CA1104112A - Methode de preparation de graphite active, et catalyseur a base de ce graphite - Google Patents

Methode de preparation de graphite active, et catalyseur a base de ce graphite

Info

Publication number: CA1104112A
Authority: CA; Canada
Prior art keywords: graphite; platinum; heating; particles; weight
Prior art date: 1977-03-03
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA297,963A

Other languages

English (en)

Inventor

Carl D. Keith

Anton B. Weber

Kurt W. Cornely

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Engelhard Minerals and Chemicals Corp

Original Assignee

Engelhard Minerals and Chemicals Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1977-03-03

Filing date

1978-03-01

Publication date

1981-06-30

1978-03-01 Application filed by Engelhard Minerals and Chemicals Corp filed Critical Engelhard Minerals and Chemicals Corp

1981-06-30 Application granted granted Critical

1981-06-30 Publication of CA1104112A publication Critical patent/CA1104112A/fr

Status Expired legal-status Critical Current

Links

OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical class [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 180
239000003054 catalyst Substances 0.000 title claims abstract description 51
238000000034 method Methods 0.000 title claims description 58
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims abstract description 257
229910002804 graphite Inorganic materials 0.000 claims abstract description 167
239000010439 graphite Substances 0.000 claims abstract description 167
229910052697 platinum Inorganic materials 0.000 claims abstract description 115
238000010438 heat treatment Methods 0.000 claims abstract description 99
239000002245 particle Substances 0.000 claims abstract description 72
239000000463 material Substances 0.000 claims abstract description 51
229910052751 metal Inorganic materials 0.000 claims abstract description 35
239000002184 metal Substances 0.000 claims abstract description 34
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 24
150000003058 platinum compounds Chemical class 0.000 claims abstract description 24
229910052760 oxygen Inorganic materials 0.000 claims abstract description 23
239000001301 oxygen Substances 0.000 claims abstract description 23
150000001875 compounds Chemical class 0.000 claims abstract description 20
230000000694 effects Effects 0.000 claims abstract description 20
239000003960 organic solvent Substances 0.000 claims abstract description 20
239000007770 graphite material Substances 0.000 claims abstract description 18
230000001427 coherent effect Effects 0.000 claims abstract description 13
230000004580 weight loss Effects 0.000 claims description 45
239000000203 mixture Substances 0.000 claims description 44
239000010953 base metal Substances 0.000 claims description 21
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 20
239000010970 precious metal Substances 0.000 claims description 18
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 14
239000000956 alloy Substances 0.000 claims description 10
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239000000446 fuel Substances 0.000 claims description 10
229910052742 iron Inorganic materials 0.000 claims description 10
230000001590 oxidative effect Effects 0.000 claims description 8
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 7
ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 7
229910052804 chromium Inorganic materials 0.000 claims description 7
239000011651 chromium Substances 0.000 claims description 7
229910017052 cobalt Inorganic materials 0.000 claims description 7
239000010941 cobalt Substances 0.000 claims description 7
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 7
239000001257 hydrogen Substances 0.000 claims description 7
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WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims description 7
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WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 6
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BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims description 5
150000001335 aliphatic alkanes Chemical class 0.000 claims description 5
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WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 claims description 5
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UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 4
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ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 claims 4
239000012530 fluid Substances 0.000 claims 1
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CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
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229910003481 amorphous carbon Inorganic materials 0.000 description 4
229910021383 artificial graphite Inorganic materials 0.000 description 4
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XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 3
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VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
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YNKFCNRZZPFMEX-XHPDKPNGSA-N desmopressin acetate trihydrate Chemical compound O.O.O.CC(O)=O.C([C@H]1C(=O)N[C@H](C(N[C@@H](CC(N)=O)C(=O)N[C@@H](CSSCCC(=O)N[C@@H](CC=2C=CC(O)=CC=2)C(=O)N1)C(=O)N1[C@@H](CCC1)C(=O)N[C@H](CCCNC(N)=N)C(=O)NCC(N)=O)=O)CCC(=O)N)C1=CC=CC=C1 YNKFCNRZZPFMEX-XHPDKPNGSA-N 0.000 description 1
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QXTCFDCJXWLNAP-UHFFFAOYSA-N sulfidonitrogen(.) Chemical compound S=[N] QXTCFDCJXWLNAP-UHFFFAOYSA-N 0.000 description 1
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PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 1
229930006978 terpinene Natural products 0.000 description 1
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RAOIDOHSFRTOEL-UHFFFAOYSA-N tetrahydrothiophene Chemical compound C1CCSC1 RAOIDOHSFRTOEL-UHFFFAOYSA-N 0.000 description 1
125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
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125000000101 thioether group Chemical group 0.000 description 1
150000003573 thiols Chemical class 0.000 description 1
238000012876 topography Methods 0.000 description 1
DNYWZCXLKNTFFI-UHFFFAOYSA-N uranium Chemical compound [U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U] DNYWZCXLKNTFFI-UHFFFAOYSA-N 0.000 description 1
SYOKIDBDQMKNDQ-XWTIBIIYSA-N vildagliptin Chemical compound C1C(O)(C2)CC(C3)CC1CC32NCC(=O)N1CCC[C@H]1C#N SYOKIDBDQMKNDQ-XWTIBIIYSA-N 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
229910052726 zirconium Inorganic materials 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/18—Carbon
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
- B01J37/0203—Impregnation the impregnation liquid containing organic compounds
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23D—BURNERS
- F23D14/00—Burners for combustion of a gas, e.g. of a gas stored under pressure as a liquid
- F23D14/12—Radiant burners
- F23D14/18—Radiant burners using catalysis for flameless combustion
- F23D14/181—Radiant burners using catalysis for flameless combustion with carbon containing radiating surface
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23D—BURNERS
- F23D2900/00—Special features of, or arrangements for burners using fluid fuels or solid fuels suspended in a carrier gas
- F23D2900/14—Special features of gas burners
- F23D2900/14582—Special features of gas burners with outlets consisting of layers of spherical particles

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Materials Engineering (AREA)
General Life Sciences & Earth Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Geology (AREA)
Inorganic Chemistry (AREA)
Combustion & Propulsion (AREA)
Mechanical Engineering (AREA)
General Engineering & Computer Science (AREA)
Catalysts (AREA)
Gas Burners (AREA)
Exhaust Gas Treatment By Means Of Catalyst (AREA)

CA297,963A 1977-03-03 1978-03-01 Methode de preparation de graphite active, et catalyseur a base de ce graphite Expired CA1104112A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US77392377A	1977-03-03	1977-03-03
US773,923		1985-09-09

Publications (1)

Publication Number	Publication Date
CA1104112A true CA1104112A (fr)	1981-06-30

Family

ID=25099726

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA297,963A Expired CA1104112A (fr)	1977-03-03	1978-03-01	Methode de preparation de graphite active, et catalyseur a base de ce graphite

Country Status (7)

Country	Link
JP (1)	JPS5456093A (fr)
AU (1)	AU519502B2 (fr)
CA (1)	CA1104112A (fr)
DE (1)	DE2809027A1 (fr)
FR (1)	FR2383882A1 (fr)
GB (1)	GB1601715A (fr)
IT (1)	IT7848255A0 (fr)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5929525U (ja) *	1982-08-16	1984-02-23	プリンス開発興業株式会社	燃焼器における触媒装置
JPS5929526U (ja) *	1982-08-18	1984-02-23	プリンス開発興業株式会社	燃焼器用触媒装置
TW272146B (en) *	1993-05-21	1996-03-11		The preparation of eggshell catalysts having selective reversal or oxidation reaction
US6417133B1 (en) *	1998-02-25	2002-07-09	Monsanto Technology Llc	Deeply reduced oxidation catalyst and its use for catalyzing liquid phase oxidation reactions
KR20020073147A (ko)	1999-12-21	2002-09-19	몬산토 테크놀로지 엘엘씨	탄소-지지된, 귀금속-함유 촉매의 존재하에 보충적촉진제의 액상 산화 반응에서의 용도
AR038654A1 (es)	2000-05-22	2005-01-26	Monsanto Technology Llc	Sistemas de reaccion para producir compuestos de n-(fosfonometil) glicina
EP1560648A1 (fr)	2002-06-28	2005-08-10	Monsanto Technology LLC	Utilisation du tellure dans des catalyseurs supportes par le carbone et contenant des metaux nobles dans des reactions d'oxydation en phase liquide
AR051926A1 (es)	2004-09-15	2007-02-21	Monsanto Technology Llc	Catalizadores de oxidacion, procedimientos de preparacion de dichos catalizadores y proceso para la elaboracion de n-( fosfonometil)glicina o una sal de la misma
US8252953B2 (en)	2008-05-01	2012-08-28	Monsanto Technology Llc	Metal utilization in supported, metal-containing catalysts
FR2944336A1 (fr) *	2009-04-14	2010-10-15	Air Liquide	Bruleur en regime de premelange et son utilisation

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2538346C2 (de) *	1974-09-02	1986-04-30	The British Petroleum Co., Ltd., London	Verfahren zur Herstellung von graphithaltigem Kohlenstoff und seine Verwendung
GB1471589A (en) *	1974-10-24	1977-04-27	British Petroleum Co	Desulphurisation catalyst and process

1978
- 1978-02-20 GB GB6617/78A patent/GB1601715A/en not_active Expired
- 1978-03-01 FR FR7805856A patent/FR2383882A1/fr active Granted
- 1978-03-01 CA CA297,963A patent/CA1104112A/fr not_active Expired
- 1978-03-01 JP JP2217878A patent/JPS5456093A/ja active Pending
- 1978-03-02 DE DE19782809027 patent/DE2809027A1/de not_active Withdrawn
- 1978-03-02 IT IT7848255A patent/IT7848255A0/it unknown
- 1978-03-02 AU AU33753/78A patent/AU519502B2/en not_active Expired

Also Published As

Publication number	Publication date
AU519502B2 (en)	1981-12-10
DE2809027A1 (de)	1978-09-07
GB1601715A (en)	1981-11-04
AU3375378A (en)	1979-09-06
JPS5456093A (en)	1979-05-04
IT7848255A0 (it)	1978-03-02
FR2383882A1 (fr)	1978-10-13
FR2383882B1 (fr)	1983-02-11

Legal Events

Date	Code	Title	Description
1998-06-30	MKEX	Expiry

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Singh et al.	2021	Non-oxidative coupling of methane over Pd-loaded gallium oxide photocatalysts in a flow reactor
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Yonezawa et al.	1995	Mechanistic consideration of formation of polymer-protected nanoscopic bimetallic clusters
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Sales et al.	1998	Alumina-supported Pd, Ag and Pd–Ag catalysts: preparation through the polyol process, characterization and reactivity in hexa-1, 5-diene hydrogenation
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