CA1081252A - Preparation d'un agent de blanchiment - Google Patents

Preparation d'un agent de blanchiment

Info

Publication number: CA1081252A
Authority: CA; Canada
Prior art keywords: hydrogen peroxide; peroxide; phthalic anhydride; diphthaloyl; reaction
Prior art date: 1975-11-18
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA265,400A

Other languages

English (en)

Inventor

Robert C.P. Cubbon

Peter J. Russell

Robert E. Talbot

David T. Woodbridge

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Solvay Interox Ltd

Original Assignee

Interox Chemicals Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-11-18

Filing date

1976-11-10

Publication date

1980-07-08

1976-11-10 Application filed by Interox Chemicals Ltd filed Critical Interox Chemicals Ltd

1980-07-08 Application granted granted Critical

1980-07-08 Publication of CA1081252A publication Critical patent/CA1081252A/fr

Status Expired legal-status Critical Current

Links

238000002360 preparation method Methods 0.000 title description 2
239000007844 bleaching agent Substances 0.000 title 1
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 104
LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 claims abstract description 40
JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 claims abstract description 40
238000000034 method Methods 0.000 claims abstract description 37
DEQYKFQEQDSGBB-UHFFFAOYSA-N 2-(2-carboxybenzoyl)peroxycarbonylbenzoic acid Chemical compound OC(=O)C1=CC=CC=C1C(=O)OOC(=O)C1=CC=CC=C1C(O)=O DEQYKFQEQDSGBB-UHFFFAOYSA-N 0.000 claims abstract description 35
238000006243 chemical reaction Methods 0.000 claims abstract description 30
239000002002 slurry Substances 0.000 claims abstract description 25
239000007788 liquid Substances 0.000 claims description 23
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
GLVYLTSKTCWWJR-UHFFFAOYSA-N 2-carbonoperoxoylbenzoic acid Chemical compound OOC(=O)C1=CC=CC=C1C(O)=O GLVYLTSKTCWWJR-UHFFFAOYSA-N 0.000 claims description 12
239000003085 diluting agent Substances 0.000 claims description 12
239000000203 mixture Substances 0.000 claims description 10
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 10
239000002736 nonionic surfactant Substances 0.000 claims description 5
235000010265 sodium sulphite Nutrition 0.000 claims description 5
239000002253 acid Substances 0.000 claims description 4
239000003638 chemical reducing agent Substances 0.000 claims description 4
239000007921 spray Substances 0.000 claims description 4
229910052500 inorganic mineral Inorganic materials 0.000 claims description 3
239000011707 mineral Substances 0.000 claims description 3
DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 2
238000004519 manufacturing process Methods 0.000 claims description 2
239000002904 solvent Substances 0.000 claims 3
RPAJSBKBKSSMLJ-DFWYDOINSA-N (2s)-2-aminopentanedioic acid;hydrochloride Chemical class Cl.OC(=O)[C@@H](N)CCC(O)=O RPAJSBKBKSSMLJ-DFWYDOINSA-N 0.000 claims 1
239000008346 aqueous phase Substances 0.000 abstract description 3
238000005406 washing Methods 0.000 abstract description 3
238000004061 bleaching Methods 0.000 abstract 1
239000004744 fabric Substances 0.000 abstract 1
229960001922 sodium perborate Drugs 0.000 abstract 1
YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 abstract 1
229960002163 hydrogen peroxide Drugs 0.000 description 27
239000000047 product Substances 0.000 description 10
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
239000007787 solid Substances 0.000 description 9
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 6
239000003960 organic solvent Substances 0.000 description 4
239000005639 Lauric acid Substances 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
239000002245 particle Substances 0.000 description 3
238000000926 separation method Methods 0.000 description 3
-1 sodium hydroxide Chemical class 0.000 description 3
239000001117 sulphuric acid Substances 0.000 description 3
235000011149 sulphuric acid Nutrition 0.000 description 3
ZLJZRMPDVNSERU-UHFFFAOYSA-N 3,4,5-trimethyl-2-nonylphenol Chemical compound CCCCCCCCCC1=C(C)C(C)=C(C)C=C1O ZLJZRMPDVNSERU-UHFFFAOYSA-N 0.000 description 2
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
239000000654 additive Substances 0.000 description 2
238000001035 drying Methods 0.000 description 2
238000001914 filtration Methods 0.000 description 2
239000012530 fluid Substances 0.000 description 2
238000011065 in-situ storage Methods 0.000 description 2
239000000463 material Substances 0.000 description 2
235000010755 mineral Nutrition 0.000 description 2
238000002156 mixing Methods 0.000 description 2
XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
239000011541 reaction mixture Substances 0.000 description 2
239000000243 solution Substances 0.000 description 2
239000004215 Carbon black (E152) Substances 0.000 description 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
240000001987 Pyrus communis Species 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
239000003513 alkali Substances 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
239000012670 alkaline solution Substances 0.000 description 1
229910000147 aluminium phosphate Inorganic materials 0.000 description 1
229910000323 aluminium silicate Inorganic materials 0.000 description 1
150000008064 anhydrides Chemical class 0.000 description 1
239000000440 bentonite Substances 0.000 description 1
229910000278 bentonite Inorganic materials 0.000 description 1
SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
238000001816 cooling Methods 0.000 description 1
239000006071 cream Substances 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
239000011928 denatured alcohol Substances 0.000 description 1
235000014113 dietary fatty acids Nutrition 0.000 description 1
WMJRPJZQQSSDBU-UHFFFAOYSA-L disodium;sulfite;heptahydrate Chemical compound O.O.O.O.O.O.O.[Na+].[Na+].[O-]S([O-])=O WMJRPJZQQSSDBU-UHFFFAOYSA-L 0.000 description 1
239000000194 fatty acid Substances 0.000 description 1
229930195729 fatty acid Natural products 0.000 description 1
150000004665 fatty acids Chemical class 0.000 description 1
239000012065 filter cake Substances 0.000 description 1
238000000227 grinding Methods 0.000 description 1
231100001261 hazardous Toxicity 0.000 description 1
239000008240 homogeneous mixture Substances 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
230000002209 hydrophobic effect Effects 0.000 description 1
239000012535 impurity Substances 0.000 description 1
229910052943 magnesium sulfate Inorganic materials 0.000 description 1
235000019341 magnesium sulphate Nutrition 0.000 description 1
229920000847 nonoxynol Polymers 0.000 description 1
150000002978 peroxides Chemical class 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
FVEFRICMTUKAML-UHFFFAOYSA-M sodium tetradecyl sulfate Chemical compound [Na+].CCCCC(CC)CCC(CC(C)C)OS([O-])(=O)=O FVEFRICMTUKAML-UHFFFAOYSA-M 0.000 description 1
239000010457 zeolite Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/32—Peroxy compounds the —O—O— group being bound between two >C=O groups
- C07C409/34—Peroxy compounds the —O—O— group being bound between two >C=O groups both belonging to carboxylic acids
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

CA265,400A 1975-11-18 1976-11-10 Preparation d'un agent de blanchiment Expired CA1081252A (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GB47388/75A GB1541219A (en)	1975-11-18	1975-11-18	Preparation of a dipthaloyl peroxide

Publications (1)

Publication Number	Publication Date
CA1081252A true CA1081252A (fr)	1980-07-08

Family

ID=10444790

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA265,400A Expired CA1081252A (fr)	1975-11-18	1976-11-10	Preparation d'un agent de blanchiment

Country Status (17)

Country	Link
JP (1)	JPS6017785B2 (fr)
AT (1)	AT355555B (fr)
AU (1)	AU517655B2 (fr)
BE (1)	BE848246A (fr)
BR (1)	BR7607682A (fr)
CA (1)	CA1081252A (fr)
CH (1)	CH616153A5 (fr)
DE (1)	DE2652422C2 (fr)
DK (1)	DK514676A (fr)
ES (1)	ES453284A1 (fr)
FR (1)	FR2332267A1 (fr)
GB (1)	GB1541219A (fr)
IT (1)	IT1069566B (fr)
LU (1)	LU76174A1 (fr)
NL (1)	NL7612797A (fr)
SE (1)	SE7612862L (fr)
ZA (1)	ZA766689B (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS62111076U (fr) *	1985-12-27	1987-07-15
CN121271301A (zh) *	2025-11-05	2026-01-06	英德市雅凯高新材料有限公司	环保型过氧化环己酮固化剂组合物在高铁腻子中的应用

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB271725A (en) *	1926-10-26	1927-06-02	Ralph Harper Mckee	Improvements in or relating to methods of making peroxides of organic acids
FR1528458A (fr) *	1966-06-23	1968-06-07	Chefaro Mij Nv	Compositions stabilisées de peroxydes organiques solides

1975
- 1975-11-18 GB GB47388/75A patent/GB1541219A/en not_active Expired
1976
- 1976-11-02 AU AU19242/76A patent/AU517655B2/en not_active Expired
- 1976-11-09 ZA ZA766689A patent/ZA766689B/xx unknown
- 1976-11-10 CA CA265,400A patent/CA1081252A/fr not_active Expired
- 1976-11-11 LU LU76174A patent/LU76174A1/xx unknown
- 1976-11-12 FR FR7634405A patent/FR2332267A1/fr active Granted
- 1976-11-12 BE BE1007765A patent/BE848246A/fr not_active IP Right Cessation
- 1976-11-12 ES ES453284A patent/ES453284A1/es not_active Expired
- 1976-11-15 CH CH1435976A patent/CH616153A5/fr not_active IP Right Cessation
- 1976-11-15 AT AT847776A patent/AT355555B/de not_active IP Right Cessation
- 1976-11-16 DK DK514676A patent/DK514676A/da unknown
- 1976-11-17 BR BR7607682A patent/BR7607682A/pt unknown
- 1976-11-17 DE DE2652422A patent/DE2652422C2/de not_active Expired
- 1976-11-17 IT IT52225/76A patent/IT1069566B/it active
- 1976-11-17 NL NL7612797A patent/NL7612797A/xx not_active Application Discontinuation
- 1976-11-17 SE SE7612862A patent/SE7612862L/xx unknown
- 1976-11-18 JP JP51139025A patent/JPS6017785B2/ja not_active Expired

Also Published As

Publication number	Publication date
LU76174A1 (fr)	1977-05-18
SE7612862L (sv)	1977-05-19
DK514676A (da)	1977-05-19
FR2332267A1 (fr)	1977-06-17
AT355555B (de)	1980-03-10
ZA766689B (en)	1977-10-26
IT1069566B (it)	1985-03-25
JPS6017785B2 (ja)	1985-05-07
ATA847776A (de)	1979-08-15
BR7607682A (pt)	1977-10-04
CH616153A5 (en)	1980-03-14
JPS5262236A (en)	1977-05-23
FR2332267B1 (fr)	1981-09-18
NL7612797A (nl)	1977-05-23
ES453284A1 (es)	1977-11-01
DE2652422A1 (de)	1977-05-26
GB1541219A (en)	1979-02-28
BE848246A (fr)	1977-05-12
AU1924276A (en)	1978-05-11
DE2652422C2 (de)	1985-10-03
AU517655B2 (en)	1981-08-20

Legal Events

Date	Code	Title	Description
1997-07-08	MKEX	Expiry

Publication	Publication Date	Title
EP0682652B1 (fr)	1997-05-28	Procede pour ameliorer les compositions tensio-actives a base de sulfonate d'alkylester
EP0612726B1 (fr)	1997-03-19	Peroxyacide et procédé pour la préparation de peroxyacides
US5426217A (en)	1995-06-20	Process for the production of therephthalic acid
CA1184929A (fr)	1985-04-02	Procede d'obtention de composes peroxydes
EP0046048B1 (fr)	1985-03-06	Procédé pour la production d'hypochlorite de calcium
JPH0337533B2 (fr)	1991-06-05
CA1301186C (fr)	1992-05-19	Preparation d'esters
JPH0420426B2 (fr)	1992-04-02
US4097536A (en)	1978-06-27	Preparation of a bleach
JPH0482142B2 (fr)	1992-12-25
JPS6318581B2 (fr)	1988-04-19
JPS6017785B2 (ja)	1985-05-07	ジフタロイルパーオキシドの製法
US4083877A (en)	1978-04-11	Preparation of a peroxide
US4148867A (en)	1979-04-10	Production of synthetic fluorspar
US5030381A (en)	1991-07-09	Process for the preparation of stabilized aliphatic diperoxydicarboxylic acids
US4450111A (en)	1984-05-22	Process for the purification of anthraquinone
US4069391A (en)	1978-01-17	Process for the production of poly(allyl silicofurmate)
US4139558A (en)	1979-02-13	Process for preparing free-flowing 2-nitro-4-acetylamino-anisole
JPH02129163A (ja)	1990-05-17	不飽和カルボン酸−２−イソシアナトアルキルエステルの製造方法
US3321512A (en)	1967-05-23	Manufacture of perbenzoic acids
EP0210791B1 (fr)	1991-11-13	Résotropine
US3522254A (en)	1970-07-28	Process of preparing halogenated compounds
EP0778826B1 (fr)	1999-11-03	Procede de production de peracides solides
US2503452A (en)	1950-04-11	Manufacture of ddt
JPH0127072B2 (fr)	1989-05-26