CA1097616A - Extraction des substances nutritives de l'avoine - Google Patents

Extraction des substances nutritives de l'avoine

Info

Publication number: CA1097616A
Authority: CA; Canada
Prior art keywords: protein; acid; separation; insoluble material; groats
Prior art date: 1975-02-06
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA343,909A

Other languages

English (en)

Inventor

Albert Bell

John R. B. Boocock

Richard W. Oughton

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

DuPont Canada Inc

Original Assignee

DuPont Canada Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-02-06

Filing date

1980-01-17

Publication date

1981-03-17

1975-02-06 Priority claimed from GB5055/75A external-priority patent/GB1526552A/en

1980-01-17 Application filed by DuPont Canada Inc filed Critical DuPont Canada Inc

1980-01-17 Priority to CA343,909A priority Critical patent/CA1097616A/fr

1981-03-17 Application granted granted Critical

1981-03-17 Publication of CA1097616A publication Critical patent/CA1097616A/fr

Status Expired legal-status Critical Current

Links

235000007319 Avena orientalis Nutrition 0.000 title claims abstract description 77
238000000605 extraction Methods 0.000 title abstract description 13
235000013305 food Nutrition 0.000 title abstract description 10
241000209761 Avena Species 0.000 title 1
108090000623 proteins and genes Proteins 0.000 claims abstract description 130
102000004169 proteins and genes Human genes 0.000 claims abstract description 130
244000075850 Avena orientalis Species 0.000 claims abstract description 76
238000000034 method Methods 0.000 claims abstract description 61
239000000243 solution Substances 0.000 claims abstract description 51
238000000926 separation method Methods 0.000 claims abstract description 37
239000002198 insoluble material Substances 0.000 claims abstract description 23
239000012670 alkaline solution Substances 0.000 claims abstract description 20
239000000047 product Substances 0.000 claims description 33
239000007788 liquid Substances 0.000 claims description 28
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 24
HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 22
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 20
229920002472 Starch Polymers 0.000 claims description 19
235000019698 starch Nutrition 0.000 claims description 19
239000008107 starch Substances 0.000 claims description 19
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 10
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 10
239000003960 organic solvent Substances 0.000 claims description 8
239000002244 precipitate Substances 0.000 claims description 6
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
239000003513 alkali Substances 0.000 claims description 5
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 4
-1 aliphatic alcohols Chemical class 0.000 claims description 4
239000000908 ammonium hydroxide Substances 0.000 claims description 4
XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 3
238000006243 chemical reaction Methods 0.000 claims description 3
150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims 2
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
239000011575 calcium Substances 0.000 claims 1
229910052791 calcium Inorganic materials 0.000 claims 1
239000003995 emulsifying agent Substances 0.000 abstract description 3
239000007864 aqueous solution Substances 0.000 abstract description 2
235000013312 flour Nutrition 0.000 abstract 1
239000002253 acid Substances 0.000 description 29
239000002002 slurry Substances 0.000 description 19
239000006228 supernatant Substances 0.000 description 18
239000003921 oil Substances 0.000 description 16
235000019198 oils Nutrition 0.000 description 15
238000011282 treatment Methods 0.000 description 14
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
239000011343 solid material Substances 0.000 description 13
239000002904 solvent Substances 0.000 description 13
239000007787 solid Substances 0.000 description 11
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 9
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
230000002378 acidificating effect Effects 0.000 description 9
235000013361 beverage Nutrition 0.000 description 9
239000002245 particle Substances 0.000 description 9
239000012141 concentrate Substances 0.000 description 7
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
238000004458 analytical method Methods 0.000 description 5
230000000694 effects Effects 0.000 description 5
239000002195 soluble material Substances 0.000 description 5
VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 4
244000068988 Glycine max Species 0.000 description 4
235000010469 Glycine max Nutrition 0.000 description 4
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
241001465754 Metazoa Species 0.000 description 4
235000013351 cheese Nutrition 0.000 description 4
238000004108 freeze drying Methods 0.000 description 4
239000000463 material Substances 0.000 description 4
235000019624 protein content Nutrition 0.000 description 4
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
241000237074 Centris Species 0.000 description 3
239000005862 Whey Substances 0.000 description 3
102000007544 Whey Proteins Human genes 0.000 description 3
108010046377 Whey Proteins Proteins 0.000 description 3
239000003929 acidic solution Substances 0.000 description 3
150000007513 acids Chemical class 0.000 description 3
235000011114 ammonium hydroxide Nutrition 0.000 description 3
229940043379 ammonium hydroxide Drugs 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
238000004519 manufacturing process Methods 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
229940070376 protein Drugs 0.000 description 3
239000011734 sodium Substances 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 2
244000066764 Ailanthus triphysa Species 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 2
241000209140 Triticum Species 0.000 description 2
235000021307 Triticum Nutrition 0.000 description 2
229910052783 alkali metal Inorganic materials 0.000 description 2
150000001340 alkali metals Chemical class 0.000 description 2
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
239000000920 calcium hydroxide Substances 0.000 description 2
229910001861 calcium hydroxide Inorganic materials 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
235000012343 cottonseed oil Nutrition 0.000 description 2
239000000839 emulsion Substances 0.000 description 2
239000001530 fumaric acid Substances 0.000 description 2
HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
239000011521 glass Substances 0.000 description 2
230000007062 hydrolysis Effects 0.000 description 2
238000006460 hydrolysis reaction Methods 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
235000016709 nutrition Nutrition 0.000 description 2
239000011591 potassium Substances 0.000 description 2
229910052700 potassium Inorganic materials 0.000 description 2
235000011118 potassium hydroxide Nutrition 0.000 description 2
229940093932 potassium hydroxide Drugs 0.000 description 2
238000001556 precipitation Methods 0.000 description 2
238000003756 stirring Methods 0.000 description 2
235000000346 sugar Nutrition 0.000 description 2
150000008163 sugars Chemical class 0.000 description 2
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 2
235000015112 vegetable and seed oil Nutrition 0.000 description 2
239000008158 vegetable oil Substances 0.000 description 2
108010042653 IgA receptor Proteins 0.000 description 1
101710173438 Late L2 mu core protein Proteins 0.000 description 1
DQLICUFHXKXHCU-UHFFFAOYSA-K N.[OH-].[OH-].[OH-].[K+].[Ca+2] Chemical compound N.[OH-].[OH-].[OH-].[K+].[Ca+2] DQLICUFHXKXHCU-UHFFFAOYSA-K 0.000 description 1
241001163743 Perlodes Species 0.000 description 1
102100034014 Prolyl 3-hydroxylase 3 Human genes 0.000 description 1
101710188315 Protein X Proteins 0.000 description 1
238000000944 Soxhlet extraction Methods 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
239000005864 Sulphur Substances 0.000 description 1
240000008042 Zea mays Species 0.000 description 1
235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
235000002017 Zea mays subsp mays Nutrition 0.000 description 1
239000000654 additive Substances 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
235000021152 breakfast Nutrition 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
239000000470 constituent Substances 0.000 description 1
238000011109 contamination Methods 0.000 description 1
235000005822 corn Nutrition 0.000 description 1
239000002537 cosmetic Substances 0.000 description 1
238000010908 decantation Methods 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
235000013325 dietary fiber Nutrition 0.000 description 1
MCWXGJITAZMZEV-UHFFFAOYSA-N dimethoate Chemical compound CNC(=O)CSP(=S)(OC)OC MCWXGJITAZMZEV-UHFFFAOYSA-N 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
ZYBWTEQKHIADDQ-UHFFFAOYSA-N ethanol;methanol Chemical compound OC.CCO ZYBWTEQKHIADDQ-UHFFFAOYSA-N 0.000 description 1
239000002657 fibrous material Substances 0.000 description 1
239000000796 flavoring agent Substances 0.000 description 1
235000019634 flavors Nutrition 0.000 description 1
235000013373 food additive Nutrition 0.000 description 1
239000002778 food additive Substances 0.000 description 1
150000004679 hydroxides Chemical class 0.000 description 1
JCYWCSGERIELPG-UHFFFAOYSA-N imes Chemical class CC1=CC(C)=CC(C)=C1N1C=CN(C=2C(=CC(C)=CC=2C)C)[C]1 JCYWCSGERIELPG-UHFFFAOYSA-N 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
229910000000 metal hydroxide Inorganic materials 0.000 description 1
150000004692 metal hydroxides Chemical class 0.000 description 1
239000000203 mixture Substances 0.000 description 1
235000015205 orange juice Nutrition 0.000 description 1
210000000056 organ Anatomy 0.000 description 1
239000013618 particulate matter Substances 0.000 description 1
230000003334 potential effect Effects 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
230000006920 protein precipitation Effects 0.000 description 1
238000011084 recovery Methods 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
WTGQALLALWYDJH-WYHSTMEOSA-N scopolamine hydrobromide Chemical compound Br.C1([C@@H](CO)C(=O)OC2C[C@@H]3N([C@H](C2)[C@@H]2[C@H]3O2)C)=CC=CC=C1 WTGQALLALWYDJH-WYHSTMEOSA-N 0.000 description 1
230000035807 sensation Effects 0.000 description 1
235000019615 sensations Nutrition 0.000 description 1
238000007873 sieving Methods 0.000 description 1
235000020183 skimmed milk Nutrition 0.000 description 1
235000014214 soft drink Nutrition 0.000 description 1
238000001694 spray drying Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000001117 sulphuric acid Substances 0.000 description 1
235000011149 sulphuric acid Nutrition 0.000 description 1
239000000725 suspension Substances 0.000 description 1
UMFCIIBZHQXRCJ-NSCUHMNNSA-N trans-anol Chemical compound C\C=C\C1=CC=C(O)C=C1 UMFCIIBZHQXRCJ-NSCUHMNNSA-N 0.000 description 1
238000001291 vacuum drying Methods 0.000 description 1
239000011345 viscous material Substances 0.000 description 1
235000013618 yogurt Nutrition 0.000 description 1

Landscapes

Peptides Or Proteins (AREA)

CA343,909A 1975-02-06 1980-01-17 Extraction des substances nutritives de l'avoine Expired CA1097616A (fr)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CA343,909A CA1097616A (fr)	1975-02-06	1980-01-17	Extraction des substances nutritives de l'avoine

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date	Title
GB5055/75		1975-02-06
GB5055/75A GB1526552A (en)	1975-02-06	1975-02-06	Protein extraction from oats
CA245,163A CA1082174A (fr)	1975-02-06	1976-02-04	Extraction des principes nutritifs de l'avoine
CA343,909A CA1097616A (fr)	1975-02-06	1980-01-17	Extraction des substances nutritives de l'avoine

Publications (1)

Publication Number	Publication Date
CA1097616A true CA1097616A (fr)	1981-03-17

Family

ID=27164321

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA343,909A Expired CA1097616A (fr)	1975-02-06	1980-01-17	Extraction des substances nutritives de l'avoine

Country Status (1)

Country	Link
CA (1)	CA1097616A (fr)

1980
- 1980-01-17 CA CA343,909A patent/CA1097616A/fr not_active Expired

Legal Events

Date	Code	Title	Description
1998-03-17	MKEX	Expiry

Publication	Publication Date	Title
CA1082174A (fr)	1980-07-22	Extraction des principes nutritifs de l'avoine
US3966971A (en)	1976-06-29	Separation of protein from vegetable sources
US3697285A (en)	1972-10-10	Fish protein solubilization using alkaline bacterial protease
US4418013A (en)	1983-11-29	Rapeseed protein isolate
US5312636A (en)	1994-05-17	Process for fractioning crop into industrial raw material
JPS6261543A (ja)	1987-03-18	低フイチン酸塩大豆タンパク質アイソレ−トを製造する方法
US3809771A (en)	1974-05-07	Process for obtaining full-fat oilseed-protein beverages
US4108847A (en)	1978-08-22	Method for preparing bland protein enriched products from grain gluten
US4211801A (en)	1980-07-08	Process for the treatment of comminuted oats
Habib et al.	2025	Ultrasonication modifies the structural, thermal and functional properties of pumpkin seed protein isolate (PSPI)
US7156981B2 (en)	2007-01-02	ITFM extraction of oil seeds
US3852504A (en)	1974-12-03	Process for complete separation of constituents of rice-bran and the like
US20060073250A1 (en)	2006-04-06	Continuous adsorption process for the preparation of a soy protein-containing composition having improved flavor, odor, appearance, or functionality
US4376133A (en)	1983-03-08	Agglomeration of proteinaceous solids
US4215040A (en)	1980-07-29	Density separation process
US20080182002A1 (en)	2008-07-31	Processes for Removing Bitter Components from Soy Protein Isolates
US4219469A (en)	1980-08-26	Extraction of cottonseed and concentrates to improve the color of protein isolate
US4642236A (en)	1987-02-10	Process for reducing the level of objectionable flavors in vegetable protein by microorganism contact
US4366097A (en)	1982-12-28	Novel protein isolation procedure
EP1307113A1 (fr)	2003-05-07	Traitement d'oleagineux
EP0051943A2 (fr)	1982-05-19	Recupération d'une fraction protéique d'avoine à partir d'une dispersion la contenant, dans un solvant hydrocarboné
US4151310A (en)	1979-04-24	Soybean protein extract
US3885050A (en)	1975-05-20	Treatment of protein - containing microbial cells to remove undesirable flavor and odor substances
EP0379499B1 (fr)	1994-02-02	Procede de fractionnement de grains de cereales en vue de leur transformation en matiere premiere pour l'industrie
US3865802A (en)	1975-02-11	Process for obtaining full-fat oilseed-protein beverages using water and initial acid pH