CA1088957A - Procede de purification du methanol extrait des condensats resultant de la fabrication de pate kraft - Google Patents

Procede de purification du methanol extrait des condensats resultant de la fabrication de pate kraft

Info

Publication number: CA1088957A
Authority: CA; Canada
Prior art keywords: methanol; solution; condensates; separate; purification
Prior art date: 1976-04-22
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA276,674A

Other languages

English (en)

Inventor

Elias Suokas

Allan Johansson

Veli-Antti Kivilinna

Heikki J. Nyman

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Kemi Oy

Original Assignee

Kemi Oy

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-04-22

Filing date

1977-04-21

Publication date

1980-11-04

1977-04-21 Application filed by Kemi Oy filed Critical Kemi Oy

1980-11-04 Application granted granted Critical

1980-11-04 Publication of CA1088957A publication Critical patent/CA1088957A/fr

Status Expired legal-status Critical Current

Links

OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 title claims abstract description 174
238000000034 method Methods 0.000 title claims abstract description 33
239000002655 kraft paper Substances 0.000 title claims abstract description 14
238000000746 purification Methods 0.000 title claims abstract description 13
238000004537 pulping Methods 0.000 title claims abstract description 7
239000000243 solution Substances 0.000 claims abstract description 24
239000002253 acid Substances 0.000 claims abstract description 5
239000003795 chemical substances by application Substances 0.000 claims abstract description 5
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 8
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 5
238000004821 distillation Methods 0.000 claims description 5
235000011149 sulphuric acid Nutrition 0.000 claims description 5
RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims description 4
239000001117 sulphuric acid Substances 0.000 claims description 4
239000012535 impurity Substances 0.000 claims description 3
239000002032 methanolic fraction Substances 0.000 claims description 3
239000005708 Sodium hypochlorite Substances 0.000 claims description 2
239000007864 aqueous solution Substances 0.000 claims description 2
239000007789 gas Substances 0.000 claims description 2
SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 2
235000010269 sulphur dioxide Nutrition 0.000 claims description 2
239000004291 sulphur dioxide Substances 0.000 claims description 2
239000003784 tall oil Substances 0.000 claims description 2
BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims 1
229910052921 ammonium sulfate Inorganic materials 0.000 claims 1
235000011130 ammonium sulphate Nutrition 0.000 claims 1
239000012670 alkaline solution Substances 0.000 abstract 1
GBMDVOWEEQVZKZ-UHFFFAOYSA-N methanol;hydrate Chemical compound O.OC GBMDVOWEEQVZKZ-UHFFFAOYSA-N 0.000 abstract 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
239000000126 substance Substances 0.000 description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
239000002244 precipitate Substances 0.000 description 6
239000012141 concentrate Substances 0.000 description 5
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
239000000203 mixture Substances 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
235000011121 sodium hydroxide Nutrition 0.000 description 4
241000779819 Syncarpia glomulifera Species 0.000 description 3
238000001914 filtration Methods 0.000 description 3
239000001739 pinus spp. Substances 0.000 description 3
229940083608 sodium hydroxide Drugs 0.000 description 3
229940036248 turpentine Drugs 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
230000007613 environmental effect Effects 0.000 description 2
239000002994 raw material Substances 0.000 description 2
238000000926 separation method Methods 0.000 description 2
229910052938 sodium sulfate Inorganic materials 0.000 description 2
235000011152 sodium sulphate Nutrition 0.000 description 2
241000196324 Embryophyta Species 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
239000005864 Sulphur Substances 0.000 description 1
PFRUBEOIWWEFOL-UHFFFAOYSA-N [N].[S] Chemical class [N].[S] PFRUBEOIWWEFOL-UHFFFAOYSA-N 0.000 description 1
239000003513 alkali Substances 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
229910001863 barium hydroxide Inorganic materials 0.000 description 1
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
239000000920 calcium hydroxide Substances 0.000 description 1
229910001861 calcium hydroxide Inorganic materials 0.000 description 1
235000011116 calcium hydroxide Nutrition 0.000 description 1
229940095643 calcium hydroxide Drugs 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000001816 cooling Methods 0.000 description 1
BERDEBHAJNAUOM-UHFFFAOYSA-N copper(I) oxide Inorganic materials [Cu]O[Cu] BERDEBHAJNAUOM-UHFFFAOYSA-N 0.000 description 1
229940112669 cuprous oxide Drugs 0.000 description 1
KRFJLUBVMFXRPN-UHFFFAOYSA-N cuprous oxide Chemical compound [O-2].[Cu+].[Cu+] KRFJLUBVMFXRPN-UHFFFAOYSA-N 0.000 description 1
230000003292 diminished effect Effects 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
239000000446 fuel Substances 0.000 description 1
229940046892 lead acetate Drugs 0.000 description 1
229940057952 methanol Drugs 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
239000000047 product Substances 0.000 description 1
239000007787 solid Substances 0.000 description 1
UUCCCPNEFXQJEL-UHFFFAOYSA-L strontium dihydroxide Chemical compound [OH-].[OH-].[Sr+2] UUCCCPNEFXQJEL-UHFFFAOYSA-L 0.000 description 1
229910001866 strontium hydroxide Inorganic materials 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
229910021653 sulphate ion Inorganic materials 0.000 description 1
239000013589 supplement Substances 0.000 description 1
150000003505 terpenes Chemical class 0.000 description 1
235000007586 terpenes Nutrition 0.000 description 1
231100000331 toxic Toxicity 0.000 description 1
230000002588 toxic effect Effects 0.000 description 1
231100000419 toxicity Toxicity 0.000 description 1
230000001988 toxicity Effects 0.000 description 1
239000012855 volatile organic compound Substances 0.000 description 1
239000002699 waste material Substances 0.000 description 1
239000002351 wastewater Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/02—Monohydroxylic acyclic alcohols
- C07C31/04—Methanol
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Paper (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)

CA276,674A 1976-04-22 1977-04-21 Procede de purification du methanol extrait des condensats resultant de la fabrication de pate kraft Expired CA1088957A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
FI761096		1976-04-22
FI761096A FI52710C (fi)	1976-04-22	1976-04-22	Menetelmä sulfaattiprosessin lauhteista erotetun metanolin puhdistamis eksi.

Publications (1)

Publication Number	Publication Date
CA1088957A true CA1088957A (fr)	1980-11-04

Family

ID=8509936

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA276,674A Expired CA1088957A (fr)	1976-04-22	1977-04-21	Procede de purification du methanol extrait des condensats resultant de la fabrication de pate kraft

Country Status (6)

Country	Link
JP (1)	JPS52156804A (fr)
BR (1)	BR7702535A (fr)
CA (1)	CA1088957A (fr)
FI (1)	FI52710C (fr)
NO (1)	NO146135C (fr)
SE (1)	SE430411B (fr)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4961918A (en) *	1988-10-11	1990-10-09	Eka Nobel Ab	Process for production of chlorine dioxide
WO2009059920A3 (fr) *	2007-11-09	2009-11-05	Upm-Kymmene Oyj	Utilisation de méthanol dans la production d'hydrogène et de combustible, procédés et installations pour la production d'hydrogène et de combustible
WO2010091492A1 (fr) *	2009-02-12	2010-08-19	A.H Lundberg Systems Limited	Procédé et appareil de purification de méthanol
US10160706B2 (en)	2013-10-11	2018-12-25	Andritz Oy	Process for removal of sulphur from raw methanol
WO2019240654A1 (fr) *	2018-06-11	2019-12-19	Valmet Ab	Procédé et système d'obtention de méthanol à partir d'un condensat vicié d'un processus de trituration
US20230265031A1 (en) *	2020-06-30	2023-08-24	Andritz Oy	A method of purifying raw methanol
US12358813B2 (en)	2019-03-18	2025-07-15	Noram Engineering And Constructors Ltd.	Kraft pulping foul condensate treatment process and apparatus
WO2026062324A1 (fr) *	2024-09-17	2026-03-26	Andritz Oy	Procédé de traitement du méthanol brut

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH0657603B2 (ja) *	1990-04-05	1994-08-03	エカノーベルアクチェボラーグ	二酸化塩素の製造方法
FI126459B (fi) *	2011-02-03	2016-12-15	Stora Enso Oyj	Menetelmä dimetyylisulfonin valmistamiseksi
FI127304B (fi)	2011-02-03	2018-03-15	Stora Enso Oyj	Menetelmä puhdistetun metanolin valmistamiseksi sulfaattisellukeiton lauhteesta
EP3010877B1 (fr) *	2013-06-19	2019-12-18	FPInnovations	Procédé pour la production de biométhanol dans une usine de pâte à papier
SE542659C2 (en) *	2018-07-10	2020-06-23	Stora Enso Oyj	Method for desulfurization of methanol

1976
- 1976-04-22 FI FI761096A patent/FI52710C/fi not_active IP Right Cessation
1977
- 1977-04-21 CA CA276,674A patent/CA1088957A/fr not_active Expired
- 1977-04-21 JP JP4520977A patent/JPS52156804A/ja active Pending
- 1977-04-21 NO NO771384A patent/NO146135C/no unknown
- 1977-04-21 SE SE7704558A patent/SE430411B/xx unknown
- 1977-04-22 BR BR7702535A patent/BR7702535A/pt unknown

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4961918A (en) *	1988-10-11	1990-10-09	Eka Nobel Ab	Process for production of chlorine dioxide
WO2009059920A3 (fr) *	2007-11-09	2009-11-05	Upm-Kymmene Oyj	Utilisation de méthanol dans la production d'hydrogène et de combustible, procédés et installations pour la production d'hydrogène et de combustible
US10407304B2 (en)	2007-11-09	2019-09-10	Upm-Kymmene Oyj	Use of methanol in the production of hydrogen and fuel, processes and plants for the production of hydrogen and fuel
EA020038B1 (ru) *	2009-02-12	2014-08-29	А.Х. Лундберг Системз Лимитед	Способ и устройство для очистки метанола
AU2009339923B2 (en) *	2009-02-12	2014-04-24	A.H Lundberg Systems Limited	Methanol purification method and apparatus
US9320986B2 (en)	2009-02-12	2016-04-26	A.H. Lundberg Systems Limited	Methanol purification method and apparatus
US9938216B2 (en)	2009-02-12	2018-04-10	A.H. Lundberg Systems Limited	Methanol purification method and apparatus
WO2010091492A1 (fr) *	2009-02-12	2010-08-19	A.H Lundberg Systems Limited	Procédé et appareil de purification de méthanol
US10160706B2 (en)	2013-10-11	2018-12-25	Andritz Oy	Process for removal of sulphur from raw methanol
CN112262241A (zh) *	2018-06-11	2021-01-22	维美德公司	从制浆工艺的污冷凝物中获取甲醇的方法和系统
WO2019240654A1 (fr) *	2018-06-11	2019-12-19	Valmet Ab	Procédé et système d'obtention de méthanol à partir d'un condensat vicié d'un processus de trituration
CN112262241B (zh) *	2018-06-11	2022-09-30	维美德公司	从制浆工艺的污冷凝物中获取甲醇的方法和系统
US11898309B2 (en)	2018-06-11	2024-02-13	Valmet Ab	Method and a system for obtaining methanol from foul condensate of a pulping process
US12358813B2 (en)	2019-03-18	2025-07-15	Noram Engineering And Constructors Ltd.	Kraft pulping foul condensate treatment process and apparatus
US20230265031A1 (en) *	2020-06-30	2023-08-24	Andritz Oy	A method of purifying raw methanol
US12503417B2 (en) *	2020-06-30	2025-12-23	Andritz Oy	Method of purifying raw methanol
WO2026062324A1 (fr) *	2024-09-17	2026-03-26	Andritz Oy	Procédé de traitement du méthanol brut

Also Published As

Publication number	Publication date
JPS52156804A (en)	1977-12-27
SE430411B (sv)	1983-11-14
FI52710B (fr)	1977-08-01
FI52710C (fi)	1977-11-10
BR7702535A (pt)	1978-03-21
NO771384L (no)	1977-10-25
NO146135C (no)	1982-08-04
SE7704558L (sv)	1977-10-23
NO146135B (no)	1982-04-26

Legal Events

Date	Code	Title	Description
1997-11-04	MKEX	Expiry
2023-05-26	MKEX	Expiry	Effective date: 19971104

Publication	Publication Date	Title
CA1088957A (fr)	1980-11-04	Procede de purification du methanol extrait des condensats resultant de la fabrication de pate kraft
SE8304858L (sv)	1985-03-13	Forfarande for rening av fororenade vattenlosningar innehallande arsenik och/eller fosfor
RU2377185C2 (ru)	2009-12-27	Экстракция фенолсодержащих потоков сточных вод
JPS61225149A (ja)	1986-10-06	バニリンの製造方法
SE463670B (sv)	1991-01-07	Foerfarande foer framstaellning av klordioxid
DE69716680D1 (de)	2002-12-05	Verfahren zur Produktion von gereinigten Epoxyverbindung
DE69304082D1 (de)	1996-09-19	Verfahren zur herstellung von grünlauge bei der rückgewinnung von chemikalien in einer sulfat- und sulfitzellstoff-anlage
US2890225A (en)	1959-06-09	Process for the conversion of dihydroquercetin to quercetin
US3489740A (en)	1970-01-13	Removing sulfur containing or bearing compounds from organic compounds and resulting products
US2318919A (en)	1943-05-11	Treatment of waste liquor
AU2004215591B2 (en)	2007-11-08	Process
US2430029A (en)	1947-11-04	Splitting tall oil soaps
US4461676A (en)	1984-07-24	Process for refining tetrahydrofuran
KR900016076A (ko)	1990-11-12	산화알킬렌 부가물의 정제방법
CA1121384A (fr)	1982-04-06	Methode de preparation de la vanilline
US2006589A (en)	1935-07-02	Method of purifying phenols
US2595516A (en)	1952-05-06	Process for recovery of tar acids and bases from hydrocarbon oils
JP5528671B2 (ja)	2014-06-25	硫黄酸化物の製造のための方法
US2806068A (en)	1957-09-10	Process for the purification of
US2433227A (en)	1947-12-23	Treatment of lignin substances
US2696508A (en)	1954-12-07	Isopropanol quality improvement process
KR830004206A (ko)	1983-07-06	이소류우신의 정제방법
US5880279A (en)	1999-03-09	Cobalt dihalodihydroxydisulfophthalocyanines
KR950006148B1 (ko)	1995-06-09	유제함유된 폴리아미드로부터 락탐을 회수하는 방법
US2600621A (en)	1952-06-17	Obtaining purified phenols and cresols of petroleum origin