CA1196877A - Hydrogenation de la houille a retention accrue de solides dans un reacteur a lit bouillonnant - Google Patents

Hydrogenation de la houille a retention accrue de solides dans un reacteur a lit bouillonnant

Info

Publication number: CA1196877A
Authority: CA; Canada
Prior art keywords: liquid; reactor; solids; coal; baffle
Prior art date: 1981-12-21
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000418157A

Other languages

English (en)

Inventor

Michael C. Chervenak

Alfred G. Comolli

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

HRI Inc

Original Assignee

HRI Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-12-21

Filing date

1982-12-20

Publication date

1985-11-19

1982-12-20 Application filed by HRI Inc filed Critical HRI Inc

1985-11-19 Application granted granted Critical

1985-11-19 Publication of CA1196877A publication Critical patent/CA1196877A/fr

Status Expired legal-status Critical Current

Links

239000007787 solid Substances 0.000 title claims abstract description 114
239000003245 coal Substances 0.000 title claims abstract description 85
238000005984 hydrogenation reaction Methods 0.000 title claims description 15
230000014759 maintenance of location Effects 0.000 title description 8
239000007788 liquid Substances 0.000 claims abstract description 90
238000000034 method Methods 0.000 claims abstract description 25
230000008569 process Effects 0.000 claims abstract description 23
238000006243 chemical reaction Methods 0.000 claims abstract description 22
239000004215 Carbon black (E152) Substances 0.000 claims abstract description 19
229930195733 hydrocarbon Natural products 0.000 claims abstract description 19
150000002430 hydrocarbons Chemical class 0.000 claims abstract description 19
238000000926 separation method Methods 0.000 claims abstract description 15
239000000047 product Substances 0.000 claims abstract description 14
239000012263 liquid product Substances 0.000 claims abstract description 7
238000011144 upstream manufacturing Methods 0.000 claims abstract description 5
238000009903 catalytic hydrogenation reaction Methods 0.000 claims abstract description 4
239000003054 catalyst Substances 0.000 claims description 32
239000007789 gas Substances 0.000 claims description 19
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 15
239000002245 particle Substances 0.000 claims description 14
229910052739 hydrogen Inorganic materials 0.000 claims description 13
239000001257 hydrogen Substances 0.000 claims description 13
239000002002 slurry Substances 0.000 claims description 12
239000003921 oil Substances 0.000 claims description 10
230000003197 catalytic effect Effects 0.000 claims description 7
239000000463 material Substances 0.000 claims description 6
239000010742 number 1 fuel oil Substances 0.000 claims description 4
239000012071 phase Substances 0.000 claims description 4
239000007791 liquid phase Substances 0.000 claims description 3
239000003034 coal gas Substances 0.000 claims description 2
238000005194 fractionation Methods 0.000 claims description 2
238000004064 recycling Methods 0.000 claims description 2
239000003250 coal slurry Substances 0.000 claims 1
238000004821 distillation Methods 0.000 claims 1
230000002035 prolonged effect Effects 0.000 abstract description 3
238000009835 boiling Methods 0.000 description 5
230000000717 retained effect Effects 0.000 description 5
238000006555 catalytic reaction Methods 0.000 description 3
238000001556 precipitation Methods 0.000 description 3
239000002904 solvent Substances 0.000 description 3
238000005292 vacuum distillation Methods 0.000 description 3
239000002802 bituminous coal Substances 0.000 description 2
230000000694 effects Effects 0.000 description 2
150000002431 hydrogen Chemical class 0.000 description 2
239000002956 ash Substances 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
238000004517 catalytic hydrocracking Methods 0.000 description 1
238000004939 coking Methods 0.000 description 1
230000002301 combined effect Effects 0.000 description 1
230000008030 elimination Effects 0.000 description 1
238000003379 elimination reaction Methods 0.000 description 1
230000003628 erosive effect Effects 0.000 description 1
238000001914 filtration Methods 0.000 description 1
238000004508 fractional distillation Methods 0.000 description 1
239000000446 fuel Substances 0.000 description 1
239000010763 heavy fuel oil Substances 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
239000011707 mineral Substances 0.000 description 1
239000000203 mixture Substances 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000005191 phase separation Methods 0.000 description 1
238000004886 process control Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
239000000376 reactant Substances 0.000 description 1
239000012056 semi-solid material Substances 0.000 description 1
239000003476 subbituminous coal Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/06—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by destructive hydrogenation
- C10G1/065—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by destructive hydrogenation in the presence of a solvent
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/005—Separating solid material from the gas/liquid stream
- B01J8/0065—Separating solid material from the gas/liquid stream by impingement against stationary members
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/08—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts
- C10G1/083—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts in the presence of a solvent

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Life Sciences & Earth Sciences (AREA)
Wood Science & Technology (AREA)
General Chemical & Material Sciences (AREA)
Combustion & Propulsion (AREA)
Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

CA000418157A 1981-12-21 1982-12-20 Hydrogenation de la houille a retention accrue de solides dans un reacteur a lit bouillonnant Expired CA1196877A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US33243381A	1981-12-21	1981-12-21
US332,433		1981-12-21

Publications (1)

Publication Number	Publication Date
CA1196877A true CA1196877A (fr)	1985-11-19

Family

ID=23298216

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000418157A Expired CA1196877A (fr)	1981-12-21	1982-12-20	Hydrogenation de la houille a retention accrue de solides dans un reacteur a lit bouillonnant

Country Status (6)

Country	Link
JP (1)	JPS58111892A (fr)
AU (1)	AU9137582A (fr)
CA (1)	CA1196877A (fr)
DE (1)	DE3245494A1 (fr)
GB (1)	GB2111848A (fr)
ZA (1)	ZA829012B (fr)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN104818050A (zh) *	2015-05-07	2015-08-05	北京中科诚毅科技发展有限公司	一种多重优化的浆态床加氢反应器及其用途与设计方法
CN107694483A (zh) *	2017-09-22	2018-02-16	北京中科诚毅科技发展有限公司	一种新型结构加氢反应器及其设计方法与用途
CN108970544A (zh) *	2017-06-02	2018-12-11	何巨堂	一种气液料上流加氢反应器的液相产物回流动力增加方法
CN111804245A (zh) *	2019-04-12	2020-10-23	Ifp 新能源公司	包括具有逐渐减小的截面和变化的倾斜角的再循环杯的三相反应器

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4495055A (en) *	1982-04-05	1985-01-22	Hri, Inc.	Coal catalytic hydrogenation process using direct coal slurry feed to reactor with controlled mixing conditions
US4557904A (en) *	1984-03-26	1985-12-10	Union Carbide Corporation	Integral reactor apparatus
US6846405B2 (en) *	2001-08-31	2005-01-25	Exxonmobil Chemical Patents Inc.	Circulating fluid bed reactor system
DE102005021056A1 (de) *	2005-05-06	2006-11-09	Basf Ag	Verfahren zur Isolierung von Methylglycinnitril-N,N-diacetonitrilen aus einem wässrigen Rohgemisch
CN107790073A (zh) *	2017-09-28	2018-03-13	北京中科诚毅科技发展有限公司	一种反应器新型内部结构及其设计方法和用途
CN108148739B (zh) *	2018-02-08	2023-05-16	沈阳农业大学	循环脱气式流化床生物反应器
WO2021050010A1 (fr) *	2019-09-09	2021-03-18	Ptt Exploration And Production Public Company Limited	Dispositif de décontamination de condensat
CN113566470B (zh) *	2021-08-20	2023-01-31	楼建军	一种氢浆发生器、连续批量制备氢浆的系统及方法

1982
- 1982-12-03 GB GB08234509A patent/GB2111848A/en not_active Withdrawn
- 1982-12-08 ZA ZA829012A patent/ZA829012B/xx unknown
- 1982-12-09 AU AU91375/82A patent/AU9137582A/en not_active Abandoned
- 1982-12-09 DE DE19823245494 patent/DE3245494A1/de not_active Withdrawn
- 1982-12-20 JP JP57222242A patent/JPS58111892A/ja active Pending
- 1982-12-20 CA CA000418157A patent/CA1196877A/fr not_active Expired

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN104818050A (zh) *	2015-05-07	2015-08-05	北京中科诚毅科技发展有限公司	一种多重优化的浆态床加氢反应器及其用途与设计方法
CN108970544A (zh) *	2017-06-02	2018-12-11	何巨堂	一种气液料上流加氢反应器的液相产物回流动力增加方法
CN107694483A (zh) *	2017-09-22	2018-02-16	北京中科诚毅科技发展有限公司	一种新型结构加氢反应器及其设计方法与用途
CN107694483B (zh) *	2017-09-22	2018-12-21	北京中科诚毅科技发展有限公司	一种加氢反应器及其设计方法与用途
CN111804245A (zh) *	2019-04-12	2020-10-23	Ifp 新能源公司	包括具有逐渐减小的截面和变化的倾斜角的再循环杯的三相反应器
CN111804245B (zh) *	2019-04-12	2024-01-09	Ifp 新能源公司	包括具有逐渐减小的截面和变化的倾斜角的再循环杯的三相反应器

Also Published As

Publication number	Publication date
JPS58111892A (ja)	1983-07-04
ZA829012B (en)	1984-09-26
AU9137582A (en)	1983-06-30
GB2111848A (en)	1983-07-13
DE3245494A1 (de)	1983-06-30

Legal Events

Date	Code	Title	Description
2002-11-20	MKEC	Expiry (correction)
2002-12-20	MKEX	Expiry

Publication	Publication Date	Title
CA1229570A (fr)	1987-11-24	Hydroconversion catalytique bi-etagee des charges d'hydrocarbures par recyclage des residus
US2987465A (en)	1961-06-06	Gas-liquid contacting process
US6835756B2 (en)	2004-12-28	Fischer-tropsch synthesis process
USRE25770E (en)	1965-04-27	Gas-liquid contacting process
US5374348A (en)	1994-12-20	Hydrocracking of heavy hydrocarbon oils with heavy hydrocarbon recycle
CA1108079A (fr)	1981-09-01	Hydrogenation etagee de charbon de mauvaise qualite
US3622498A (en)	1971-11-23	Slurry processing for black oil conversion
DE69322475T2 (de)	1999-08-05	Verfahren zur katalytischen Umsetzung von Wasserstoff und Kohlenmonoxid
US6270654B1 (en)	2001-08-07	Catalytic hydrogenation process utilizing multi-stage ebullated bed reactors
US3321393A (en)	1967-05-23	Hydrogenation of coal
US3412010A (en)	1968-11-19	High conversion level hydrogenation of residuum
US3197288A (en)	1965-07-27	Catalytic reactor
US3617465A (en)	1971-11-02	Coal hydrogenation
US3622495A (en)	1971-11-23	Multiple-stage slurry processing for black oil conversion
US3188286A (en)	1965-06-08	Hydrocracking heavy hydrocarbon oil
GB2111848A (en)	1983-07-13	Coal hydrogenation process and apparatus having increased solids retention in ebullated bed reactor
US4045329A (en)	1977-08-30	Coal hydrogenation with selective recycle of liquid to reactor
US3635943A (en)	1972-01-18	Hydrotreating process with coarse and fine catalysts
US3151057A (en)	1964-09-29	Suspension hydrogenation of heavy stocks
KR100493978B1 (ko)	2005-09-02	탄화수소공급원료의유동층접촉분해방법및장치
US4159240A (en)	1979-06-26	Separating liquid and solid products of liquefaction of coal or like carbonaceous materials
US3338820A (en)	1967-08-29	High conversion level hydrogenation of residuum
US3291721A (en)	1966-12-13	Combined hydrocracking and hydrofining process
US2498088A (en)	1950-02-21	Conversion of hydrocarbons with suspended catalyst
US2459444A (en)	1949-01-18	Hydrocarbon synthesis