CA1166114A - Methode d'obtention d'un tabac a fumer libere de ses proteines, sans nicotine ni pigment vert - Google Patents

Methode d'obtention d'un tabac a fumer libere de ses proteines, sans nicotine ni pigment vert

Info

Publication number: CA1166114A
Authority: CA; Canada
Prior art keywords: liquid portion; process according; pigmented; water; nicotine
Prior art date: 1981-09-14
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000385783A

Other languages

English (en)

Inventor

Samuel G. Wildman

Shuh J. Sheen

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Leaf Proteins Inc

Original Assignee

Leaf Proteins Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-09-14

Filing date

1981-09-14

Publication date

1984-04-24

1981-09-14 Application filed by Leaf Proteins Inc filed Critical Leaf Proteins Inc

1981-09-14 Priority to CA000385783A priority Critical patent/CA1166114A/fr

1984-04-24 Application granted granted Critical

1984-04-24 Publication of CA1166114A publication Critical patent/CA1166114A/fr

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 74
230000008569 process Effects 0.000 title claims abstract description 73
235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 70
241000208125 Nicotiana Species 0.000 title claims abstract description 62
SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 title claims abstract description 33
229960002715 nicotine Drugs 0.000 title claims abstract description 33
SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 title claims abstract description 33
230000000391 smoking effect Effects 0.000 title claims abstract description 11
239000001056 green pigment Substances 0.000 title abstract description 7
239000000463 material Substances 0.000 claims abstract description 101
239000007788 liquid Substances 0.000 claims abstract description 78
108090000623 proteins and genes Proteins 0.000 claims abstract description 48
102000004169 proteins and genes Human genes 0.000 claims abstract description 48
241000196324 Embryophyta Species 0.000 claims abstract description 18
238000000926 separation method Methods 0.000 claims abstract description 11
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 36
239000011343 solid material Substances 0.000 claims description 25
239000000243 solution Substances 0.000 claims description 20
238000010438 heat treatment Methods 0.000 claims description 19
239000002904 solvent Substances 0.000 claims description 17
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 16
235000019505 tobacco product Nutrition 0.000 claims description 16
239000011236 particulate material Substances 0.000 claims description 15
YAHZABJORDUQGO-NQXXGFSBSA-N D-ribulose 1,5-bisphosphate Chemical compound OP(=O)(O)OC[C@@H](O)[C@@H](O)C(=O)COP(O)(O)=O YAHZABJORDUQGO-NQXXGFSBSA-N 0.000 claims description 9
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 9
239000012454 non-polar solvent Substances 0.000 claims description 7
239000000725 suspension Substances 0.000 claims description 6
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
239000000203 mixture Substances 0.000 claims description 5
239000001301 oxygen Substances 0.000 claims description 5
229910052760 oxygen Inorganic materials 0.000 claims description 5
238000000638 solvent extraction Methods 0.000 claims description 5
239000002253 acid Substances 0.000 claims description 4
238000001256 steam distillation Methods 0.000 claims description 4
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 3
125000001931 aliphatic group Chemical group 0.000 claims description 3
239000000908 ammonium hydroxide Substances 0.000 claims description 3
239000007864 aqueous solution Substances 0.000 claims description 3
239000003849 aromatic solvent Substances 0.000 claims description 3
238000001816 cooling Methods 0.000 claims description 3
235000019628 coolness Nutrition 0.000 claims 1
235000019504 cigarettes Nutrition 0.000 abstract description 16
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 12
238000004519 manufacturing process Methods 0.000 abstract description 8
239000007787 solid Substances 0.000 abstract description 8
239000000945 filler Substances 0.000 abstract description 5
235000018102 proteins Nutrition 0.000 description 33
239000000047 product Substances 0.000 description 22
239000011269 tar Substances 0.000 description 11
244000061176 Nicotiana tabacum Species 0.000 description 8
230000003647 oxidation Effects 0.000 description 7
238000007254 oxidation reaction Methods 0.000 description 7
238000002425 crystallisation Methods 0.000 description 6
230000008025 crystallization Effects 0.000 description 6
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
239000003638 chemical reducing agent Substances 0.000 description 5
239000000796 flavoring agent Substances 0.000 description 5
235000019634 flavors Nutrition 0.000 description 5
230000009467 reduction Effects 0.000 description 5
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
239000003795 chemical substances by application Substances 0.000 description 4
235000011389 fruit/vegetable juice Nutrition 0.000 description 4
239000010802 sludge Substances 0.000 description 4
239000000779 smoke Substances 0.000 description 4
DGVVWUTYPXICAM-UHFFFAOYSA-N β‐Mercaptoethanol Chemical compound OCCS DGVVWUTYPXICAM-UHFFFAOYSA-N 0.000 description 4
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 3
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
238000001704 evaporation Methods 0.000 description 3
230000008020 evaporation Effects 0.000 description 3
238000001914 filtration Methods 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
239000000049 pigment Substances 0.000 description 3
238000012545 processing Methods 0.000 description 3
230000000717 retained effect Effects 0.000 description 3
235000000346 sugar Nutrition 0.000 description 3
239000006228 supernatant Substances 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
ZAQJHHRNXZUBTE-NQXXGFSBSA-N D-ribulose Chemical compound OC[C@@H](O)[C@@H](O)C(=O)CO ZAQJHHRNXZUBTE-NQXXGFSBSA-N 0.000 description 2
ZAQJHHRNXZUBTE-UHFFFAOYSA-N D-threo-2-Pentulose Natural products OCC(O)C(O)C(=O)CO ZAQJHHRNXZUBTE-UHFFFAOYSA-N 0.000 description 2
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
229920002472 Starch Polymers 0.000 description 2
238000013019 agitation Methods 0.000 description 2
-1 aromatic amino acids Chemical class 0.000 description 2
230000008901 benefit Effects 0.000 description 2
238000005119 centrifugation Methods 0.000 description 2
238000005345 coagulation Methods 0.000 description 2
230000015271 coagulation Effects 0.000 description 2
239000000470 constituent Substances 0.000 description 2
230000003544 deproteinization Effects 0.000 description 2
239000001177 diphosphate Substances 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000000284 extract Substances 0.000 description 2
238000000605 extraction Methods 0.000 description 2
239000012530 fluid Substances 0.000 description 2
238000003306 harvesting Methods 0.000 description 2
230000036541 health Effects 0.000 description 2
239000003208 petroleum Substances 0.000 description 2
238000004537 pulping Methods 0.000 description 2
238000005507 spraying Methods 0.000 description 2
239000008107 starch Substances 0.000 description 2
235000019698 starch Nutrition 0.000 description 2
XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 description 1
101710138460 Leaf protein Proteins 0.000 description 1
102000035195 Peptidases Human genes 0.000 description 1
108091005804 Peptidases Proteins 0.000 description 1
108010064851 Plant Proteins Proteins 0.000 description 1
229930182558 Sterol Natural products 0.000 description 1
102000003425 Tyrosinase Human genes 0.000 description 1
108060008724 Tyrosinase Proteins 0.000 description 1
230000002411 adverse Effects 0.000 description 1
229910021529 ammonia Inorganic materials 0.000 description 1
239000003963 antioxidant agent Substances 0.000 description 1
230000003078 antioxidant effect Effects 0.000 description 1
238000010923 batch production Methods 0.000 description 1
238000009835 boiling Methods 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
235000021466 carotenoid Nutrition 0.000 description 1
150000001747 carotenoids Chemical class 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
235000019506 cigar Nutrition 0.000 description 1
238000010924 continuous production Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000003111 delayed effect Effects 0.000 description 1
235000014113 dietary fatty acids Nutrition 0.000 description 1
230000029087 digestion Effects 0.000 description 1
230000003292 diminished effect Effects 0.000 description 1
VHJLVAABSRFDPM-QWWZWVQMSA-N dithiothreitol Chemical compound SC[C@@H](O)[C@H](O)CS VHJLVAABSRFDPM-QWWZWVQMSA-N 0.000 description 1
239000012259 ether extract Substances 0.000 description 1
239000000194 fatty acid Substances 0.000 description 1
229930195729 fatty acid Natural products 0.000 description 1
150000004665 fatty acids Chemical class 0.000 description 1
239000002657 fibrous material Substances 0.000 description 1
239000007789 gas Substances 0.000 description 1
238000000227 grinding Methods 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
230000001939 inductive effect Effects 0.000 description 1
206010022000 influenza Diseases 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
238000002955 isolation Methods 0.000 description 1
238000000622 liquid--liquid extraction Methods 0.000 description 1
210000004072 lung Anatomy 0.000 description 1
230000007246 mechanism Effects 0.000 description 1
235000013379 molasses Nutrition 0.000 description 1
229930014626 natural product Natural products 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
150000007524 organic acids Chemical class 0.000 description 1
230000020477 pH reduction Effects 0.000 description 1
235000021118 plant-derived protein Nutrition 0.000 description 1
150000008442 polyphenolic compounds Chemical class 0.000 description 1
235000013824 polyphenols Nutrition 0.000 description 1
239000011148 porous material Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
238000003825 pressing Methods 0.000 description 1
229940070376 protein Drugs 0.000 description 1
229940024999 proteolytic enzymes for treatment of wounds and ulcers Drugs 0.000 description 1
238000010992 reflux Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
239000013557 residual solvent Substances 0.000 description 1
HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 description 1
229940001584 sodium metabisulfite Drugs 0.000 description 1
235000010262 sodium metabisulphite Nutrition 0.000 description 1
239000002195 soluble material Substances 0.000 description 1
239000007858 starting material Substances 0.000 description 1
150000003432 sterols Chemical class 0.000 description 1
235000003702 sterols Nutrition 0.000 description 1
150000008163 sugars Chemical class 0.000 description 1
230000001629 suppression Effects 0.000 description 1
150000003505 terpenes Chemical class 0.000 description 1
OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1

Landscapes

Manufacture Of Tobacco Products (AREA)

CA000385783A 1981-09-14 1981-09-14 Methode d'obtention d'un tabac a fumer libere de ses proteines, sans nicotine ni pigment vert Expired CA1166114A (fr)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CA000385783A CA1166114A (fr)	1981-09-14	1981-09-14	Methode d'obtention d'un tabac a fumer libere de ses proteines, sans nicotine ni pigment vert

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CA000385783A CA1166114A (fr)	1981-09-14	1981-09-14	Methode d'obtention d'un tabac a fumer libere de ses proteines, sans nicotine ni pigment vert

Publications (1)

Publication Number	Publication Date
CA1166114A true CA1166114A (fr)	1984-04-24

Family

ID=4120934

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000385783A Expired CA1166114A (fr)	1981-09-14	1981-09-14	Methode d'obtention d'un tabac a fumer libere de ses proteines, sans nicotine ni pigment vert

Country Status (1)

Country	Link
CA (1)	CA1166114A (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO2014159617A1 (fr) *	2013-03-14	2014-10-02	R. J. Reynolds Tobacco Company	Composition dérivée du tabac enrichie en protéines
US11612183B2 (en)	2015-12-10	2023-03-28	R.J. Reynolds Tobacco Company	Protein-enriched tobacco composition

1981
- 1981-09-14 CA CA000385783A patent/CA1166114A/fr not_active Expired

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO2014159617A1 (fr) *	2013-03-14	2014-10-02	R. J. Reynolds Tobacco Company	Composition dérivée du tabac enrichie en protéines
US9301544B2 (en)	2013-03-14	2016-04-05	R.J. Reynolds Tobacco Company	Protein-enriched tobacco-derived composition
US11166485B2 (en)	2013-03-14	2021-11-09	R.J. Reynolds Tobacco Company	Protein-enriched tobacco-derived composition
US11375741B2 (en)	2013-03-14	2022-07-05	R.J. Reynolds Tobacco Company	Protein-enriched tobacco-derived composition
US11612183B2 (en)	2015-12-10	2023-03-28	R.J. Reynolds Tobacco Company	Protein-enriched tobacco composition
US12178237B2 (en)	2015-12-10	2024-12-31	R.J. Reynolds Tobacco Company	Protein-enriched tobacco composition

Legal Events

Date	Code	Title	Description
2001-04-24	MKEX	Expiry

Publication	Publication Date	Title
US4289147A (en)	1981-09-15	Process for obtaining deproteinized tobacco freed of nicotine and green pigment, for use as a smoking product
JP6994069B2 (ja)	2022-01-14	タンパク質濃縮タバコ由来組成物
US4267847A (en)	1981-05-19	Tobacco additives
US4991599A (en)	1991-02-12	Fiberless tobacco product for smoking and chewing
US5158771A (en)	1992-10-27	Nicotine compositions
US20240365841A1 (en)	2024-11-07	Purification of tobacco-derived protein compositions
GB2113065A (en)	1983-08-03	Process for obtaining deproteinized tobacco freed of nicotine and green pigment, for use as a smoking product
WO1994007382A1 (fr)	1994-04-14	Procede de traitement de tabac vert et produit ainsi obtenu
GB2203022A (en)	1988-10-12	Smoking material
JPH0218058B2 (fr)	1990-04-24
DE3136353C2 (de)	1986-07-17	Verfahren zur Behandlung von Tabakblättern
FR2512646A1 (fr)	1983-03-18	Procede de traitement de feuilles de tabac et produit obtenu
JPS5831914B2 (ja)	1983-07-09	たばこ用香喫味改良剤
CH632907A5 (en)	1982-11-15	Method of treating tobacco
JPS6319497B2 (fr)	1988-04-22
JPS61145142A (ja)	1986-07-02	たばこ用香喫味改良剤
KR840002455B1 (ko)	1984-12-29	토오스트(Toast)에 의한 저(低) 니코틴 판상엽의 가공 방법
JPS5932451B2 (ja)	1984-08-09	オクシド−ル・アイソマ−・１及びたばこ用香喫味改良剤
DeGraffe	1896	OPUNTIA VULGARIS, MILL.
JPS5811191B2 (ja)	1983-03-01	たばこ用香喫味改良剤
JPS5831915B2 (ja)	1983-07-09	たばこ用香喫味改良剤
JPS6328583B2 (fr)	1988-06-09
GB315715A (en)	1931-01-16	Improvements in the treatment of smoking tobaccos
JPS5932452B2 (ja)	1984-08-09	オクシド−ル・アイソマ−・２及びたばこ用香喫味改良剤
JPS5831913B2 (ja)	1983-07-09	たばこ用香喫味改良剤