[Hg] MJGFBOZCAJSGQW-UHFFFAOYSA-N 0.000 description 2
229910052751 metal Inorganic materials 0.000 description 2
239000002184 metal Substances 0.000 description 2
238000002161 passivation Methods 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
150000003018 phosphorus compounds Chemical class 0.000 description 2
230000010287 polarization Effects 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
239000002994 raw material Substances 0.000 description 2
239000011369 resultant mixture Substances 0.000 description 2
229910052814 silicon oxide Inorganic materials 0.000 description 2
229910001023 sodium amalgam Inorganic materials 0.000 description 2
239000010959 steel Substances 0.000 description 2
229910052725 zinc Inorganic materials 0.000 description 2
239000011701 zinc Substances 0.000 description 2
229910000166 zirconium phosphate Inorganic materials 0.000 description 2
WKCZSFRAGKIIKN-UHFFFAOYSA-N 2-(4-tert-butylphenyl)ethanamine Chemical compound CC(C)(C)C1=CC=C(CCN)C=C1 WKCZSFRAGKIIKN-UHFFFAOYSA-N 0.000 description 1
229910018626 Al(OH) Inorganic materials 0.000 description 1
DJHGAFSJWGLOIV-UHFFFAOYSA-L Arsenate2- Chemical compound O[As]([O-])([O-])=O DJHGAFSJWGLOIV-UHFFFAOYSA-L 0.000 description 1
101100087530 Caenorhabditis elegans rom-1 gene Proteins 0.000 description 1
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
241000518994 Conta Species 0.000 description 1
229910000807 Ga alloy Inorganic materials 0.000 description 1
101100305983 Mus musculus Rom1 gene Proteins 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
230000002411 adverse Effects 0.000 description 1
239000003513 alkali Substances 0.000 description 1
WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
238000010420 art technique Methods 0.000 description 1
238000009835 boiling Methods 0.000 description 1
229910052793 cadmium Inorganic materials 0.000 description 1
BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
239000000292 calcium oxide Substances 0.000 description 1
ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
229910052804 chromium Inorganic materials 0.000 description 1
239000011651 chromium Substances 0.000 description 1
230000002844 continuous effect Effects 0.000 description 1
230000018044 dehydration Effects 0.000 description 1
238000006297 dehydration reaction Methods 0.000 description 1
230000003292 diminished effect Effects 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
239000007772 electrode material Substances 0.000 description 1
239000003792 electrolyte Substances 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
239000000284 extract Substances 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
238000012840 feeding operation Methods 0.000 description 1
230000005484 gravity Effects 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
230000002401 inhibitory effect Effects 0.000 description 1
230000002045 lasting effect Effects 0.000 description 1
239000011133 lead Substances 0.000 description 1
230000000670 limiting effect Effects 0.000 description 1
WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
238000005259 measurement Methods 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
230000036961 partial effect Effects 0.000 description 1
239000010452 phosphate Substances 0.000 description 1
230000003334 potential effect Effects 0.000 description 1
230000001376 precipitating effect Effects 0.000 description 1
230000000135 prohibitive effect Effects 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
230000001737 promoting effect Effects 0.000 description 1
238000011160 research Methods 0.000 description 1
230000000979 retarding effect Effects 0.000 description 1
239000004065 semiconductor Substances 0.000 description 1
238000004088 simulation Methods 0.000 description 1
FZHLWVUAICIIPW-UHFFFAOYSA-M sodium gallate Chemical compound [Na+].OC1=CC(C([O-])=O)=CC(O)=C1O FZHLWVUAICIIPW-UHFFFAOYSA-M 0.000 description 1
239000012265 solid product Substances 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
241000894007 species Species 0.000 description 1
238000004611 spectroscopical analysis Methods 0.000 description 1
230000000087 stabilizing effect Effects 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
231100000331 toxic Toxicity 0.000 description 1
230000002588 toxic effect Effects 0.000 description 1
238000011144 upstream manufacturing Methods 0.000 description 1
LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical class [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 description 1

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Manufacture And Refinement Of Metals (AREA)

CA236,675A 1975-09-30 1975-09-30 Extraction de gallium dans les liqueurs d'aluminate de sodium Expired CA1054801A (fr)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CA236,675A CA1054801A (fr)	1975-09-30	1975-09-30	Extraction de gallium dans les liqueurs d'aluminate de sodium

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CA236,675A CA1054801A (fr)	1975-09-30	1975-09-30	Extraction de gallium dans les liqueurs d'aluminate de sodium

Publications (1)

Publication Number	Publication Date
CA1054801A true CA1054801A (fr)	1979-05-22

Family

ID=4104168

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA236,675A Expired CA1054801A (fr)	1975-09-30	1975-09-30	Extraction de gallium dans les liqueurs d'aluminate de sodium

Country Status (1)

Country	Link
CA (1)	CA1054801A (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN116081688A (zh) *	2022-12-30	2023-05-09	靖西天桂铝业有限公司	一种从氧化铝母液制备钒酸钙协同提镓的方法

1975
- 1975-09-30 CA CA236,675A patent/CA1054801A/fr not_active Expired

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN116081688A (zh) *	2022-12-30	2023-05-09	靖西天桂铝业有限公司	一种从氧化铝母液制备钒酸钙协同提镓的方法

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CA1054801A - Extraction de gallium dans les liqueurs d'aluminate de sodium - Google Patents

Info

Links

Landscapes

Priority Applications (1)

Applications Claiming Priority (1)

Publications (1)

Family

ID=4104168

Family Applications (1)

Country Status (1)

Cited By (1)

Cited By (1)

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