CA2860614C - Recovering lead from a mixed oxidized material - Google Patents
Recovering lead from a mixed oxidized material Download PDFInfo
- Publication number
- CA2860614C CA2860614C CA2860614A CA2860614A CA2860614C CA 2860614 C CA2860614 C CA 2860614C CA 2860614 A CA2860614 A CA 2860614A CA 2860614 A CA2860614 A CA 2860614A CA 2860614 C CA2860614 C CA 2860614C
- Authority
- CA
- Canada
- Prior art keywords
- lead
- mixed oxidized
- liquid leachate
- sulfonic acid
- leachate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
- C25C1/18—Electrolytic production, recovery or refining of metals by electrolysis of solutions of lead
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B13/00—Obtaining lead
- C22B13/04—Obtaining lead by wet processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B13/00—Obtaining lead
- C22B13/04—Obtaining lead by wet processes
- C22B13/045—Recovery from waste materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Electrolytic Production Of Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261725824P | 2012-11-13 | 2012-11-13 | |
| US61/725,824 | 2012-11-13 | ||
| PCT/IB2013/002540 WO2014076547A1 (en) | 2012-11-13 | 2013-11-13 | Recovering lead from a mixed oxidized material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2860614A1 CA2860614A1 (en) | 2014-05-22 |
| CA2860614C true CA2860614C (en) | 2020-10-27 |
Family
ID=49880838
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2860614A Active CA2860614C (en) | 2012-11-13 | 2013-11-13 | Recovering lead from a mixed oxidized material |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9322104B2 (2) |
| EP (1) | EP2920330B1 (2) |
| JP (1) | JP6356137B2 (2) |
| CN (1) | CN104039991B (2) |
| AU (1) | AU2013346480B2 (2) |
| CA (1) | CA2860614C (2) |
| ES (1) | ES2657632T3 (2) |
| MX (1) | MX364711B (2) |
| PL (1) | PL2920330T3 (2) |
| PT (1) | PT2920330T (2) |
| RS (1) | RS56991B1 (2) |
| WO (1) | WO2014076547A1 (2) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101739414B1 (ko) | 2013-11-19 | 2017-05-24 | 아쿠아 메탈스 인크. | 리드 액시드 배터리들의 제련소 없는 재활용을 위한 장치 및 방법 |
| CA2968064C (en) * | 2013-11-19 | 2021-08-03 | Aqua Metals Inc. | Improved devices and method for smelterless recycling of lead acid batteries |
| US9670565B2 (en) | 2014-06-20 | 2017-06-06 | Johnson Controls Technology Company | Systems and methods for the hydrometallurgical recovery of lead from spent lead-acid batteries and the preparation of lead oxide for use in new lead-acid batteries |
| US9708689B2 (en) * | 2015-04-08 | 2017-07-18 | Honeywell International Inc. | Isotope displacement refining process for producing low alpha materials |
| JP6805240B2 (ja) | 2015-05-13 | 2020-12-23 | アクア メタルズ インコーポレーテッドAqua Metals Inc. | 鉛酸電池からの鉛の回収のためのシステムおよび方法 |
| EP3294931A4 (en) * | 2015-05-13 | 2018-12-26 | Aqua Metals Inc. | Electrodeposited lead composition, methods of production, and uses |
| KR102242697B1 (ko) | 2015-05-13 | 2021-04-20 | 아쿠아 메탈스 인크. | 납 축전지를 재활용 하기 위한 폐 루프 시스템들 및 방법들 |
| CN106676578B (zh) * | 2015-11-11 | 2018-09-28 | 沈阳有色金属研究院 | 一种锌电积新型高效联合添加剂 |
| US10316420B2 (en) | 2015-12-02 | 2019-06-11 | Aqua Metals Inc. | Systems and methods for continuous alkaline lead acid battery recycling |
| CN106498446A (zh) * | 2016-10-20 | 2017-03-15 | 北京矿冶研究总院 | 一种硫酸铅悬浮电解的方法 |
| CN106756008B (zh) * | 2017-02-22 | 2018-08-14 | 中南大学 | 磺酸溶液两段逆流常压氧化浸出硫化铅精矿中铅的方法 |
| CN107227408B (zh) * | 2017-04-28 | 2019-01-04 | 昆明理工大学 | 一种硅质硫化铅精矿的低温常压快速浸出方法 |
| US12077834B2 (en) | 2018-02-28 | 2024-09-03 | Arizona Board Of Regents On Behalf Of The University Of Arizona | Efficient copper leaching using alkanesulfonic acids |
| CN108754137A (zh) * | 2018-08-02 | 2018-11-06 | 桐乡市思远环保科技有限公司 | 采用溶剂萃取电积工艺生产金属铅的方法 |
| CN109097575B (zh) * | 2018-09-10 | 2020-06-05 | 中国恩菲工程技术有限公司 | 低品位铅锌矿中锌元素的提取方法 |
| CN110453077A (zh) * | 2019-08-26 | 2019-11-15 | 湘潭大学 | 一种废铅膏回收利用的方法 |
| CN113832344B (zh) * | 2020-06-08 | 2022-06-14 | 中南大学 | 一种从铜钴渣中回收铜、钴的方法 |
| CN111926187A (zh) * | 2020-08-19 | 2020-11-13 | 楚雄滇中有色金属有限责任公司 | 一种从酸泥中综合回收硒、汞、铅和银的方法 |
| CN114480862B (zh) * | 2022-01-25 | 2024-01-30 | 长沙有色冶金设计研究院有限公司 | 一种从铜浮渣中回收有价元素的方法 |
| GB202306674D0 (en) * | 2023-05-05 | 2023-06-21 | Bluecap Resources | Extraction method |
Family Cites Families (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1752356A (en) * | 1927-01-14 | 1930-04-01 | Primos Lead Company | Process for reclaiming battery-plate material |
| US2525942A (en) * | 1945-06-29 | 1950-10-17 | Standard Oil Co | Electrodepositing bath and process |
| US3929597A (en) * | 1974-05-17 | 1975-12-30 | Hecla Mining Co | Production of lead and silver from their sulfides |
| FI61721C (fi) * | 1976-03-25 | 1982-09-10 | Lyijyvalkoistehd Groenberg Bly | Saett att aotervinna bly av blyavfall |
| JPS5411829A (en) * | 1977-06-30 | 1979-01-29 | Sumikou Ai Esu Pii Kk | Electolytical refining of lead |
| JPS5493626A (en) * | 1978-01-06 | 1979-07-24 | Diamond Eng Co Ltd | Method of regenerating and recovering lead from leaddsulfateecontaining waste product |
| US4181588A (en) * | 1979-01-04 | 1980-01-01 | The United States Of America As Represented By The Secretary Of The Interior | Method of recovering lead through the direct reduction of lead chloride by aqueous electrolysis |
| US4272341A (en) * | 1980-01-09 | 1981-06-09 | Duval Corporation | Process for recovery of metal values from lead-zinc ores, even those having a high carbonate content |
| IT1188203B (it) * | 1985-11-19 | 1988-01-07 | Tecneco Spa | Processo idrometallurgico per ricuperare in forma metallica pura il piombo contenuto nella massa attiva delle batterie esauste |
| IT1191650B (it) * | 1986-01-09 | 1988-03-23 | Tecneco Spa | Processo idrometallurgico per un recupero complessivo dei componenti delle batterie acide al piombo esauste |
| US4650553A (en) * | 1986-03-21 | 1987-03-17 | Pennwalt Corporation | Electrolytic recovery of lead from scrap |
| IT1223314B (it) * | 1987-10-20 | 1990-09-19 | Engitec Impianti | Processo idrometallurgico per recuperare in forma metallica pura tutto il piombo contenuto nella massa attiva delle batterie esauste |
| US4944851A (en) * | 1989-06-05 | 1990-07-31 | Macdermid, Incorporated | Electrolytic method for regenerating tin or tin-lead alloy stripping compositions |
| US5262020A (en) * | 1991-03-13 | 1993-11-16 | M.A. Industries, Inc. | Hydrometallurgical method of producing metallic lead from materials containing oxides, particularly from the active material of accumulators |
| IT1245449B (it) * | 1991-03-13 | 1994-09-20 | Ginatta Spa | Procedimento idrometallurgico per la produzione del piombo sotto forma di metallo da materiali contenenti ossidi, particolarmete dalla materia attiva degli accumulatori |
| US5494649A (en) * | 1991-10-03 | 1996-02-27 | Cognis, Inc. | Process for removing heavy metals from paint chips |
| US5762683A (en) * | 1994-12-09 | 1998-06-09 | Asarco Incorporated | Ferric fluoborate/organic extractant hydrometallurgical process for recovering metals |
| US5612224A (en) * | 1995-02-21 | 1997-03-18 | 21St Century Companies, Inc. | Method for measuring the quantity of lead on the surface of a brass component |
| US5520794A (en) * | 1995-05-15 | 1996-05-28 | Elf Atochem North America, Inc. | Electrowinning of lead |
| US5935409A (en) * | 1998-03-26 | 1999-08-10 | Asarco Incorporated | Fluoboric acid control in a ferric fluoborate hydrometallurgical process for recovering metals |
| US6117209A (en) * | 1998-11-02 | 2000-09-12 | Gnb Technologies, Inc. | Hydrometallurgical process for treating alloys and drosses to recover the metal components |
| US6428676B1 (en) * | 2000-11-08 | 2002-08-06 | Enthone Inc. | Process for producing low alpha lead methane sulfonate |
| US7368043B2 (en) | 2003-04-10 | 2008-05-06 | Applied Intellectual Capital | Configurations and methods of electrochemical lead recovery from contaminated soil |
| NZ570813A (en) * | 2006-03-01 | 2010-09-30 | Basf Se | Process for the acid digestion of metal-containing compounds |
| ITVA20070007A1 (it) * | 2007-01-17 | 2008-07-18 | Millbrook Lead Recycling Techn | Recupero del piombo sottoforma di carbonato ad altissima purezza da pastello di recupero dalla frantumazione di accumulatori al piombo esausti |
| JP4798469B2 (ja) * | 2009-03-23 | 2011-10-19 | Jx日鉱日石金属株式会社 | 鉛の炭酸化方法 |
| JP2012072480A (ja) | 2010-09-27 | 2012-04-12 | Jx Nippon Mining & Metals Corp | InとSnの混合物からのInの選択的回収方法 |
| CA2869431A1 (en) * | 2012-04-06 | 2013-10-10 | Entegris, Inc. | Removal of lead from solid materials |
-
2013
- 2013-11-11 US US14/076,564 patent/US9322104B2/en active Active
- 2013-11-13 CA CA2860614A patent/CA2860614C/en active Active
- 2013-11-13 AU AU2013346480A patent/AU2013346480B2/en active Active
- 2013-11-13 MX MX2014009406A patent/MX364711B/es active IP Right Grant
- 2013-11-13 ES ES13812067.0T patent/ES2657632T3/es active Active
- 2013-11-13 RS RS20180089A patent/RS56991B1/sr unknown
- 2013-11-13 PL PL13812067T patent/PL2920330T3/pl unknown
- 2013-11-13 PT PT138120670T patent/PT2920330T/pt unknown
- 2013-11-13 CN CN201380004685.0A patent/CN104039991B/zh active Active
- 2013-11-13 EP EP13812067.0A patent/EP2920330B1/en active Active
- 2013-11-13 WO PCT/IB2013/002540 patent/WO2014076547A1/en not_active Ceased
- 2013-11-13 JP JP2015541251A patent/JP6356137B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| PL2920330T3 (pl) | 2018-05-30 |
| RS56991B1 (sr) | 2018-05-31 |
| EP2920330B1 (en) | 2017-11-01 |
| JP2016502602A (ja) | 2016-01-28 |
| AU2013346480A1 (en) | 2014-07-24 |
| JP6356137B2 (ja) | 2018-07-11 |
| US9322104B2 (en) | 2016-04-26 |
| CA2860614A1 (en) | 2014-05-22 |
| MX364711B (es) | 2019-05-06 |
| ES2657632T3 (es) | 2018-03-06 |
| US20140131219A1 (en) | 2014-05-15 |
| MX2014009406A (es) | 2014-11-10 |
| WO2014076547A1 (en) | 2014-05-22 |
| PT2920330T (pt) | 2018-01-29 |
| CN104039991B (zh) | 2018-03-27 |
| CN104039991A (zh) | 2014-09-10 |
| EP2920330A1 (en) | 2015-09-23 |
| AU2013346480B2 (en) | 2017-08-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20181106 |
|
| MPN | Maintenance fee for patent paid |
Free format text: FEE DESCRIPTION TEXT: MF (PATENT, 11TH ANNIV.) - STANDARD Year of fee payment: 11 |
|
| U00 | Fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U00-U101 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE REQUEST RECEIVED Effective date: 20241104 |
|
| U11 | Full renewal or maintenance fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT DETERMINED COMPLIANT Effective date: 20241104 Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT PAID IN FULL Effective date: 20241104 |
|
| MPN | Maintenance fee for patent paid |
Free format text: FEE DESCRIPTION TEXT: MF (PATENT, 12TH ANNIV.) - STANDARD Year of fee payment: 12 |
|
| U00 | Fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U00-U101 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE REQUEST RECEIVED Effective date: 20251023 |
|
| U11 | Full renewal or maintenance fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT PAID IN FULL Effective date: 20251023 |