CA1172808A - Methode de recuperation du surplus des liqueurs servant a la fabrication du papier kraft - Google Patents

Methode de recuperation du surplus des liqueurs servant a la fabrication du papier kraft

Info

Publication number: CA1172808A
Authority: CA; Canada
Prior art keywords: kraft; acidified; lignin; rest; recovery
Prior art date: 1981-07-23
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000382387A

Other languages

English (en)

Inventor

Marc F. Beaupre

Emile A. Cambron

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Domtar Inc

Original Assignee

Domtar Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-07-23

Filing date

1981-07-23

Publication date

1984-08-21

1981-07-23 Application filed by Domtar Inc filed Critical Domtar Inc

1981-07-23 Priority to CA000382387A priority Critical patent/CA1172808A/fr

1982-07-16 Priority to SE8204364A priority patent/SE8204364L/

1982-07-22 Priority to FI822591A priority patent/FI75614C/fi

1982-07-23 Priority to JP12883082A priority patent/JPS5836292A/ja

1984-08-21 Application granted granted Critical

1984-08-21 Publication of CA1172808A publication Critical patent/CA1172808A/fr

Status Expired legal-status Critical Current

Links

238000011084 recovery Methods 0.000 title claims abstract description 43
239000002655 kraft paper Substances 0.000 title claims abstract description 37
229920005610 lignin Polymers 0.000 claims abstract description 26
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 23
239000002253 acid Substances 0.000 claims abstract description 18
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 29
238000000034 method Methods 0.000 claims description 29
230000008569 process Effects 0.000 claims description 29
229910052938 sodium sulfate Inorganic materials 0.000 claims description 19
235000011152 sodium sulphate Nutrition 0.000 claims description 19
238000004537 pulping Methods 0.000 claims description 10
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
239000007787 solid Substances 0.000 claims description 5
239000003513 alkali Substances 0.000 claims description 4
238000010908 decantation Methods 0.000 claims description 4
238000001914 filtration Methods 0.000 claims description 4
238000005119 centrifugation Methods 0.000 claims description 3
238000002156 mixing Methods 0.000 claims description 2
238000006386 neutralization reaction Methods 0.000 claims 3
239000000126 substance Substances 0.000 abstract description 5
238000011282 treatment Methods 0.000 abstract description 5
238000010411 cooking Methods 0.000 abstract description 3
235000000346 sugar Nutrition 0.000 description 12
150000007513 acids Chemical class 0.000 description 7
239000007788 liquid Substances 0.000 description 7
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 6
239000011734 sodium Substances 0.000 description 6
229910052708 sodium Inorganic materials 0.000 description 6
239000010446 mirabilite Substances 0.000 description 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
238000006243 chemical reaction Methods 0.000 description 4
OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 description 4
150000003839 salts Chemical class 0.000 description 4
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
238000001816 cooling Methods 0.000 description 3
238000007872 degassing Methods 0.000 description 3
239000007789 gas Substances 0.000 description 3
239000012978 lignocellulosic material Substances 0.000 description 3
238000000926 separation method Methods 0.000 description 3
239000002023 wood Substances 0.000 description 3
239000004155 Chlorine dioxide Substances 0.000 description 2
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
241001062472 Stokellia anisodon Species 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
230000003190 augmentative effect Effects 0.000 description 2
239000011230 binding agent Substances 0.000 description 2
239000001569 carbon dioxide Substances 0.000 description 2
229910002092 carbon dioxide Inorganic materials 0.000 description 2
235000019398 chlorine dioxide Nutrition 0.000 description 2
238000004090 dissolution Methods 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000000446 fuel Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
229910000037 hydrogen sulfide Inorganic materials 0.000 description 2
150000007524 organic acids Chemical class 0.000 description 2
230000020477 pH reduction Effects 0.000 description 2
229910000029 sodium carbonate Inorganic materials 0.000 description 2
235000017550 sodium carbonate Nutrition 0.000 description 2
VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000004061 bleaching Methods 0.000 description 1
238000007664 blowing Methods 0.000 description 1
239000013078 crystal Substances 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
230000004927 fusion Effects 0.000 description 1
230000036571 hydration Effects 0.000 description 1
238000006703 hydration reaction Methods 0.000 description 1
150000002484 inorganic compounds Chemical class 0.000 description 1
229910010272 inorganic material Inorganic materials 0.000 description 1
238000009434 installation Methods 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000000463 material Substances 0.000 description 1
239000000203 mixture Substances 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
235000005985 organic acids Nutrition 0.000 description 1
239000002245 particle Substances 0.000 description 1
239000001632 sodium acetate Substances 0.000 description 1
235000017281 sodium acetate Nutrition 0.000 description 1
229910052979 sodium sulfide Inorganic materials 0.000 description 1
GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
150000008163 sugars Chemical class 0.000 description 1
239000003039 volatile agent Substances 0.000 description 1

Classifications

- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/04—Regeneration of pulp liquors or effluent waste waters of alkali lye

Landscapes

Paper (AREA)
Compounds Of Unknown Constitution (AREA)

CA000382387A 1981-07-23 1981-07-23 Methode de recuperation du surplus des liqueurs servant a la fabrication du papier kraft Expired CA1172808A (fr)

Priority Applications (4)

Application Number	Priority Date	Filing Date	Title
CA000382387A CA1172808A (fr)	1981-07-23	1981-07-23	Methode de recuperation du surplus des liqueurs servant a la fabrication du papier kraft
SE8204364A SE8204364L (sv)	1981-07-23	1982-07-16	Sett for behandling av svartlut fran kraftmassaprocessen
FI822591A FI75614C (fi)	1981-07-23	1982-07-22	Aotervinningsprocess foer oeverbelastningskraft.
JP12883082A JPS5836292A (ja)	1981-07-23	1982-07-23	クラフト過負荷回収方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CA000382387A CA1172808A (fr)	1981-07-23	1981-07-23	Methode de recuperation du surplus des liqueurs servant a la fabrication du papier kraft

Publications (1)

Publication Number	Publication Date
CA1172808A true CA1172808A (fr)	1984-08-21

Family

ID=4120514

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000382387A Expired CA1172808A (fr)	1981-07-23	1981-07-23	Methode de recuperation du surplus des liqueurs servant a la fabrication du papier kraft

Country Status (4)

Country	Link
JP (1)	JPS5836292A (fr)
CA (1)	CA1172808A (fr)
FI (1)	FI75614C (fr)
SE (1)	SE8204364L (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN1109659C (zh) *	1999-04-29	2003-05-28	中国科学院化工冶金研究所	一种回收造纸黑液中碱的方法
WO2012005677A1 (fr) *	2010-07-07	2012-01-12	Stora Enso Oyj	Procédé de production de lignine précipitée à partir de liqueur noire et lignine précipitée ainsi produite

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
SE0402437D0 (sv) *	2004-10-07	2004-10-07	Stfi Packforsk Ab	Method for separating lignin from a lignin containing liquid/slurry
CL2010001609A1 (es) *	2010-12-29	2011-03-18	Univ De Concepcion 50%	Proceso para obtener tall oil util que comprende la reaccion entre una solucion de sesquisulfato de sodio y jabon de tall oil.
CN104178777B (zh) *	2014-07-18	2017-05-17	广西大学	制浆碱性废液的木素提取结合电解回收氢氧化钠的方法

1981
- 1981-07-23 CA CA000382387A patent/CA1172808A/fr not_active Expired
1982
- 1982-07-16 SE SE8204364A patent/SE8204364L/ not_active Application Discontinuation
- 1982-07-22 FI FI822591A patent/FI75614C/fi not_active IP Right Cessation
- 1982-07-23 JP JP12883082A patent/JPS5836292A/ja active Pending

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN1109659C (zh) *	1999-04-29	2003-05-28	中国科学院化工冶金研究所	一种回收造纸黑液中碱的方法
WO2012005677A1 (fr) *	2010-07-07	2012-01-12	Stora Enso Oyj	Procédé de production de lignine précipitée à partir de liqueur noire et lignine précipitée ainsi produite
US9567360B2 (en)	2010-07-07	2017-02-14	Stora Enso Oyj	Process for production of precipitated lignin from black liquor and precipitated lignin produced by the process

Also Published As

Publication number	Publication date
FI75614B (fi)	1988-03-31
FI75614C (fi)	1988-07-11
FI822591A0 (fi)	1982-07-22
SE8204364D0 (sv)	1982-07-16
FI822591L (fi)	1983-01-24
SE8204364L (sv)	1983-01-24
JPS5836292A (ja)	1983-03-03

Legal Events

Date	Code	Title	Description
2001-08-21	MKEX	Expiry

Publication	Publication Date	Title
US4470876A (en)	1984-09-11	Kraft overload recovery process
EP1797236B1 (fr)	2011-06-15	Procede de separation de lignine d'un liquide/d'une boue contenant de la lignine
CN104603357B (zh)	2017-03-29	回收制浆化学品和减少其中的钾和氯浓度的方法
EP0908554B1 (fr)	2010-06-23	Procédé pour la récupération des sels alcalins et de l' énergie à partir d'une liqueur noire contenant du silicate
CA2706663C (fr)	2016-01-12	Procede visant a l'extraction du sel d'ammonium et du methanol dans un liquide obtenu a partir des condensats vicies dans une usine de pate de cellulose
AU681613B2 (en)	1997-09-04	Method of bleaching pulp without using chlorine-containing chemicals
US4302281A (en)	1981-11-24	Method for producing pulp
US4504356A (en)	1985-03-12	Continuous process of removing silica from spent pulping liquors
US3833462A (en)	1974-09-03	Process of removing sodium chloride from kraft pulping process chemical recovery systems
EP0903436B1 (fr)	2001-05-23	Procédé pour l'imprégnation et digestion de matériaux lignocellulosiques
US6830696B1 (en)	2004-12-14	Treatment of spent pulping liquor with lignin separation to recover alkali pulping chemicals in manufacture of paper pulp
US2792350A (en)	1957-05-14	Treatment of sodium base sulfite residual liquor
FI75614B (fi)	1988-03-31	Aotervinningsprocess foer oeverbelastningskraft.
CA1163424A (fr)	1984-03-13	Methode de separation de l'ammoniac
US3525666A (en)	1970-08-25	Process for preparing kraft pulping liquor from black liquor including separate carbonation with combustion gases and evaporation steps
CA1247809A (fr)	1989-01-03	Procede de recuperation de lessive residuelle
US5989387A (en)	1999-11-23	Method for controlling chloride concentration in the flue gas of a recovery boiler
JP4205855B2 (ja)	2009-01-07	ポリサルファイドパルプ化プロセス
EP0687766A1 (fr)	1995-12-20	Procédé pour la manufacturing de liqueurs de cuisson par crystallisation de la liqueur verte
US3554858A (en)	1971-01-12	Process for regeneration of white liquor with hydrogen sulfide recycle
CA1053412A (fr)	1979-05-01	Procede et appareil de recuperation du soufre d'un defibrage au polysulfure
US5562804A (en)	1996-10-08	Method for adjusting the sulphur/sodium ratio in the flue gases of a soda recovery boiler
JPS5836291A (ja)	1983-03-03	アルカリパルプ化薬品回収系
US5976318A (en)	1999-11-02	Method for burning secondary sludge in a recovery boiler
JP2713429B2 (ja)	1998-02-16	硫酸塩パルププロセスを行う方法および装置