CA1171608A - Methode de separation des composantes de la liqueur noire - Google Patents

Methode de separation des composantes de la liqueur noire

Info

Publication number: CA1171608A
Authority: CA; Canada
Prior art keywords: iron; pellets; reducing; sodium; liquor
Prior art date: 1982-06-21
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000405594A

Other languages

English (en)

Inventor

Xuan T. Nguyen

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Domtar Inc

Original Assignee

Domtar Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-06-21

Filing date

1982-06-21

Publication date

1984-07-31

1982-06-21 Application filed by Domtar Inc filed Critical Domtar Inc

1982-06-21 Priority to CA000405594A priority Critical patent/CA1171608A/fr

1984-07-31 Application granted granted Critical

1984-07-31 Publication of CA1171608A publication Critical patent/CA1171608A/fr

Status Expired legal-status Critical Current

Links

239000002655 kraft paper Substances 0.000 title claims abstract description 23
238000011084 recovery Methods 0.000 title abstract description 19
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 103
229910052742 iron Inorganic materials 0.000 claims abstract description 51
239000008188 pellet Substances 0.000 claims abstract description 48
230000001603 reducing effect Effects 0.000 claims abstract description 37
238000000034 method Methods 0.000 claims abstract description 25
230000008569 process Effects 0.000 claims abstract description 25
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 21
229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 21
235000011152 sodium sulphate Nutrition 0.000 claims abstract description 21
229910052979 sodium sulfide Inorganic materials 0.000 claims abstract description 12
GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 claims abstract description 11
150000001875 compounds Chemical class 0.000 claims abstract description 9
239000000463 material Substances 0.000 claims abstract description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
230000009467 reduction Effects 0.000 claims description 53
239000007789 gas Substances 0.000 claims description 25
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 24
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 22
229910052739 hydrogen Inorganic materials 0.000 claims description 19
239000001257 hydrogen Substances 0.000 claims description 19
UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 15
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 15
229910002091 carbon monoxide Inorganic materials 0.000 claims description 15
238000004537 pulping Methods 0.000 claims description 14
229910000029 sodium carbonate Inorganic materials 0.000 claims description 12
239000000126 substance Substances 0.000 claims description 12
239000002002 slurry Substances 0.000 claims description 5
150000002431 hydrogen Chemical class 0.000 claims description 4
230000001590 oxidative effect Effects 0.000 claims description 4
150000004763 sulfides Chemical class 0.000 claims description 3
LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 claims description 3
150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 3
238000009993 causticizing Methods 0.000 claims description 2
230000006872 improvement Effects 0.000 claims description 2
239000003265 pulping liquor Substances 0.000 claims description 2
150000003388 sodium compounds Chemical class 0.000 claims description 2
229940105305 carbon monoxide Drugs 0.000 claims 3
229940001593 sodium carbonate Drugs 0.000 claims 2
235000017550 sodium carbonate Nutrition 0.000 claims 2
239000000470 constituent Substances 0.000 claims 1
150000002484 inorganic compounds Chemical class 0.000 abstract description 2
229910010272 inorganic material Inorganic materials 0.000 abstract description 2
238000006722 reduction reaction Methods 0.000 description 51
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 15
238000002485 combustion reaction Methods 0.000 description 15
150000002506 iron compounds Chemical class 0.000 description 15
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
239000000203 mixture Substances 0.000 description 6
239000003345 natural gas Substances 0.000 description 6
239000002245 particle Substances 0.000 description 5
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
239000011734 sodium Substances 0.000 description 4
229910052708 sodium Inorganic materials 0.000 description 4
239000002023 wood Substances 0.000 description 4
241001062472 Stokellia anisodon Species 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
239000012530 fluid Substances 0.000 description 3
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
235000008733 Citrus aurantifolia Nutrition 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 2
235000011941 Tilia x europaea Nutrition 0.000 description 2
238000010411 cooking Methods 0.000 description 2
230000001419 dependent effect Effects 0.000 description 2
229930195733 hydrocarbon Natural products 0.000 description 2
150000002430 hydrocarbons Chemical class 0.000 description 2
229920005610 lignin Polymers 0.000 description 2
239000004571 lime Substances 0.000 description 2
230000008018 melting Effects 0.000 description 2
238000002844 melting Methods 0.000 description 2
230000003647 oxidation Effects 0.000 description 2
238000007254 oxidation reaction Methods 0.000 description 2
239000007790 solid phase Substances 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
239000002028 Biomass Substances 0.000 description 1
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
OOIOHEBTXPTBBE-UHFFFAOYSA-N [Na].[Fe] Chemical class [Na].[Fe] OOIOHEBTXPTBBE-UHFFFAOYSA-N 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
230000002411 adverse Effects 0.000 description 1
-1 calcium Chemical class 0.000 description 1
239000011575 calcium Substances 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
238000010531 catalytic reduction reaction Methods 0.000 description 1
150000001768 cations Chemical class 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000003245 coal Substances 0.000 description 1
229940000425 combination drug Drugs 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
230000005496 eutectics Effects 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
238000004880 explosion Methods 0.000 description 1
238000010304 firing Methods 0.000 description 1
238000009434 installation Methods 0.000 description 1
239000012978 lignocellulosic material Substances 0.000 description 1
238000002156 mixing Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000009972 noncorrosive effect Effects 0.000 description 1
231100000252 nontoxic Toxicity 0.000 description 1
230000003000 nontoxic effect Effects 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 1
239000012071 phase Substances 0.000 description 1
235000000346 sugar Nutrition 0.000 description 1
150000008163 sugars Chemical class 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
229910000859 α-Fe Inorganic materials 0.000 description 1

Classifications

- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0085—Introduction of auxiliary substances into the regenerating system in order to improve the performance of certain steps of the latter, the presence of these substances being confined to the regeneration cycle
- D21C11/0092—Substances modifying the evaporation, combustion, or thermal decomposition processes of black liquor

Landscapes

Paper (AREA)

CA000405594A 1982-06-21 1982-06-21 Methode de separation des composantes de la liqueur noire Expired CA1171608A (fr)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CA000405594A CA1171608A (fr)	1982-06-21	1982-06-21	Methode de separation des composantes de la liqueur noire

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CA000405594A CA1171608A (fr)	1982-06-21	1982-06-21	Methode de separation des composantes de la liqueur noire

Publications (1)

Publication Number	Publication Date
CA1171608A true CA1171608A (fr)	1984-07-31

Family

ID=4123057

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000405594A Expired CA1171608A (fr)	1982-06-21	1982-06-21	Methode de separation des composantes de la liqueur noire

Country Status (1)

Country	Link
CA (1)	CA1171608A (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO1994007797A1 (fr) *	1992-09-30	1994-04-14	North Broken Hill Limited	Procede de recuperation d'hydroxyde de metal alcalin a partir de liqueurs organiques
CN114875241A (zh) *	2022-04-07	2022-08-09	江西理工大学	硫酸体系下从钕铁硼废料酸浸渣中综合回收有价金属的方法
CN115074530A (zh) *	2022-04-07	2022-09-20	江西理工大学	盐酸体系下从钕铁硼废料酸浸渣中综合回收有价金属的方法

1982
- 1982-06-21 CA CA000405594A patent/CA1171608A/fr not_active Expired

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO1994007797A1 (fr) *	1992-09-30	1994-04-14	North Broken Hill Limited	Procede de recuperation d'hydroxyde de metal alcalin a partir de liqueurs organiques
US5545385A (en) *	1992-09-30	1996-08-13	Amcor Limited	Process for recovering alkali metal hydroxide from organic liquors
CN114875241A (zh) *	2022-04-07	2022-08-09	江西理工大学	硫酸体系下从钕铁硼废料酸浸渣中综合回收有价金属的方法
CN115074530A (zh) *	2022-04-07	2022-09-20	江西理工大学	盐酸体系下从钕铁硼废料酸浸渣中综合回收有价金属的方法

Legal Events

Date	Code	Title	Description
2001-08-01	MKEC	Expiry (correction)
2002-06-21	MKEX	Expiry

Publication	Publication Date	Title
US4011129A (en)	1977-03-08	Pulp mill recovery system
CA1142756A (fr)	1983-03-15	Methode de combustion de la houille
US4135968A (en)	1979-01-23	Spent liquor treatment
FI75616C (fi)	1988-07-11	Foerfarande foer aotervinning av en alkali- eller jordalkalimetalloxid eller -hydroxid.
FI73756B (fi)	1987-07-31	Metod och anordning foer regenerering av pappersindustrins avlut.
US4526760A (en)	1985-07-02	Recovery of heat and chemical values from spent pulping liquors
CA2043538A1 (fr)	1991-12-01	Epuration d'un gaz de traitement, faisant appel a la combustion partielle de liqueur noire
CA1289336C (fr)	1991-09-24	Methode pour separer les composes sulfureux et l'oxyde de soufre en phase gazeuse des gaz de cheminee
US4524049A (en)	1985-06-18	Process for concurrent steam generation and metal recovery
US3323858A (en)	1967-06-06	Process for recovering the alkali metal content of spent pulping liquor
US5449505A (en)	1995-09-12	Method for disposing of radioactive graphite and silicon carbide in graphite fuel elements
CA1313577C (fr)	1993-02-16	Recuperation a basse temperature de boue noire kraft
US4377439A (en)	1983-03-22	Pulp mill recovery
US4441959A (en)	1984-04-10	Recovery of heat and chemical values from spent pulping liquors
EP0179803B1 (fr)	1989-08-02	Procede de production d'une liqueur de pulpage epuisee, concentree et partiellement oxydee
US2334621A (en)	1943-11-16	Method of treating sulphite waste liquors
CA2078934A1 (fr)	1993-03-28	Methode de traitement d'une matiere contenant du sulphate de sodiu, du carbonate de sodium ou les deux dans une usine de pate
US5545385A (en)	1996-08-13	Process for recovering alkali metal hydroxide from organic liquors
US3111377A (en)	1963-11-19	Treatment of sulfite spent liquor
GB2201423A (en)	1988-09-01	Process for producing smokeless, cured fuel briquettes
CA1061059A (fr)	1979-08-28	Systeme de recuperation pour usine de pate a papier
CA1090532A (fr)	1980-12-02	Production de liqueur de pulpe a base de polysulfure
CA2164328C (fr)	2005-04-12	Combustion des liqueurs noires et traitement des boues de chaux dans une chaudiere de recuperation
CA1199454A (fr)	1986-01-21	Extraction de la chaleur et des elements chimiques des liqueurs epuisees de la fabrication de la pate a papier
CA2078958C (fr)	1995-01-17	Traitement de la fonte dans une chaudiere de recuperation