CA2688091C - Composition lubrifiante contenant du soufre, du phosphore et un agent anti-usure sans cendres et agent de modification du frottement contenant une aminene - Google Patents

Composition lubrifiante contenant du soufre, du phosphore et un agent anti-usure sans cendres et agent de modification du frottement contenant une aminene Download PDF

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Publication number
CA2688091C
CA2688091C CA2688091A CA2688091A CA2688091C CA 2688091 C CA2688091 C CA 2688091C CA 2688091 A CA2688091 A CA 2688091A CA 2688091 A CA2688091 A CA 2688091A CA 2688091 C CA2688091 C CA 2688091C
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CA
Canada
Prior art keywords
lubricating composition
amine
lubricating
antiwear agent
friction modifier
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2688091A
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English (en)
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CA2688091A1 (fr
Inventor
Jody Kocsis
Patrick E. Mosier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lubrizol Corp
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Lubrizol Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lubrizol Corp filed Critical Lubrizol Corp
Publication of CA2688091A1 publication Critical patent/CA2688091A1/fr
Application granted granted Critical
Publication of CA2688091C publication Critical patent/CA2688091C/fr
Active legal-status Critical Current
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M141/00—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential
    • C10M141/06—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential at least one of them being an organic nitrogen-containing compound
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/028—Overbased salts thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/26—Overbased carboxylic acid salts
    • C10M2207/262—Overbased carboxylic acid salts derived from hydroxy substituted aromatic acids, e.g. salicylates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/282—Esters of (cyclo)aliphatic oolycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/287—Partial esters
    • C10M2207/288—Partial esters containing free carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/287—Partial esters
    • C10M2207/289—Partial esters containing free hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
    • C10M2215/08—Amides [having hydrocarbon substituents containing less than thirty carbon atoms]
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
    • C10M2215/08—Amides [having hydrocarbon substituents containing less than thirty carbon atoms]
    • C10M2215/082—Amides [having hydrocarbon substituents containing less than thirty carbon atoms] containing hydroxyl groups; Alkoxylated derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
    • C10M2215/086—Imides [having hydrocarbon substituents containing less than thirty carbon atoms]
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions
    • C10M2215/24—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant Compositions having hydrocarbon substituents containing thirty or more carbon atoms, e.g. nitrogen derivatives of substituted succinic acid
    • C10M2215/28—Amides; Imides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/046—Overbased sulfonic acid salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/045—Metal containing thio derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02—Pour-point; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/40—Low content or no content compositions
    • C10N2030/42—Phosphor free or low phosphor content compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/40—Low content or no content compositions
    • C10N2030/43—Sulfur free or low sulfur content compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/40—Low content or no content compositions
    • C10N2030/45—Ash-less or low ash content
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/54—Fuel economy
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/25—Internal-combustion engines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

L'invention concerne une composition lubrifiante contenant une huile présentant une viscosité de lubrification, un agent de modification du frottement contenant une amine et un agent anti-usure sans cendres. La composition lubrifiante est appropriée pour lubrifier un moteur à combustion interne.
CA2688091A 2007-05-24 2008-05-15 Composition lubrifiante contenant du soufre, du phosphore et un agent anti-usure sans cendres et agent de modification du frottement contenant une aminene Active CA2688091C (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US93995207P 2007-05-24 2007-05-24
US60/939,952 2007-05-24
PCT/US2008/063653 WO2008147700A1 (fr) 2007-05-24 2008-05-15 Composition lubrifiante contenant du soufre, du phosphore et un agent anti-usure sans cendres et un agent de modification du frottement contenant une amine

Publications (2)

Publication Number Publication Date
CA2688091A1 CA2688091A1 (fr) 2008-12-04
CA2688091C true CA2688091C (fr) 2015-04-14

Family

ID=39595597

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2688091A Active CA2688091C (fr) 2007-05-24 2008-05-15 Composition lubrifiante contenant du soufre, du phosphore et un agent anti-usure sans cendres et agent de modification du frottement contenant une aminene

Country Status (5)

Country Link
US (1) US20100093573A1 (fr)
EP (1) EP2160453B1 (fr)
JP (1) JP2010528154A (fr)
CA (1) CA2688091C (fr)
WO (1) WO2008147700A1 (fr)

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CN102272275B (zh) 2008-11-05 2015-02-04 卢布里佐尔公司 润滑内燃机的方法
CN101945981A (zh) * 2008-12-05 2011-01-12 卢布里佐尔公司 用于改进的燃料效率的船用柴油机气缸润滑剂
US20120172265A1 (en) * 2008-12-09 2012-07-05 The Lubrizol Corporation Lubricating Composition Containing a Compound Derived from a Hydroxy-carboxylic Acid
JP5480259B2 (ja) * 2009-03-10 2014-04-23 ザ ルブリゾル コーポレイション 動力伝達系路デバイスを潤滑する、耐摩耗組成物および方法
CA2764436C (fr) 2009-06-04 2018-08-14 The Lubrizol Corporation Polymethacrylates comme modificateurs de viscosite a iv eleve
CN102459542B (zh) 2009-06-04 2013-12-11 卢布里佐尔公司 含摩擦改进剂和粘度改进剂的润滑组合物
US20130324448A1 (en) 2012-05-08 2013-12-05 The Lubrizol Corporation Antiwear Composition and Method of Lubricating Driveline Device
ES2453146T3 (es) 2009-08-18 2014-04-04 The Lubrizol Corporation Composición lubricante que contiene un agente antidesgaste
KR20120090042A (ko) * 2009-08-18 2012-08-16 더루우브리졸코오포레이션 내마모 조성물 및 동력전달장치를 윤활처리하는 방법
CN102549125B (zh) * 2009-10-09 2014-09-24 国际壳牌研究有限公司 润滑组合物
US9528067B2 (en) 2009-11-30 2016-12-27 The Lubrizol Corporation Stabilized blends containing friction modifiers
US20120309657A1 (en) 2009-12-14 2012-12-06 The Lubrizol Corporation Lubricating Composition Containing an Antiwear Agent
EP2545148B1 (fr) 2010-03-10 2019-08-14 The Lubrizol Corporation Composés et complexes de titane et molybdène utilisés comme additifs dans des lubrifiants
JP5512344B2 (ja) * 2010-03-23 2014-06-04 株式会社Ａｄｅｋａ 内燃機関用潤滑油組成物
WO2011161406A1 (fr) * 2010-06-25 2011-12-29 Castrol Limited Utilisations et compositions
US9090846B2 (en) 2010-08-31 2015-07-28 The Lubrizol Corporation Lubricating composition containing an antiwear agent
EP2633009B1 (fr) 2010-10-26 2016-04-06 Castrol Limited Compositions de carburant et de lubrifiant non aqueuses comprenant des esters d'acides gras d'acides hydroxycarboxyliques et leurs utilisations
WO2012087773A1 (fr) 2010-12-21 2012-06-28 The Lubrizol Corporation Composition lubrifiante contenant un agent anti-usure
JP2014500387A (ja) 2010-12-21 2014-01-09 ザ ルブリゾル コーポレイション 清浄剤を含む潤滑組成物
JP6034807B2 (ja) 2011-02-16 2016-11-30 ザ ルブリゾル コーポレイションＴｈｅ Ｌｕｂｒｉｚｏｌ Ｃｏｒｐｏｒａｔｉｏｎ 潤滑組成物およびドライブライン装置を潤滑する方法
US10590363B2 (en) 2011-10-31 2020-03-17 Daniel J. Saccomando Ashless-friction modifiers for lubricating compositions
US9321979B2 (en) * 2012-03-13 2016-04-26 Chemtura Corporation Friction modifier composition for lubricants
US10072230B2 (en) * 2012-05-23 2018-09-11 Chemtura Corporation Method for reducing engine wear with lubricants comprising 2-hydroxyalkylamide friction modifying/anti-wear compositions
WO2013189674A1 (fr) 2012-06-20 2013-12-27 Castrol Limited Modificateur de frottement et son utilisation dans des lubrifiants et des carburants
CN104685042B (zh) 2012-06-20 2017-05-24 卡斯特罗尔有限公司 摩擦改性剂及其在润滑剂和燃料中的用途
US20140187455A1 (en) * 2012-12-28 2014-07-03 Chevron Oronite LLC Ultra-low saps lubricants for internal combustion engines
EP3004297A2 (fr) * 2013-05-30 2016-04-13 The Lubrizol Corporation Compositions synergiques d'additifs pour des huiles d'engrenages industrielles
CN104419499A (zh) * 2013-08-30 2015-03-18 中国石油天然气股份有限公司 一种具有极性两端的螺旋高分子摩擦改进剂
JP6776495B2 (ja) * 2015-03-20 2020-10-28 出光興産株式会社 潤滑油組成物
US9879198B2 (en) * 2015-11-25 2018-01-30 Santolubes Llc Low shear strength lubricating fluids
CA3021039A1 (fr) 2016-04-20 2017-10-26 The Lubrizol Corporation Lubrifiant pour moteurs a deux temps
EP3487968B1 (fr) 2016-07-22 2020-10-21 The Lubrizol Corporation Composés de borate tétraédrique destinés à des compositions lubrifiantes à formulation complète
US20200032158A1 (en) * 2018-07-24 2020-01-30 Exxonmobil Research And Engineering Company Lubricating oil compositions with engine corrosion protection
EP3940046B1 (fr) * 2019-03-14 2025-04-16 NOF Corporation Additif pour huile lubrifiante, composition d'additif pour huile lubrifiante et préparation d'une composition d'huile lubrifiante les contenant
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US7696136B2 (en) 2004-03-11 2010-04-13 Crompton Corporation Lubricant compositions containing hydroxy carboxylic acid and hydroxy polycarboxylic acid esters
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US7651987B2 (en) 2004-10-12 2010-01-26 The Lubrizol Corporation Tartaric acid derivatives as fuel economy improvers and antiwear agents in crankcase oils and preparation thereof

Also Published As

Publication number Publication date
CA2688091A1 (fr) 2008-12-04
EP2160453B1 (fr) 2012-07-11
EP2160453A1 (fr) 2010-03-10
US20100093573A1 (en) 2010-04-15
WO2008147700A1 (fr) 2008-12-04
JP2010528154A (ja) 2010-08-19

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