CA1232902A - Cristallisation du fructose a l'aide d'alcools - Google Patents

Cristallisation du fructose a l'aide d'alcools

Info

Publication number: CA1232902A
Authority: CA; Canada
Prior art keywords: fructose; aqueous; dispersion; alcohols; ethanol
Prior art date: 1984-03-09
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000474319A

Other languages

English (en)

Inventor

Gary A. Day

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Primary Products Ingredients Americas LLC

Original Assignee

Tate and Lyle Ingredients Americas LLC

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-03-09

Filing date

1985-02-14

Publication date

1988-02-16

1984-03-09 Priority claimed from US06/588,479 external-priority patent/US4643773A/en

1985-02-14 Application filed by Tate and Lyle Ingredients Americas LLC filed Critical Tate and Lyle Ingredients Americas LLC

1988-02-16 Application granted granted Critical

1988-02-16 Publication of CA1232902A publication Critical patent/CA1232902A/fr

Status Expired legal-status Critical Current

Links

RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 title claims abstract description 76
229930091371 Fructose Natural products 0.000 title claims abstract description 76
239000005715 Fructose Substances 0.000 title claims abstract description 76
150000001298 alcohols Chemical class 0.000 title claims abstract description 26
238000002425 crystallisation Methods 0.000 title claims abstract description 9
230000008025 crystallization Effects 0.000 title claims abstract description 9
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 59
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 24
239000000203 mixture Substances 0.000 claims abstract description 21
239000006185 dispersion Substances 0.000 claims description 27
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 20
238000000034 method Methods 0.000 claims description 20
238000010899 nucleation Methods 0.000 claims description 12
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 9
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
239000008121 dextrose Substances 0.000 claims description 8
238000002156 mixing Methods 0.000 claims description 8
239000007787 solid Substances 0.000 claims description 8
150000001720 carbohydrates Chemical class 0.000 claims description 4
238000011084 recovery Methods 0.000 claims description 4
229960004592 isopropanol Drugs 0.000 claims 3
229920000136 polysorbate Polymers 0.000 claims 1
239000006188 syrup Substances 0.000 description 16
235000020357 syrup Nutrition 0.000 description 16
WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 8
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 6
229930006000 Sucrose Natural products 0.000 description 6
239000005720 sucrose Substances 0.000 description 5
240000008042 Zea mays Species 0.000 description 3
235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 3
235000002017 Zea mays subsp mays Nutrition 0.000 description 3
235000005822 corn Nutrition 0.000 description 3
239000000463 material Substances 0.000 description 3
238000000926 separation method Methods 0.000 description 3
239000000243 solution Substances 0.000 description 3
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 2
230000000052 comparative effect Effects 0.000 description 2
238000001816 cooling Methods 0.000 description 2
239000002002 slurry Substances 0.000 description 2
235000016068 Berberis vulgaris Nutrition 0.000 description 1
241000335053 Beta vulgaris Species 0.000 description 1
241000196324 Embryophyta Species 0.000 description 1
235000010650 Hyssopus officinalis Nutrition 0.000 description 1
240000001812 Hyssopus officinalis Species 0.000 description 1
229920001202 Inulin Polymers 0.000 description 1
241000694408 Isomeris Species 0.000 description 1
235000012839 cake mixes Nutrition 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000018044 dehydration Effects 0.000 description 1
238000006297 dehydration reaction Methods 0.000 description 1
239000003398 denaturant Substances 0.000 description 1
-1 dextrose Chemical class 0.000 description 1
235000013681 dietary sucrose Nutrition 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
235000013305 food Nutrition 0.000 description 1
235000003599 food sweetener Nutrition 0.000 description 1
238000009472 formulation Methods 0.000 description 1
239000008103 glucose Substances 0.000 description 1
239000008187 granular material Substances 0.000 description 1
230000000977 initiatory effect Effects 0.000 description 1
JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 description 1
229940029339 inulin Drugs 0.000 description 1
238000006317 isomerization reaction Methods 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
239000002245 particle Substances 0.000 description 1
239000000843 powder Substances 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
238000007670 refining Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
239000012047 saturated solution Substances 0.000 description 1
235000014214 soft drink Nutrition 0.000 description 1
238000003756 stirring Methods 0.000 description 1
235000000346 sugar Nutrition 0.000 description 1
239000003765 sweetening agent Substances 0.000 description 1

Landscapes

Saccharide Compounds (AREA)

CA000474319A 1984-03-09 1985-02-14 Cristallisation du fructose a l'aide d'alcools Expired CA1232902A (fr)

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date	Title
US06/588,479 US4643773A (en)	1984-03-09	1984-03-09	Crystallization of fructose utilizing a mixture of alcohols
US06/588,479		1984-03-09
US69698285A	1985-01-31	1985-01-31
US696,982		1985-01-31

Publications (1)

Publication Number	Publication Date
CA1232902A true CA1232902A (fr)	1988-02-16

Family

ID=27080297

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000474319A Expired CA1232902A (fr)	1984-03-09	1985-02-14	Cristallisation du fructose a l'aide d'alcools

Country Status (1)

Country	Link
CA (1)	CA1232902A (fr)

1985
- 1985-02-14 CA CA000474319A patent/CA1232902A/fr not_active Expired

Legal Events

Date	Code	Title	Description
2005-02-16	MKEX	Expiry
2023-05-26	MKEX	Expiry	Effective date: 20050216

Publication	Publication Date	Title
US4643773A (en)	1987-02-17	Crystallization of fructose utilizing a mixture of alcohols
US4199374A (en)	1980-04-22	Process of preparing crystalline fructose from high fructose corn syrup
JP3751033B2 (ja)	2006-03-01	長鎖イヌリンの製造方法
KR100531965B1 (ko)	2006-02-02	용액으로부터 유기화합물의 회수 방법
DE69617088T2 (de)	2002-06-20	Verfahren zur Herstellung von kristallisiertem Maltit und diesen enthaltenden Kristallinen.
MXPA97000916A (en)	1998-04-01	Preparation of inul products
DE69525839T2 (de)	2002-10-31	Kristallisierung von alpha-L-aspartyl-L-phenylalaninmethylester aus wässerigen Lösungen
WO2021239813A1 (fr)	2021-12-02	Cristallisation d'allulose sous pression réduite
EP0109009B1 (fr)	1987-05-13	Procédé pour la préparation de 1-0-alpha-D-glucopyranisido-D-fructose
DE3446380C1 (de)	1986-05-22	Suessungsmittel,Verfahren zur Herstellung und Verwendung desselben
DE69631689T2 (de)	2005-01-13	Kristalline 1-kestose und verfahren zu ihrer herstellung
EP0983392B1 (fr)	2003-03-19	Methode de cristallisation
CH496093A (de)	1970-09-15	Verfahren zur Herstellung von Cyclodextrin
CA1232902A (fr)	1988-02-16	Cristallisation du fructose a l'aide d'alcools
DE2166121C3 (de)	1981-02-26	Verfahren zur Herstellung von Verzuckerungsprodukten von Stärke
EP0155803B1 (fr)	1988-08-03	Préparation de fructose cristalline
EP0156571A2 (fr)	1985-10-02	Cristallisation de fructose
US6756490B2 (en)	2004-06-29	Method of crystallizing maltitol
WO2022219094A1 (fr)	2022-10-20	Processus de production de compositions d'isomalt enrichies en 1,1-gpm et/ou en 1,6-gps
DE60010787T2 (de)	2005-07-14	Vefahren zur Herstellung von hochreiner alphakristalliner wasserfreier Dextrose
CH641205A5 (en)	1984-02-15	Process for the production of maltose crystals
EP0081185B1 (fr)	1984-08-29	Procédé et dispositif pour la fabrication d'isomérose
US4888060A (en)	1989-12-19	Enrichment of fructose syrups
JPH0517239B2 (fr)	1993-03-08
Jackson et al.	1926	The preparation of levulose