CA1317961C - Methode d'extraction au solvent des matieres essentielles contenues dans les plants - Google Patents

Methode d'extraction au solvent des matieres essentielles contenues dans les plants

Info

Publication number: CA1317961C
Authority: CA; Canada
Prior art keywords: tobacco; acid; nicotine; solvent; extraction
Prior art date: 1986-12-29
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA000555304A

Other languages

English (en)

Inventor

Harvey J. Grubbs

Ravi Prasad

Tony M. Howell

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

PHILIP MORRIS PRODUCTS Inc

Original Assignee

PHILIP MORRIS PRODUCTS Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1986-12-29

Filing date

1987-12-23

Publication date

1993-05-18

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25485521&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA1317961(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

1987-12-23 Application filed by PHILIP MORRIS PRODUCTS Inc filed Critical PHILIP MORRIS PRODUCTS Inc

1993-05-18 Application granted granted Critical

1993-05-18 Publication of CA1317961C publication Critical patent/CA1317961C/fr

2010-05-18 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 67
230000008569 process Effects 0.000 title abstract description 32
239000000463 material Substances 0.000 title abstract description 27
238000000638 solvent extraction Methods 0.000 title 1
241000208125 Nicotiana Species 0.000 claims abstract description 145
235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 145
238000000605 extraction Methods 0.000 claims abstract description 104
SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims abstract description 93
229960002715 nicotine Drugs 0.000 claims abstract description 86
SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims abstract description 86
239000002904 solvent Substances 0.000 claims abstract description 82
239000002253 acid Substances 0.000 claims abstract description 49
239000000126 substance Substances 0.000 claims abstract description 18
241000196324 Embryophyta Species 0.000 claims abstract description 11
239000007788 liquid Substances 0.000 claims abstract description 4
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 35
229910002092 carbon dioxide Inorganic materials 0.000 claims description 31
150000003839 salts Chemical group 0.000 claims description 18
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 14
229930182474 N-glycoside Natural products 0.000 claims description 14
239000001569 carbon dioxide Substances 0.000 claims description 12
150000007513 acids Chemical class 0.000 claims description 10
239000000945 filler Substances 0.000 claims description 10
ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 9
QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 8
229910052799 carbon Inorganic materials 0.000 claims description 8
ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims description 7
229910000013 Ammonium bicarbonate Inorganic materials 0.000 claims description 7
229920000742 Cotton Polymers 0.000 claims description 7
235000012538 ammonium bicarbonate Nutrition 0.000 claims description 7
239000001099 ammonium carbonate Substances 0.000 claims description 7
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 6
239000004744 fabric Substances 0.000 claims description 6
BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 6
GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 claims description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 5
229920002678 cellulose Polymers 0.000 claims description 5
239000001913 cellulose Substances 0.000 claims description 5
150000002341 glycosylamines Chemical class 0.000 claims description 5
235000015861 monopotassium citrate Nutrition 0.000 claims description 5
239000002444 monopotassium citrate Substances 0.000 claims description 5
WKZJASQVARUVAW-UHFFFAOYSA-M potassium;hydron;2-hydroxypropane-1,2,3-tricarboxylate Chemical compound [K+].OC(=O)CC(O)(C(O)=O)CC([O-])=O WKZJASQVARUVAW-UHFFFAOYSA-M 0.000 claims description 5
NAVWVHRQSDHCHD-UHFFFAOYSA-N 2-hydroxypropane-1,2,3-tricarboxylic acid;potassium Chemical compound [K].OC(=O)CC(O)(C(O)=O)CC(O)=O NAVWVHRQSDHCHD-UHFFFAOYSA-N 0.000 claims description 4
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 4
208000007976 Ketosis Diseases 0.000 claims description 4
150000001323 aldoses Chemical class 0.000 claims description 4
150000002584 ketoses Chemical class 0.000 claims description 4
229910052786 argon Inorganic materials 0.000 claims description 3
150000008282 halocarbons Chemical class 0.000 claims description 3
229930195733 hydrocarbon Natural products 0.000 claims description 3
150000002430 hydrocarbons Chemical class 0.000 claims description 3
235000015497 potassium bicarbonate Nutrition 0.000 claims description 3
229910000027 potassium carbonate Inorganic materials 0.000 claims description 3
235000011181 potassium carbonates Nutrition 0.000 claims description 3
229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
JCXJVPUVTGWSNB-UHFFFAOYSA-N Nitrogen dioxide Chemical compound O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 claims 2
GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims 2
229910018503 SF6 Inorganic materials 0.000 claims 2
UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims 2
239000011260 aqueous acid Substances 0.000 claims 2
239000011736 potassium bicarbonate Substances 0.000 claims 2
229910000028 potassium bicarbonate Inorganic materials 0.000 claims 2
TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 claims 2
239000012266 salt solution Substances 0.000 claims 2
235000017550 sodium carbonate Nutrition 0.000 claims 2
SFZCNBIFKDRMGX-UHFFFAOYSA-N sulfur hexafluoride Chemical compound FS(F)(F)(F)(F)F SFZCNBIFKDRMGX-UHFFFAOYSA-N 0.000 claims 2
239000000306 component Substances 0.000 description 23
239000000796 flavoring agent Substances 0.000 description 17
235000019634 flavors Nutrition 0.000 description 17
239000002585 base Substances 0.000 description 14
239000000203 mixture Substances 0.000 description 14
239000003463 adsorbent Substances 0.000 description 13
239000001508 potassium citrate Substances 0.000 description 13
229960002635 potassium citrate Drugs 0.000 description 13
QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 description 13
235000011082 potassium citrates Nutrition 0.000 description 13
244000299461 Theobroma cacao Species 0.000 description 8
235000009470 Theobroma cacao Nutrition 0.000 description 8
239000000758 substrate Substances 0.000 description 8
150000001875 compounds Chemical class 0.000 description 7
230000000391 smoking effect Effects 0.000 description 7
239000000243 solution Substances 0.000 description 7
235000011089 carbon dioxide Nutrition 0.000 description 6
239000000047 product Substances 0.000 description 6
-1 tartaric Chemical class 0.000 description 6
239000003039 volatile agent Substances 0.000 description 6
239000007864 aqueous solution Substances 0.000 description 5
230000009467 reduction Effects 0.000 description 5
238000006722 reduction reaction Methods 0.000 description 5
230000002411 adverse Effects 0.000 description 4
238000006386 neutralization reaction Methods 0.000 description 4
235000019505 tobacco product Nutrition 0.000 description 4
125000003277 amino group Chemical group 0.000 description 3
150000007514 bases Chemical class 0.000 description 3
230000008901 benefit Effects 0.000 description 3
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
238000002474 experimental method Methods 0.000 description 3
230000005484 gravity Effects 0.000 description 3
229910052751 metal Inorganic materials 0.000 description 3
239000002184 metal Substances 0.000 description 3
OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 3
229920006395 saturated elastomer Polymers 0.000 description 3
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 description 2
150000001412 amines Chemical class 0.000 description 2
229910021529 ammonia Inorganic materials 0.000 description 2
239000006227 byproduct Substances 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
239000000919 ceramic Substances 0.000 description 2
238000005056 compaction Methods 0.000 description 2
238000013461 design Methods 0.000 description 2
230000009977 dual effect Effects 0.000 description 2
239000000284 extract Substances 0.000 description 2
239000012632 extractable Substances 0.000 description 2
239000012458 free base Substances 0.000 description 2
239000004615 ingredient Substances 0.000 description 2
238000011068 loading method Methods 0.000 description 2
238000013508 migration Methods 0.000 description 2
230000005012 migration Effects 0.000 description 2
DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 2
230000000717 retained effect Effects 0.000 description 2
CMXPERZAMAQXSF-UHFFFAOYSA-M sodium;1,4-bis(2-ethylhexoxy)-1,4-dioxobutane-2-sulfonate;1,8-dihydroxyanthracene-9,10-dione Chemical compound [Na+].O=C1C2=CC=CC(O)=C2C(=O)C2=C1C=CC=C2O.CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC CMXPERZAMAQXSF-UHFFFAOYSA-M 0.000 description 2
238000001179 sorption measurement Methods 0.000 description 2
238000012546 transfer Methods 0.000 description 2
WCWOEQFAYSXBRK-RWOPYEJCSA-N (2r,3s,4s,5s,6r)-2-amino-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound N[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@@H]1O WCWOEQFAYSXBRK-RWOPYEJCSA-N 0.000 description 1
UTVXFQMLZSPQLB-JFNONXLTSA-N (3R,4R,5R,6S)-2-amino-6-methyloxane-3,4,5-triol Chemical compound C1([C@H](O)[C@H](O)[C@@H](O)[C@@H](O1)C)N UTVXFQMLZSPQLB-JFNONXLTSA-N 0.000 description 1
UUSMORJRYZFLSS-SOOFDHNKSA-N (3r,4s,5r)-2-amino-5-(hydroxymethyl)oxolane-3,4-diol Chemical compound NC1O[C@H](CO)[C@@H](O)[C@H]1O UUSMORJRYZFLSS-SOOFDHNKSA-N 0.000 description 1
RQBSUMJKSOSGJJ-IOVATXLUSA-N (3r,4s,5r)-2-aminooxane-3,4,5-triol Chemical compound NC1OC[C@@H](O)[C@H](O)[C@H]1O RQBSUMJKSOSGJJ-IOVATXLUSA-N 0.000 description 1
UTVXFQMLZSPQLB-DHVFOXMCSA-N (3s,4r,5s,6s)-2-amino-6-methyloxane-3,4,5-triol Chemical compound C[C@@H]1OC(N)[C@@H](O)[C@H](O)[C@@H]1O UTVXFQMLZSPQLB-DHVFOXMCSA-N 0.000 description 1
238000003691 Amadori rearrangement reaction Methods 0.000 description 1
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
101100204059 Caenorhabditis elegans trap-2 gene Proteins 0.000 description 1
VOPWNXZWBYDODV-UHFFFAOYSA-N Chlorodifluoromethane Chemical compound FC(F)Cl VOPWNXZWBYDODV-UHFFFAOYSA-N 0.000 description 1
KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
RQBSUMJKSOSGJJ-AGQMPKSLSA-N D-lyxosylamine Chemical compound NC1OC[C@@H](O)[C@H](O)[C@@H]1O RQBSUMJKSOSGJJ-AGQMPKSLSA-N 0.000 description 1
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
239000004341 Octafluorocyclobutane Substances 0.000 description 1
PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 description 1
241000212342 Sium Species 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
239000000654 additive Substances 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
125000003275 alpha amino acid group Chemical group 0.000 description 1
238000009530 blood pressure measurement Methods 0.000 description 1
RJCQBQGAPKAMLL-UHFFFAOYSA-N bromotrifluoromethane Chemical compound FC(F)(F)Br RJCQBQGAPKAMLL-UHFFFAOYSA-N 0.000 description 1
239000001273 butane Substances 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
235000019504 cigarettes Nutrition 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
238000000576 coating method Methods 0.000 description 1
235000009508 confectionery Nutrition 0.000 description 1
239000000470 constituent Substances 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
238000006731 degradation reaction Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
235000019441 ethanol Nutrition 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
238000005243 fluidization Methods 0.000 description 1
239000000727 fraction Substances 0.000 description 1
239000007789 gas Substances 0.000 description 1
239000007792 gaseous phase Substances 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
150000002431 hydrogen Chemical class 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
CBOIHMRHGLHBPB-UHFFFAOYSA-N hydroxymethyl Chemical group O[CH2] CBOIHMRHGLHBPB-UHFFFAOYSA-N 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
239000006225 natural substrate Substances 0.000 description 1
238000009828 non-uniform distribution Methods 0.000 description 1
BCCOBQSFUDVTJQ-UHFFFAOYSA-N octafluorocyclobutane Chemical compound FC1(F)C(F)(F)C(F)(F)C1(F)F BCCOBQSFUDVTJQ-UHFFFAOYSA-N 0.000 description 1
235000019407 octafluorocyclobutane Nutrition 0.000 description 1
230000009965 odorless effect Effects 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
239000002245 particle Substances 0.000 description 1
125000006340 pentafluoro ethyl group Chemical group FC(F)(F)C(F)(F)* 0.000 description 1
239000012071 phase Substances 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
239000001294 propane Substances 0.000 description 1
238000000197 pyrolysis Methods 0.000 description 1
230000003134 recirculating effect Effects 0.000 description 1
238000004064 recycling Methods 0.000 description 1
238000005070 sampling Methods 0.000 description 1
238000012216 screening Methods 0.000 description 1
238000007086 side reaction Methods 0.000 description 1
238000002791 soaking Methods 0.000 description 1
235000015424 sodium Nutrition 0.000 description 1
239000011343 solid material Substances 0.000 description 1
238000005507 spraying Methods 0.000 description 1
238000000194 supercritical-fluid extraction Methods 0.000 description 1
238000012360 testing method Methods 0.000 description 1
229940086542 triethylamine Drugs 0.000 description 1
125000002023 trifluoromethyl group Chemical group FC(F)(F)* 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
General Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Manufacture Of Tobacco Products (AREA)
Extraction Or Liquid Replacement (AREA)
Fire-Extinguishing Compositions (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Fertilizers (AREA)
Protection Of Pipes Against Damage, Friction, And Corrosion (AREA)
Laminated Bodies (AREA)
Control Of El Displays (AREA)
Superconductors And Manufacturing Methods Therefor (AREA)
Medicines Containing Material From Animals Or Micro-Organisms (AREA)

CA000555304A 1986-12-29 1987-12-23 Methode d'extraction au solvent des matieres essentielles contenues dans les plants Expired - Fee Related CA1317961C (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US94710286A	1986-12-29	1986-12-29
US947,102		1986-12-29

Publications (1)

Publication Number	Publication Date
CA1317961C true CA1317961C (fr)	1993-05-18

Family

ID=25485521

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000555304A Expired - Fee Related CA1317961C (fr)	1986-12-29	1987-12-23	Methode d'extraction au solvent des matieres essentielles contenues dans les plants

Country Status (9)

Country	Link
EP (1)	EP0280817B1 (fr)
JP (1)	JP2694253B2 (fr)
AT (1)	ATE102446T1 (fr)
AU (1)	AU612128B2 (fr)
BR (1)	BR8707110A (fr)
CA (1)	CA1317961C (fr)
DE (1)	DE3789300D1 (fr)
FI (1)	FI88453C (fr)
ZA (1)	ZA879384B (fr)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5497792A (en) *	1987-11-19	1996-03-12	Philip Morris Incorporated	Process and apparatus for the semicontinuous extraction of nicotine from tobacco
US5435325A (en) *	1988-04-21	1995-07-25	R. J. Reynolds Tobacco Company	Process for providing tobacco extracts using a solvent in a supercritical state
US4967771A (en) *	1988-12-07	1990-11-06	R. J. Reynolds Tobacco Company	Process for extracting tobacco
US5076293A (en) *	1989-06-19	1991-12-31	R. J. Reynolds Tobacco Company	Process and apparatus for the treatment of tobacco material
US5031644A (en) *	1989-12-29	1991-07-16	R. J. Reynolds Tobacco Company	Tobacco expansion process and product
US5025812A (en) *	1989-08-10	1991-06-25	R. J. Reynolds Tobacco Company	Tobacco processing
DE4002784C1 (fr) *	1990-01-31	1991-04-18	B.A.T. Cigarettenfabriken Gmbh, 2000 Hamburg, De
US5065775A (en) *	1990-02-23	1991-11-19	R. J. Reynolds Tobacco Company	Tobacco processing
US5131414A (en) *	1990-02-23	1992-07-21	R. J. Reynolds Tobacco Company	Tobacco processing
US5234008A (en) *	1990-02-23	1993-08-10	R. J. Reynolds Tobacco Company	Tobacco processing
US5095923A (en) *	1991-04-11	1992-03-17	R. J. Reynolds Tobacco Company	Tobacco expansion process using 1,1,1,2-tetrafluoroethane
DE19654945C2 (de) *	1996-07-29	1998-05-20	Mueller Extract Co Gmbh	Im wesentlichen nikotinfreies Tabakaromaöl sowie Verfahren zu dessen Herstellung
DE19630619C2 (de) *	1996-07-29	1998-07-09	Mueller Extract Co Gmbh	Im wesentlichen nikotinfreies Tabakaromaöl sowie Verfahren zu dessen Herstellung
CN100334979C (zh)	2002-07-18	2007-09-05	法塞克斯公司	减少烟草中成分的方法及通过该方法得到的烟草
CN100540104C (zh) *	2004-10-28	2009-09-16	日本烟草产业株式会社	从被处理材料中抽提成分的方法以及该方法中使用的装置
RU2332915C1 (ru) *	2007-02-27	2008-09-10	Олег Иванович Квасенков	Установка для производства мешки легкого кретека
GB201003887D0 (en)	2010-03-09	2010-05-12	British American Tobacco Co	Methods for extracting and isolating constituents of cellulosic material
US10405571B2 (en)	2015-06-26	2019-09-10	Altria Client Services Llc	Compositions and methods for producing tobacco plants and products having altered alkaloid levels
GB201707758D0 (en)	2017-05-15	2017-06-28	British American Tobacco Investments Ltd	Ground tobacco composition
GB201707761D0 (en) *	2017-05-15	2017-06-28	British American Tobacco Investments Ltd	Method of making a tobacco extract
GB201707767D0 (en)	2017-05-15	2017-06-28	British American Tobacco Investments Ltd	Method of making a tobacco extract
GB201707759D0 (en)	2017-05-15	2017-06-28	British American Tobacco Investments Ltd	Method of making a tobacco extract
WO2019229704A1 (fr) *	2018-05-31	2019-12-05	Radient Technologies Inc.	Procédé permettant de réduire la nicotine dans une biomasse de tabac et composition de tabac
CN113115976B (zh) *	2021-03-11	2022-07-19	浙江中烟工业有限责任公司	一种烟碱盐的批量制备方法及其在电子烟中的应用
CN114868763B (zh) *	2022-05-13	2024-06-11	湖南省烟草公司郴州市公司	一种烟草降碱剂及其制备方法和应用

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FR397021A (fr) *	1907-12-11	1909-04-27	Tabacs Desintoxiques En Failli	Procédé et installation pour la dénicotinisation des tabacs
US2227863A (en) *	1938-02-14	1941-01-07	Kinetic Chemicals Inc	Extraction of tobacco with fluorochlorohydrocarbons
DE1517273B2 (de) *	1965-04-15	1976-06-24	Eresta Warenhandelsgesellschaft mbH, 6052 Mühlheim	Verfahren zur kontinuierlichen extraktion von nicotin aus tabak und zur gewinnung vorkonzentrierter nicotinsalzloesungen
US4153063A (en) *	1970-09-02	1979-05-08	Studiengesellschaft Kohle Mbh	Process for the extraction of nicotine from tobacco
US4215706A (en) *	1978-10-13	1980-08-05	Loew's Theatres, Inc.	Nicotine transfer process
US5497792A (en) *	1987-11-19	1996-03-12	Philip Morris Incorporated	Process and apparatus for the semicontinuous extraction of nicotine from tobacco

1987
- 1987-12-14 ZA ZA879384A patent/ZA879384B/xx unknown
- 1987-12-22 FI FI875673A patent/FI88453C/fi not_active IP Right Cessation
- 1987-12-23 CA CA000555304A patent/CA1317961C/fr not_active Expired - Fee Related
- 1987-12-24 EP EP87311430A patent/EP0280817B1/fr not_active Revoked
- 1987-12-24 DE DE87311430T patent/DE3789300D1/de not_active Expired - Lifetime
- 1987-12-24 AT AT87311430T patent/ATE102446T1/de not_active IP Right Cessation
- 1987-12-28 JP JP62336696A patent/JP2694253B2/ja not_active Expired - Fee Related
- 1987-12-29 AU AU83109/87A patent/AU612128B2/en not_active Ceased
- 1987-12-29 BR BR8707110A patent/BR8707110A/pt not_active IP Right Cessation

Also Published As

Publication number	Publication date
ZA879384B (en)	1988-09-28
EP0280817B1 (fr)	1994-03-09
FI88453B (fi)	1993-02-15
EP0280817A3 (en)	1990-05-16
JP2694253B2 (ja)	1997-12-24
EP0280817A2 (fr)	1988-09-07
AU612128B2 (en)	1991-07-04
DE3789300D1 (de)	1994-04-14
FI875673A0 (fi)	1987-12-22
FI88453C (fi)	1993-05-25
JPS63229102A (ja)	1988-09-26
ATE102446T1 (de)	1994-03-15
AU8310987A (en)	1988-06-30
BR8707110A (pt)	1988-08-02
FI875673L (fi)	1988-06-30

Legal Events

Date	Code	Title	Description
2008-05-20	MKLA	Lapsed

Publication	Publication Date	Title
CA1317961C (fr)	1993-05-18	Methode d'extraction au solvent des matieres essentielles contenues dans les plants
US5018540A (en)	1991-05-28	Process for removal of basic materials
US5810020A (en)	1998-09-22	Process for removing nitrogen-containing anions and tobacco-specific nitrosamines from tobacco products
US4986286A (en)	1991-01-22	Tobacco treatment process
US5435325A (en)	1995-07-25	Process for providing tobacco extracts using a solvent in a supercritical state
US4366823A (en)	1983-01-04	Process for expanding tobacco
US5025812A (en)	1991-06-25	Tobacco processing
US4366824A (en)	1983-01-04	Process for expanding tobacco
US4153063A (en)	1979-05-08	Process for the extraction of nicotine from tobacco
JP2709400B2 (ja)	1998-02-04	煙草からニコチンを半連続的に抽出する方法及び装置
CA2614730C (fr)	2013-12-24	Extraction et stockage de constituants du tabac
US5099862A (en)	1992-03-31	Tobacco extraction process
US5148819A (en)	1992-09-22	Process for extracting tobacco
FI83019C (fi)	1991-05-27	Foerfarande foer tillsaettande av aromaemnen i tobak.
US4168324A (en)	1979-09-18	Process of extracting stimulants from coffee
HUT66688A (en)	1994-12-28	Process for treating of tobacco in particular for change of character of tobacco material
US4827949A (en)	1989-05-09	Method of treating tobacco and tobacco produced thereby
EP0153817A2 (fr)	1985-09-04	Procédé pour modifier les caractéristiques aromatiques du tabac
US4243056A (en)	1981-01-06	Method for uniform incorporation of additives into tobacco
CA1115617A (fr)	1982-01-05	Methode et dispositif de gonflement des produits du tabac
US5095922A (en)	1992-03-17	Process for increasing the filling power of tobacco material
AU2013239232A1 (en)	2014-10-16	Liquid tobacco compositions
US4628947A (en)	1986-12-16	Process for modifying the flavor characteristics of bright tobacco
US3110315A (en)	1963-11-12	Denicotinization of tobacco
WO2014080229A1 (fr)	2014-05-30	Traitement de matériau de tabac