CA2870073A1 - Procede de fabrication de produits d'hydroxyde de sodium et de chlorure de sodium a partir de saumure residuaire - Google Patents

Procede de fabrication de produits d'hydroxyde de sodium et de chlorure de sodium a partir de saumure residuaire Download PDF

Info

Publication number: CA2870073A1
Authority: CA; Canada
Prior art keywords: brine; sodium; sodium chloride; process according; sodium hydroxide
Prior art date: 2013-07-09
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Abandoned

Application number

CA2870073A

Other languages

English (en)

Inventor

John H. Worsley

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Individual

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2013-07-09

Filing date

2014-11-03

Publication date

2015-01-09

2013-07-09 Priority claimed from AU2013902526A external-priority patent/AU2013902526A0/en

2014-07-06 Priority claimed from AU2014203695A external-priority patent/AU2014203695B2/en

2014-11-03 Application filed by Individual filed Critical Individual

2015-01-09 Publication of CA2870073A1 publication Critical patent/CA2870073A1/fr

Status Abandoned legal-status Critical Current

Links

FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 title claims abstract description 172
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 title claims abstract description 171
HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 title claims abstract description 129
239000012267 brine Substances 0.000 title claims abstract description 126
238000000034 method Methods 0.000 title claims abstract description 109
230000008569 process Effects 0.000 title claims abstract description 99
239000011780 sodium chloride Substances 0.000 title claims abstract description 85
238000004519 manufacturing process Methods 0.000 title claims abstract description 18
239000002699 waste material Substances 0.000 title claims abstract description 13
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 139
229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 68
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 66
150000003839 salts Chemical class 0.000 claims abstract description 54
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 51
235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 34
229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 34
239000004571 lime Substances 0.000 claims abstract description 28
238000001704 evaporation Methods 0.000 claims abstract description 26
230000008020 evaporation Effects 0.000 claims abstract description 26
235000008733 Citrus aurantifolia Nutrition 0.000 claims abstract description 25
235000011941 Tilia x europaea Nutrition 0.000 claims abstract description 25
229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 25
239000012535 impurity Substances 0.000 claims abstract description 24
239000000243 solution Substances 0.000 claims abstract description 24
239000013078 crystal Substances 0.000 claims abstract description 21
239000000356 contaminant Substances 0.000 claims abstract description 15
238000001816 cooling Methods 0.000 claims abstract description 10
230000002829 reductive effect Effects 0.000 claims abstract description 8
238000000926 separation method Methods 0.000 claims abstract description 8
239000003513 alkali Substances 0.000 claims abstract description 7
235000017550 sodium carbonate Nutrition 0.000 claims description 66
ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 35
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 30
238000006243 chemical reaction Methods 0.000 claims description 29
235000010216 calcium carbonate Nutrition 0.000 claims description 24
238000009993 causticizing Methods 0.000 claims description 24
239000011575 calcium Substances 0.000 claims description 22
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 20
239000000292 calcium oxide Substances 0.000 claims description 18
235000012255 calcium oxide Nutrition 0.000 claims description 18
238000002425 crystallisation Methods 0.000 claims description 18
238000005406 washing Methods 0.000 claims description 17
239000011777 magnesium Substances 0.000 claims description 15
229910052791 calcium Inorganic materials 0.000 claims description 14
239000000377 silicon dioxide Substances 0.000 claims description 14
229910052749 magnesium Inorganic materials 0.000 claims description 13
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 12
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 11
230000000694 effects Effects 0.000 claims description 10
238000011084 recovery Methods 0.000 claims description 9
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 6
238000007792 addition Methods 0.000 claims description 6
238000011109 contamination Methods 0.000 claims description 6
239000011552 falling film Substances 0.000 claims description 4
238000007670 refining Methods 0.000 claims description 4
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 3
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
239000003153 chemical reaction reagent Substances 0.000 claims description 3
238000000975 co-precipitation Methods 0.000 claims description 3
239000003245 coal Substances 0.000 claims description 3
230000008021 deposition Effects 0.000 claims description 3
238000000605 extraction Methods 0.000 claims description 3
239000002655 kraft paper Substances 0.000 claims description 3
239000000203 mixture Substances 0.000 claims description 3
238000004064 recycling Methods 0.000 claims description 3
230000000740 bleeding effect Effects 0.000 claims description 2
238000009297 electrocoagulation Methods 0.000 claims description 2
229910052500 inorganic mineral Inorganic materials 0.000 claims description 2
239000012528 membrane Substances 0.000 claims description 2
235000010755 mineral Nutrition 0.000 claims description 2
239000011707 mineral Substances 0.000 claims description 2
238000000746 purification Methods 0.000 claims description 2
-1 sodium chloride saturated brine Chemical class 0.000 claims description 2
238000012546 transfer Methods 0.000 claims description 2
238000000108 ultra-filtration Methods 0.000 claims description 2
235000012204 lemonade/lime carbonate Nutrition 0.000 claims 3
238000010306 acid treatment Methods 0.000 claims 1
BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims 1
238000003844 diaphragm cell process Methods 0.000 claims 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
229940088417 precipitated calcium carbonate Drugs 0.000 claims 1
239000012047 saturated solution Substances 0.000 claims 1
239000007787 solid Substances 0.000 abstract description 18
239000000047 product Substances 0.000 description 33
239000003518 caustics Substances 0.000 description 15
238000013461 design Methods 0.000 description 10
238000012545 processing Methods 0.000 description 10
108091006629 SLC13A2 Proteins 0.000 description 9
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 9
239000000920 calcium hydroxide Substances 0.000 description 9
235000011116 calcium hydroxide Nutrition 0.000 description 9
229910001861 calcium hydroxide Inorganic materials 0.000 description 9
230000009286 beneficial effect Effects 0.000 description 7
239000002244 precipitate Substances 0.000 description 7
239000002002 slurry Substances 0.000 description 7
239000012065 filter cake Substances 0.000 description 6
238000001223 reverse osmosis Methods 0.000 description 6
238000003860 storage Methods 0.000 description 6
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 5
230000015572 biosynthetic process Effects 0.000 description 5
238000001914 filtration Methods 0.000 description 5
238000005755 formation reaction Methods 0.000 description 5
238000010438 heat treatment Methods 0.000 description 5
238000002347 injection Methods 0.000 description 5
239000007924 injection Substances 0.000 description 5
238000002474 experimental method Methods 0.000 description 4
238000001556 precipitation Methods 0.000 description 4
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
239000002253 acid Substances 0.000 description 3
230000008901 benefit Effects 0.000 description 3
239000012141 concentrate Substances 0.000 description 3
239000000706 filtrate Substances 0.000 description 3
239000007788 liquid Substances 0.000 description 3
239000001095 magnesium carbonate Substances 0.000 description 3
235000014380 magnesium carbonate Nutrition 0.000 description 3
229910000021 magnesium carbonate Inorganic materials 0.000 description 3
ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 3
VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 3
239000000347 magnesium hydroxide Substances 0.000 description 3
229910001862 magnesium hydroxide Inorganic materials 0.000 description 3
235000012254 magnesium hydroxide Nutrition 0.000 description 3
238000006386 neutralization reaction Methods 0.000 description 3
239000011591 potassium Substances 0.000 description 3
229910052700 potassium Inorganic materials 0.000 description 3
230000009467 reduction Effects 0.000 description 3
229920006395 saturated elastomer Polymers 0.000 description 3
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 2
238000001035 drying Methods 0.000 description 2
230000007613 environmental effect Effects 0.000 description 2
230000005484 gravity Effects 0.000 description 2
229910052742 iron Inorganic materials 0.000 description 2
150000002681 magnesium compounds Chemical class 0.000 description 2
230000007246 mechanism Effects 0.000 description 2
238000001953 recrystallisation Methods 0.000 description 2
230000001105 regulatory effect Effects 0.000 description 2
239000002562 thickening agent Substances 0.000 description 2
238000010977 unit operation Methods 0.000 description 2
HNGIZKAMDMBRKJ-UHFFFAOYSA-N 2-acetamido-3-(1h-indol-3-yl)propanamide Chemical compound C1=CC=C2C(CC(NC(=O)C)C(N)=O)=CNC2=C1 HNGIZKAMDMBRKJ-UHFFFAOYSA-N 0.000 description 1
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
238000004131 Bayer process Methods 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
241001602876 Nata Species 0.000 description 1
208000034809 Product contamination Diseases 0.000 description 1
230000002411 adverse Effects 0.000 description 1
235000011114 ammonium hydroxide Nutrition 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
238000013459 approach Methods 0.000 description 1
229910052788 barium Inorganic materials 0.000 description 1
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
WDIHJSXYQDMJHN-UHFFFAOYSA-L barium chloride Chemical compound [Cl-].[Cl-].[Ba+2] WDIHJSXYQDMJHN-UHFFFAOYSA-L 0.000 description 1
229910001626 barium chloride Inorganic materials 0.000 description 1
238000009835 boiling Methods 0.000 description 1
238000001354 calcination Methods 0.000 description 1
229910000020 calcium bicarbonate Inorganic materials 0.000 description 1
229940043430 calcium compound Drugs 0.000 description 1
ZFXVRMSLJDYJCH-UHFFFAOYSA-N calcium magnesium Chemical compound [Mg].[Ca] ZFXVRMSLJDYJCH-UHFFFAOYSA-N 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000000701 coagulant Substances 0.000 description 1
238000010276 construction Methods 0.000 description 1
239000000498 cooling water Substances 0.000 description 1
150000004691 decahydrates Chemical class 0.000 description 1
230000007423 decrease Effects 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
239000008394 flocculating agent Substances 0.000 description 1
239000012530 fluid Substances 0.000 description 1
239000003673 groundwater Substances 0.000 description 1
238000006703 hydration reaction Methods 0.000 description 1
230000008676 import Effects 0.000 description 1
238000010348 incorporation Methods 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
238000009533 lab test Methods 0.000 description 1
230000000670 limiting effect Effects 0.000 description 1
239000010808 liquid waste Substances 0.000 description 1
230000007774 longterm Effects 0.000 description 1
229910000022 magnesium bicarbonate Inorganic materials 0.000 description 1
235000014824 magnesium bicarbonate Nutrition 0.000 description 1
239000000391 magnesium silicate Substances 0.000 description 1
229910052748 manganese Inorganic materials 0.000 description 1
239000011572 manganese Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
238000012544 monitoring process Methods 0.000 description 1
239000000123 paper Substances 0.000 description 1
230000035699 permeability Effects 0.000 description 1
238000010248 power generation Methods 0.000 description 1
238000003672 processing method Methods 0.000 description 1
238000005086 pumping Methods 0.000 description 1
238000010926 purge Methods 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
238000003756 stirring Methods 0.000 description 1
229910052712 strontium Inorganic materials 0.000 description 1
CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
239000000126 substance Substances 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
239000002352 surface water Substances 0.000 description 1
230000008719 thickening Effects 0.000 description 1
238000011144 upstream manufacturing Methods 0.000 description 1
239000002351 wastewater Substances 0.000 description 1
239000003643 water by type Substances 0.000 description 1

Classifications

- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals

Landscapes

Heat Treatment Of Water, Waste Water Or Sewage (AREA)

CA2870073A 2013-07-09 2014-11-03 Procede de fabrication de produits d'hydroxyde de sodium et de chlorure de sodium a partir de saumure residuaire Abandoned CA2870073A1 (fr)

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date	Title
AU2013902526A AU2013902526A0 (en)		2013-07-09	Process for Manufacture of Sodium Hydroxide and Sodium Chloride Products from Waste Brine
AU2013902526		2013-07-09
AU2014203695A AU2014203695B2 (en)	2013-07-09	2014-07-06	Process for Manufacture of Sodium Hydroxide and Sodium Chloride Products from Waste Brine
AU2014203695		2014-07-06

Publications (1)

Publication Number	Publication Date
CA2870073A1 true CA2870073A1 (fr)	2015-01-09

Family

ID=52274454

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA2870073A Abandoned CA2870073A1 (fr)	2013-07-09	2014-11-03	Procede de fabrication de produits d'hydroxyde de sodium et de chlorure de sodium a partir de saumure residuaire

Country Status (1)

Country	Link
CA (1)	CA2870073A1 (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
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CN113718292A (zh) *	2021-08-27	2021-11-30	河南佰利联新材料有限公司	一种氯化法钛白粉生产中废渣回收利用的方法
CN115613056A (zh) *	2022-11-07	2023-01-17	上海泓济环保科技股份有限公司	有机硅行业废盐资源化制备离子膜烧碱的方法
CN115634900A (zh) *	2022-11-29	2023-01-24	国能龙源环保有限公司	一种固废杂盐资源化回收利用的方法及系统

2014
- 2014-11-03 CA CA2870073A patent/CA2870073A1/fr not_active Abandoned

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN113718292A (zh) *	2021-08-27	2021-11-30	河南佰利联新材料有限公司	一种氯化法钛白粉生产中废渣回收利用的方法
CN115613056A (zh) *	2022-11-07	2023-01-17	上海泓济环保科技股份有限公司	有机硅行业废盐资源化制备离子膜烧碱的方法
CN115634900A (zh) *	2022-11-29	2023-01-24	国能龙源环保有限公司	一种固废杂盐资源化回收利用的方法及系统

Legal Events

Date	Code	Title	Description
2018-12-17	FZDE	Dead	Effective date: 20181105

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US20140356262A1 (en)	2014-12-04	Method for treating tailings pond liquor
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JP7422776B2 (ja)	2024-01-26	水酸化リチウムの回収
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CA2870073A1 - Procede de fabrication de produits d'hydroxyde de sodium et de chlorure de sodium a partir de saumure residuaire - Google Patents

Info

Links

Classifications

Landscapes

Applications Claiming Priority (4)

Publications (1)

Family

ID=52274454

Family Applications (1)

Country Status (1)

Cited By (3)

Cited By (3)

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