CA1174054A - Separation simultanee de l'indium, du cadmium, du zinc et du cuivre en presence dans les poussieres de fonderie ou d'affinage du plomb, du cuivre et du zinc - Google Patents
Separation simultanee de l'indium, du cadmium, du zinc et du cuivre en presence dans les poussieres de fonderie ou d'affinage du plomb, du cuivre et du zincInfo
- Publication number
- CA1174054A CA1174054A CA000381428A CA381428A CA1174054A CA 1174054 A CA1174054 A CA 1174054A CA 000381428 A CA000381428 A CA 000381428A CA 381428 A CA381428 A CA 381428A CA 1174054 A CA1174054 A CA 1174054A
- Authority
- CA
- Canada
- Prior art keywords
- zinc
- copper
- indium
- cadmium
- hydroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052738 indium Inorganic materials 0.000 title claims abstract description 78
- 239000010949 copper Substances 0.000 title claims abstract description 77
- 239000011701 zinc Substances 0.000 title claims abstract description 77
- 229910052802 copper Inorganic materials 0.000 title claims abstract description 76
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 title claims abstract description 76
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 75
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 title claims abstract description 75
- 229910052725 zinc Inorganic materials 0.000 title claims abstract description 75
- 229910052793 cadmium Inorganic materials 0.000 title claims abstract description 62
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 title claims abstract description 60
- 239000011133 lead Substances 0.000 title claims description 28
- 238000011084 recovery Methods 0.000 title claims description 13
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 58
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 52
- 239000000706 filtrate Substances 0.000 claims abstract description 28
- 239000000428 dust Substances 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 25
- 238000001914 filtration Methods 0.000 claims abstract description 13
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052751 metal Inorganic materials 0.000 claims abstract description 12
- 239000002184 metal Substances 0.000 claims abstract description 12
- 238000001556 precipitation Methods 0.000 claims abstract description 12
- 150000002739 metals Chemical class 0.000 claims abstract description 8
- 238000002386 leaching Methods 0.000 claims abstract description 7
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims abstract description 6
- 235000011941 Tilia x europaea Nutrition 0.000 claims abstract description 6
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 6
- 239000004571 lime Substances 0.000 claims abstract description 6
- 239000012065 filter cake Substances 0.000 claims abstract description 5
- 239000002244 precipitate Substances 0.000 claims description 40
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 230000003472 neutralizing effect Effects 0.000 claims description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims 3
- 239000000908 ammonium hydroxide Substances 0.000 claims 3
- 238000004821 distillation Methods 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 19
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 13
- 238000004458 analytical method Methods 0.000 description 11
- 229910052787 antimony Inorganic materials 0.000 description 10
- 229910052742 iron Inorganic materials 0.000 description 10
- 229910052785 arsenic Inorganic materials 0.000 description 9
- 229910052797 bismuth Inorganic materials 0.000 description 9
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 8
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 8
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 8
- 239000000920 calcium hydroxide Substances 0.000 description 8
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 8
- 235000011116 calcium hydroxide Nutrition 0.000 description 8
- 229910052782 aluminium Inorganic materials 0.000 description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 7
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 6
- 239000002253 acid Substances 0.000 description 5
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 229910052718 tin Inorganic materials 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000007670 refining Methods 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical group O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 238000003556 assay Methods 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000001627 detrimental effect Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 229910052745 lead Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000001226 reprecipitation Methods 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000010960 commercial process Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- UJXZVRRCKFUQKG-UHFFFAOYSA-K indium(3+);phosphate Chemical compound [In+3].[O-]P([O-])([O-])=O UJXZVRRCKFUQKG-UHFFFAOYSA-K 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 208000020442 loss of weight Diseases 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- UOURRHZRLGCVDA-UHFFFAOYSA-D pentazinc;dicarbonate;hexahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[O-]C([O-])=O.[O-]C([O-])=O UOURRHZRLGCVDA-UHFFFAOYSA-D 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 229910052716 thallium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/02—Working-up flue dust
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B58/00—Obtaining gallium or indium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacture And Refinement Of Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA000381428A CA1174054A (fr) | 1981-07-09 | 1981-07-09 | Separation simultanee de l'indium, du cadmium, du zinc et du cuivre en presence dans les poussieres de fonderie ou d'affinage du plomb, du cuivre et du zinc |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA000381428A CA1174054A (fr) | 1981-07-09 | 1981-07-09 | Separation simultanee de l'indium, du cadmium, du zinc et du cuivre en presence dans les poussieres de fonderie ou d'affinage du plomb, du cuivre et du zinc |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1174054A true CA1174054A (fr) | 1984-09-11 |
Family
ID=4120405
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000381428A Expired CA1174054A (fr) | 1981-07-09 | 1981-07-09 | Separation simultanee de l'indium, du cadmium, du zinc et du cuivre en presence dans les poussieres de fonderie ou d'affinage du plomb, du cuivre et du zinc |
Country Status (1)
| Country | Link |
|---|---|
| CA (1) | CA1174054A (fr) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2279493C1 (ru) * | 2004-12-27 | 2006-07-10 | Открытое Акционерное Общество "Челябинский цинковый завод" | Способ получения монохлорида индия высокой чистоты из чернового металлического индия |
| DE102017107097A1 (de) | 2017-04-03 | 2018-10-04 | Technische Universität Bergakademie Freiberg | Verfahren zur Abtrennung von Indium aus metallhaltigen, wässrigen Lösungen |
| DE102017213956B3 (de) | 2017-08-10 | 2018-12-06 | Technische Universität Bergakademie Freiberg | Verfahren zur Gewinnung von Indium aus wässrigen, metallhaltigen Lösungen |
| RU2752722C1 (ru) * | 2020-12-04 | 2021-07-30 | Негосударственное частное образовательное учреждение высшего образования "Технический университет УГМК" | Способ переработки свинцовых кеков |
| CN113737020A (zh) * | 2021-09-10 | 2021-12-03 | 广西万仕智稀贵金属科技有限公司 | 一种粗锑精炼过程深度除镉的方法 |
| CN115505751A (zh) * | 2022-10-01 | 2022-12-23 | 红河学院 | 一种从硫化铜矿中富集锗和铟联产粗铜的方法 |
| CN116555574A (zh) * | 2023-06-07 | 2023-08-08 | 浙江中创资源循环利用创新中心有限公司 | 一种除铜镍镉试剂及应用其的再生铅去除铜镍镉的方法 |
| CN116790905A (zh) * | 2023-08-07 | 2023-09-22 | 湖南株冶有色金属有限公司 | 粗铟除镉和锌的方法 |
-
1981
- 1981-07-09 CA CA000381428A patent/CA1174054A/fr not_active Expired
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2279493C1 (ru) * | 2004-12-27 | 2006-07-10 | Открытое Акционерное Общество "Челябинский цинковый завод" | Способ получения монохлорида индия высокой чистоты из чернового металлического индия |
| DE102017107097A1 (de) | 2017-04-03 | 2018-10-04 | Technische Universität Bergakademie Freiberg | Verfahren zur Abtrennung von Indium aus metallhaltigen, wässrigen Lösungen |
| DE102017107097B4 (de) | 2017-04-03 | 2024-02-08 | Technische Universität Bergakademie Freiberg | Verfahren zur Abtrennung von Indium aus metallhaltigen, wässrigen Lösungen |
| DE102017213956B3 (de) | 2017-08-10 | 2018-12-06 | Technische Universität Bergakademie Freiberg | Verfahren zur Gewinnung von Indium aus wässrigen, metallhaltigen Lösungen |
| RU2752722C1 (ru) * | 2020-12-04 | 2021-07-30 | Негосударственное частное образовательное учреждение высшего образования "Технический университет УГМК" | Способ переработки свинцовых кеков |
| CN113737020A (zh) * | 2021-09-10 | 2021-12-03 | 广西万仕智稀贵金属科技有限公司 | 一种粗锑精炼过程深度除镉的方法 |
| CN115505751A (zh) * | 2022-10-01 | 2022-12-23 | 红河学院 | 一种从硫化铜矿中富集锗和铟联产粗铜的方法 |
| CN116555574A (zh) * | 2023-06-07 | 2023-08-08 | 浙江中创资源循环利用创新中心有限公司 | 一种除铜镍镉试剂及应用其的再生铅去除铜镍镉的方法 |
| CN116790905A (zh) * | 2023-08-07 | 2023-09-22 | 湖南株冶有色金属有限公司 | 粗铟除镉和锌的方法 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |