CA2025746A1 - Procede de recuperation d'alcools epoxydes non hydrosolubles - Google Patents

Procede de recuperation d'alcools epoxydes non hydrosolubles

Info

Publication number: CA2025746A1
Authority: CA; Canada
Prior art keywords: water; alcohol; recovery; epoxy alcohol; epoxy
Prior art date: 1989-10-13
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

CA2025746A

Other languages

English (en)

Other versions

CA2025746C (fr

Inventor

Wilfred Pro-Sum Shum

Christopher J. Sowa

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Lyondell Chemical Technology LP

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-10-13

Filing date

1990-09-19

Publication date

1991-04-14

1990-09-19 Application filed by Individual filed Critical Individual

1991-04-14 Publication of CA2025746A1 publication Critical patent/CA2025746A1/fr

2001-02-06 Application granted granted Critical

2001-02-06 Publication of CA2025746C publication Critical patent/CA2025746C/fr

2010-09-19 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

JSPLKZUTYZBBKA-UHFFFAOYSA-N trioxidane Chemical compound OOO JSPLKZUTYZBBKA-UHFFFAOYSA-N 0.000 title abstract 3
238000000034 method Methods 0.000 title 1
238000011084 recovery Methods 0.000 title 1
239000000203 mixture Substances 0.000 abstract 2
239000004593 Epoxy Substances 0.000 abstract 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 1
ZDPVRXUQQGZTEY-SECBINFHSA-N [(2R)-2-phenyloxiran-2-yl]methanol Chemical compound C=1C=CC=CC=1[C@@]1(CO)CO1 ZDPVRXUQQGZTEY-SECBINFHSA-N 0.000 abstract 1
150000001298 alcohols Chemical class 0.000 abstract 1
238000000354 decomposition reaction Methods 0.000 abstract 1
238000004821 distillation Methods 0.000 abstract 1
238000006735 epoxidation reaction Methods 0.000 abstract 1
239000011541 reaction mixture Substances 0.000 abstract 1
238000005406 washing Methods 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/14—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by free hydroxyl radicals
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/16—Vacuum
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/23—Cooling

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Epoxy Compounds (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

CA002025746A 1989-10-13 1990-09-19 Procede de recuperation d'alcools epoxydes non hydrosolubles Expired - Fee Related CA2025746C (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US07/420,859 US4935101A (en)	1989-10-13	1989-10-13	Process for the recovery of a water-insoluble epoxy alcohol
US07/420,859		1989-10-13

Publications (2)

Publication Number	Publication Date
CA2025746A1 true CA2025746A1 (fr)	1991-04-14
CA2025746C CA2025746C (fr)	2001-02-06

Family

ID=23668130

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA002025746A Expired - Fee Related CA2025746C (fr)	1989-10-13	1990-09-19	Procede de recuperation d'alcools epoxydes non hydrosolubles

Country Status (9)

Country	Link
US (1)	US4935101A (fr)
EP (1)	EP0422897B1 (fr)
JP (1)	JP2952611B2 (fr)
KR (1)	KR0153254B1 (fr)
CA (1)	CA2025746C (fr)
DE (1)	DE69010136T2 (fr)
DK (1)	DK0422897T3 (fr)
ES (1)	ES2055338T3 (fr)
MX (1)	MX164038B (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4935101A (en) *	1989-10-13	1990-06-19	Arco Chemical Technology, Inc.	Process for the recovery of a water-insoluble epoxy alcohol
US5360811A (en) *	1990-03-13	1994-11-01	Hoechst-Roussel Pharmaceuticals Incorporated	1-alkyl-, 1-alkenyl-, and 1-alkynylaryl-2-amino-1,3-propanediols and related compounds as anti-inflammatory agents
US5834570A (en) *	1993-06-08	1998-11-10	Nippon Steel Chemical Co., Ltd.	Epoxy resin composition
KR100427458B1 (ko) *	2001-04-24	2004-04-27	동남합성공업 주식회사	젤 형태의 부산물을 포함하는 알콕시화 반응 생성물로부터액체 알콕시화 반응생성물의 효율적 분리방법
CN103827161B (zh) *	2011-09-27	2016-11-23	蓝立方知识产权有限责任公司	用于使环氧树脂环氧化的往复震动板式塔反应器

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2838524A (en) *	1955-09-20	1958-06-10	Du Pont	Epoxidation process
NL300753A (fr) *	1962-11-20
BE666663A (fr) *	1964-07-10
US3954815A (en) *	1966-01-11	1976-05-04	Fmc Corporation	Glycidol and glycerol process
US3374153A (en) *	1966-07-25	1968-03-19	Halcon International Inc	Process for recovery of glycidol from alcohol by azeotropic distillation with a hydrocarbon
US3452055A (en) *	1966-07-29	1969-06-24	Halcon International Inc	Process for the recovery of epoxides wherein alkylaromatic compound is removed in two distillation zones
US3509183A (en) *	1967-07-17	1970-04-28	Fmc Corp	Process for epoxidation of allyl alcohol by peracetic acid
US3655524A (en) *	1970-04-27	1972-04-11	Fmc Corp	Glycidol isolation by azeotropic distillation with a lower-boiling entrainer
US3849451A (en) *	1970-06-30	1974-11-19	Halcon International Inc	Epoxidation process
JPS5752341B2 (fr) *	1972-12-27	1982-11-06
SU480695A2 (ru) *	1973-07-06	1975-08-15	Ярославский Технологический Институт	Способ совместного получени глицидола и олефиновых углеводородов
US3988353A (en) *	1974-04-04	1976-10-26	Oxirane Corporation	Preferential removal of metallic catalyst from epoxidation effluent
DE2916572A1 (de) *	1979-04-24	1980-11-13	Peroxid Chemie Gmbh	Verfahren zur destillativen trennung von tert.-alkylhydroperoxiden und di- tert.-alkylperoxiden
US4471130A (en) *	1980-08-06	1984-09-11	The Board Of Trustees Of The Leland Stanford Junior University	Method for asymmetric epoxidation
US4594439A (en) *	1980-08-06	1986-06-10	The Board Of Trustees Of The Leland Stanford Jr. University	Method for asymmetric epoxidation
JPS59167579A (ja) *	1983-03-14	1984-09-21	Mitsui Toatsu Chem Inc	グリシド−ルの精製法
IL78187A (en) *	1985-04-04	1991-05-12	Massachusetts Inst Technology	Catalytic asymmetric epoxidation
JP2686975B2 (ja) *	1987-09-14	1997-12-08	アルコ・ケミカル・カンパニー	不斉エポキシン化法におけるキラルエポキシアルコールの採取法
US4935101A (en) *	1989-10-13	1990-06-19	Arco Chemical Technology, Inc.	Process for the recovery of a water-insoluble epoxy alcohol

1989
- 1989-10-13 US US07/420,859 patent/US4935101A/en not_active Expired - Fee Related
1990
- 1990-09-19 CA CA002025746A patent/CA2025746C/fr not_active Expired - Fee Related
- 1990-10-09 DE DE69010136T patent/DE69010136T2/de not_active Expired - Fee Related
- 1990-10-09 EP EP90311053A patent/EP0422897B1/fr not_active Expired - Lifetime
- 1990-10-09 ES ES90311053T patent/ES2055338T3/es not_active Expired - Lifetime
- 1990-10-09 DK DK90311053.4T patent/DK0422897T3/da active
- 1990-10-10 MX MX22765A patent/MX164038B/es unknown
- 1990-10-12 JP JP2272499A patent/JP2952611B2/ja not_active Expired - Lifetime
- 1990-10-13 KR KR1019900016362A patent/KR0153254B1/ko not_active Expired - Fee Related

Also Published As

Publication number	Publication date
DE69010136T2 (de)	1994-10-13
JP2952611B2 (ja)	1999-09-27
KR910007903A (ko)	1991-05-30
JPH03133972A (ja)	1991-06-07
EP0422897A3 (en)	1991-10-23
ES2055338T3 (es)	1994-08-16
EP0422897B1 (fr)	1994-06-22
DK0422897T3 (da)	1994-07-25
MX164038B (es)	1992-07-10
DE69010136D1 (de)	1994-07-28
US4935101A (en)	1990-06-19
CA2025746C (fr)	2001-02-06
KR0153254B1 (ko)	1998-11-16
EP0422897A2 (fr)	1991-04-17

Legal Events

Date	Code	Title	Description
1997-09-12	EEER	Examination request
2003-09-19	MKLA	Lapsed
2023-05-26	MKLA	Lapsed	Effective date: 20030919

Publication	Publication Date	Title
CA2300083A1 (fr)	1999-02-18	Purification d'oxyde de propylene
ES2149880T3 (es)	2000-11-16	Sintesis de peptidos ciclicos.
GB1519872A (en)	1978-08-02	Process for distillation and purification of a crude alcoh/l containing mixture
EP0340324A3 (en)	1990-06-13	Process for the preparation of pure dimethyl ether
Marino et al.	1979	Regioselective reactions of organocuprates with cycloalkene epoxides
ATE119893T1 (de)	1995-04-15	Herstellung von monoepoxiden.
US3374153A (en)	1968-03-19	Process for recovery of glycidol from alcohol by azeotropic distillation with a hydrocarbon
US4012424A (en)	1977-03-15	Cracking of mixtures containing hydroxyesters
EP0056932B1 (fr)	1984-09-19	Procédé de préparation et d'isolement de n-alkyloxirannes
US4379025A (en)	1983-04-05	Water removal from butylene oxides by liquid extraction with selected extractive solvents
JPS57185287A (en)	1982-11-15	Purification of bis(alkylbenzylidene)sorbitol
EP0306614A3 (en)	1989-11-15	Improvements of processes and plants for the production of urea
ES2055338T3 (es)	1994-08-16	Recuperacion de alcoholes epoxidicos insolubles en agua.
US4855465A (en)	1989-08-08	Process for the treatment of aliphatic epoxides
US3661938A (en)	1972-05-09	Process for the preparation of glycidyl esters
US4036890A (en)	1977-07-19	Preparation of organic hydroperoxides
GB1495481A (en)	1977-12-21	Process for the obtaining of isobutylene of high purity
JPS5785387A (en)	1982-05-28	Preparation of 1-(-5'-oxohexyl)-3,7-dimethylxanthine
SE322764B (fr)	1970-04-20
JPS54145604A (en)	1979-11-14	Preparation of diols
JPS6485940A (en)	1989-03-30	Production of allyl alcohol
SU602501A1 (ru)	1978-04-15	Саособ получени винилоксиэтилового эфира глицидола
SU763314A1 (ru)	1980-09-15	Способ переработки т желого остатка процесса эпоксидировани пропилена гидроперекисью этилбензола в стирол
JPS5679657A (en)	1981-06-30	Novel preparation of polyisocyanate
SU499798A4 (ru)	1976-01-15	Способ получени -формилоксиалканалей