CA1080732A - Production de styphnate de plomb - Google Patents

Production de styphnate de plomb

Info

Publication number: CA1080732A
Authority: CA; Canada
Prior art keywords: styphnate; lead; lead styphnate; aqueous solution; crystals
Prior art date: 1975-09-02
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA260,355A

Other languages

English (en)

Inventor

Joachim Grzesiek

Jan Guga

Jozef Piecuch

Maria Sekita

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

ZAKTADY TWORZYW SZTUCZNYCH "NITRON-ERG"

Original Assignee

ZAKTADY TWORZYW SZTUCZNYCH "NITRON-ERG"

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-09-02

Filing date

1976-09-01

Publication date

1980-07-01

1975-09-02 Priority claimed from PL18309175A external-priority patent/PL116447B1/pl

1976-04-12 Priority claimed from PL18874176A external-priority patent/PL110860B1/pl

1976-09-01 Application filed by ZAKTADY TWORZYW SZTUCZNYCH "NITRON-ERG" filed Critical ZAKTADY TWORZYW SZTUCZNYCH "NITRON-ERG"

1980-07-01 Application granted granted Critical

1980-07-01 Publication of CA1080732A publication Critical patent/CA1080732A/fr

Status Expired legal-status Critical Current

Links

WETZJIOEDGMBMA-UHFFFAOYSA-L lead styphnate Chemical compound [Pb+2].[O-]C1=C([N+]([O-])=O)C=C([N+]([O-])=O)C([O-])=C1[N+]([O-])=O WETZJIOEDGMBMA-UHFFFAOYSA-L 0.000 title claims abstract description 50
238000000034 method Methods 0.000 title claims abstract description 21
239000007864 aqueous solution Substances 0.000 claims abstract description 21
239000013078 crystal Substances 0.000 claims abstract description 21
NVYSURDBVCQFBV-UHFFFAOYSA-L magnesium;2,4,6-trinitrobenzene-1,3-diolate Chemical compound [Mg+2].[O-]C1=C([N+]([O-])=O)C=C([N+]([O-])=O)C([O-])=C1[N+]([O-])=O NVYSURDBVCQFBV-UHFFFAOYSA-L 0.000 claims abstract description 15
238000003756 stirring Methods 0.000 claims abstract description 15
RLJMLMKIBZAXJO-UHFFFAOYSA-N lead nitrate Chemical compound [O-][N+](=O)O[Pb]O[N+]([O-])=O RLJMLMKIBZAXJO-UHFFFAOYSA-N 0.000 claims abstract description 12
239000000725 suspension Substances 0.000 claims abstract description 4
239000000243 solution Substances 0.000 claims description 9
230000001376 precipitating effect Effects 0.000 claims description 2
239000000203 mixture Substances 0.000 abstract description 11
230000037452 priming Effects 0.000 abstract description 10
239000002360 explosive Substances 0.000 abstract description 4
230000000977 initiatory effect Effects 0.000 abstract description 2
239000002245 particle Substances 0.000 description 9
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
238000004519 manufacturing process Methods 0.000 description 5
239000000843 powder Substances 0.000 description 5
238000002425 crystallisation Methods 0.000 description 4
238000010908 decantation Methods 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
238000011049 filling Methods 0.000 description 3
239000003380 propellant Substances 0.000 description 3
IWOUKMZUPDVPGQ-UHFFFAOYSA-N barium nitrate Chemical compound [Ba+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O IWOUKMZUPDVPGQ-UHFFFAOYSA-N 0.000 description 2
238000000354 decomposition reaction Methods 0.000 description 2
YADSGOSSYOOKMP-UHFFFAOYSA-N dioxolead Chemical compound O=[Pb]=O YADSGOSSYOOKMP-UHFFFAOYSA-N 0.000 description 2
239000007788 liquid Substances 0.000 description 2
239000002002 slurry Substances 0.000 description 2
241000695274 Processa Species 0.000 description 1
XBDYBAVJXHJMNQ-UHFFFAOYSA-N Tetrahydroanthracene Natural products C1=CC=C2C=C(CCCC3)C3=CC2=C1 XBDYBAVJXHJMNQ-UHFFFAOYSA-N 0.000 description 1
235000010489 acacia gum Nutrition 0.000 description 1
239000001785 acacia senegal l. willd gum Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000005337 ground glass Substances 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
IFLREYGFSNHWGE-UHFFFAOYSA-N tetracene Chemical compound C1=CC=CC2=CC3=CC4=CC=CC=C4C=C3C=C21 IFLREYGFSNHWGE-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B41/00—Compositions containing a nitrated metallo-organic compound
- C06B41/02—Compositions containing a nitrated metallo-organic compound the compound containing lead
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Catalysts (AREA)

CA260,355A 1975-09-02 1976-09-01 Production de styphnate de plomb Expired CA1080732A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
PL18309175A PL116447B1 (en)	1975-09-02	1975-09-02	Method of manufacture of microcrystalline lead trinitroresorcinate
PL18874176A PL110860B1 (en)	1976-04-12	1976-04-12	Method of manufacture of priming composition

Publications (1)

Publication Number	Publication Date
CA1080732A true CA1080732A (fr)	1980-07-01

Family

ID=26652877

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA260,355A Expired CA1080732A (fr)	1975-09-02	1976-09-01	Production de styphnate de plomb

Country Status (3)

Country	Link
AU (1)	AU1718876A (fr)
BE (1)	BE845713A (fr)
CA (1)	CA1080732A (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN102030598A (zh) *	2010-11-04	2011-04-27	云南燃一有限责任公司	一种dplg起爆药及其制备方法
RU2754562C1 (ru) *	2020-10-08	2021-09-03	Акционерное общество "Новосибирский механический завод "Искра"	Способ получения тринитрорезорцината свинца мелкокристаллического
RU2756556C1 (ru) *	2020-10-08	2021-10-01	Акционерное общество "Новосибирский механический завод "Искра"	Тринитрорезорцинат свинца, модифицированный углеродными нанотрубками, и способ его получения

1976
- 1976-08-26 AU AU17188/76A patent/AU1718876A/en not_active Expired
- 1976-08-31 BE BE170243A patent/BE845713A/fr unknown
- 1976-09-01 CA CA260,355A patent/CA1080732A/fr not_active Expired

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN102030598A (zh) *	2010-11-04	2011-04-27	云南燃一有限责任公司	一种dplg起爆药及其制备方法
RU2754562C1 (ru) *	2020-10-08	2021-09-03	Акционерное общество "Новосибирский механический завод "Искра"	Способ получения тринитрорезорцината свинца мелкокристаллического
RU2756556C1 (ru) *	2020-10-08	2021-10-01	Акционерное общество "Новосибирский механический завод "Искра"	Тринитрорезорцинат свинца, модифицированный углеродными нанотрубками, и способ его получения

Also Published As

Publication number	Publication date
AU1718876A (en)	1978-03-02
BE845713A (fr)	1976-12-16

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Legal Events

Date	Code	Title	Description
1997-07-02	MKEX	Expiry