CA3101904A1 - Production de 5-hydroxymethylfurfural catalyse a l'aide d'un melange de sel et d'acide - Google Patents

Production de 5-hydroxymethylfurfural catalyse a l'aide d'un melange de sel et d'acide Download PDF

Info

Publication number
CA3101904A1
CA3101904A1 CA3101904A CA3101904A CA3101904A1 CA 3101904 A1 CA3101904 A1 CA 3101904A1 CA 3101904 A CA3101904 A CA 3101904A CA 3101904 A CA3101904 A CA 3101904A CA 3101904 A1 CA3101904 A1 CA 3101904A1
Authority
CA
Canada
Prior art keywords
acid
hmf
fructose
fraction
mol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CA3101904A
Other languages
English (en)
Inventor
Alireza Haji Begli
Christine Kroner
Kay MANTYK
Ralf RIEMENSCHNITTER
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suedzucker AG
Original Assignee
Suedzucker AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suedzucker AG filed Critical Suedzucker AG
Publication of CA3101904A1 publication Critical patent/CA3101904A1/fr
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)

Abstract

Production de HMF catalysée par un mélange de sels et d'acides La présente invention concerne un procédé pour la production de 5-hydroxyméthylfurfural (HMF), dans lequel un composant contenant du fructose est transformé par utilisation d'un système catalytique comprenant une solution d'un mélange de sels et d'acides, à une température de 90 jusqu'à 200 °C, ce qui mène à l'obtention d'un mélange de produits contenant du HMF, une sélectivité élevée pour le HMF avec simultanément une production de sous-produits notablement plus faible étant avantageusement atteintes.
CA3101904A 2018-05-29 2019-05-28 Production de 5-hydroxymethylfurfural catalyse a l'aide d'un melange de sel et d'acide Pending CA3101904A1 (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102018208510.2 2018-05-29
DE102018208510.2A DE102018208510A1 (de) 2018-05-29 2018-05-29 Salz- und Säuregemisch-katalysierte HMF-Herstellung
PCT/EP2019/063862 WO2019229080A1 (fr) 2018-05-29 2019-05-28 Production de hmf catalysée par un mélange de sels et d'acides

Publications (1)

Publication Number Publication Date
CA3101904A1 true CA3101904A1 (fr) 2019-12-05

Family

ID=66867095

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3101904A Pending CA3101904A1 (fr) 2018-05-29 2019-05-28 Production de 5-hydroxymethylfurfural catalyse a l'aide d'un melange de sel et d'acide

Country Status (10)

Country Link
US (1) US11548863B2 (fr)
EP (1) EP3802505A1 (fr)
JP (1) JP7410058B2 (fr)
CN (1) CN112236419B (fr)
AU (1) AU2019276050B2 (fr)
CA (1) CA3101904A1 (fr)
DE (1) DE102018208510A1 (fr)
EA (1) EA202092881A1 (fr)
MX (1) MX2020012880A (fr)
WO (1) WO2019229080A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10208006B2 (en) 2016-01-13 2019-02-19 Stora Enso Oyj Processes for the preparation of 2,5-furandicarboxylic acid and intermediates and derivatives thereof
WO2019014382A1 (fr) 2017-07-12 2019-01-17 Stora Enso Oyj Produits purifiés de la voie de l'acide 2,5-furandicarboxylique
WO2024216102A1 (fr) * 2023-04-12 2024-10-17 Origin Materials Operating, Inc. Procédés d'extraction d'acide lévulinique à l'aide de 2-méthyl tétrahydrofurane

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3601281A1 (de) * 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
FR2663933B1 (fr) * 1990-06-27 1994-06-17 Beghin Say Sa Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides.
DE102004063006A1 (de) 2004-12-22 2006-07-13 Basf Ag Verfahren zur Isolierung von Coenzym Q10
BR112012024133A2 (pt) * 2010-04-07 2015-09-15 Novozymes As método para produzir 5-hidroximetilfurfural e para converter hmf, e, uso de ácido 2, 5-furanodicarboxílico
JPWO2013002397A1 (ja) 2011-06-29 2015-02-23 国立大学法人愛媛大学 フルフラール類の製造方法、及び、フルフラール類の製造装置
IN2014CN03466A (fr) 2011-10-12 2015-07-03 Novozymes As
WO2013066776A1 (fr) * 2011-10-31 2013-05-10 E. I. Du Pont De Nemours And Company Procédés de production de 5-(hydroxyméthyl)furfural
CN102399202B (zh) * 2011-12-02 2014-03-05 复旦大学 一种利用生物质糖制备5-羟甲基糠醛的方法
AU2012364787A1 (en) 2012-01-10 2014-07-03 Archer Daniels Midland Company Process for making HMF and HMF derivatives from sugars, with recovery of unreacted sugars suitable for direct fermentation to ethanol
RU2659166C2 (ru) 2013-03-14 2018-06-28 Арчер Дэниелс Мидлэнд Компани Способ получения HMF из сахаров с пониженным образованием побочных продуктов и композиции HMF с улучшенной стабильностью
CN104761519A (zh) * 2014-01-02 2015-07-08 湖南师范大学 一种在纯水中碳水化合物有效转化为5-羟甲基糠醛的方法
CN106029642B (zh) 2014-01-27 2019-11-29 阿彻丹尼尔斯米德兰公司 含果糖的原料向含hmf的产物的转化
JP6328990B2 (ja) 2014-04-28 2018-05-23 国立研究開発法人産業技術総合研究所 ヒドロキシメチルフルフラールの合成方法
DE102014220517A1 (de) * 2014-10-09 2016-04-14 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt Verbesserte 5-Hydroxyfurfural-Herstellung
CN104844543A (zh) 2015-05-27 2015-08-19 厦门大学 一种由果糖制备5-羟甲基糠醛的方法
JP2017000110A (ja) 2015-06-12 2017-01-05 国立大学法人金沢大学 イオン液体、グルコースの製造方法及びエタノールの製造方法
WO2017184545A1 (fr) 2016-04-18 2017-10-26 Rennovia, Inc. Conversion de matières premières contenant du fructose en produit contenant de l'hmf
DE102016224073A1 (de) * 2016-12-02 2018-06-07 Südzucker AG Verbessertes HMF-Herstellungsverfahren

Also Published As

Publication number Publication date
EP3802505A1 (fr) 2021-04-14
US11548863B2 (en) 2023-01-10
DE102018208510A1 (de) 2019-12-05
JP2021525732A (ja) 2021-09-27
MX2020012880A (es) 2021-02-18
BR112020024326A2 (pt) 2021-05-04
WO2019229080A1 (fr) 2019-12-05
CN112236419A (zh) 2021-01-15
EA202092881A1 (ru) 2021-03-11
WO2019229080A4 (fr) 2020-01-23
AU2019276050A1 (en) 2020-12-10
US20210214326A1 (en) 2021-07-15
CN112236419B (zh) 2025-03-18
AU2019276050B2 (en) 2024-01-25
JP7410058B2 (ja) 2024-01-09

Similar Documents

Publication Publication Date Title
CN110035999B (zh) 羟甲基糠醛制备方法
US10017486B2 (en) Conversion of fructose-containing feedstocks to HMF-containing product
CA2914308A1 (fr) Procede de production de 5-hydroxymethylfurfural (hmf)
WO2013146085A1 (fr) Procédé de fabrication du 5-hydroxyméthyl furfural
JP2013203666A (ja) ５−ヒドロキシメチルフルフラール酸化物の製造方法
AU2019276050B2 (en) Salt and acid mixture catalyzed hmf production
WO2017184545A1 (fr) Conversion de matières premières contenant du fructose en produit contenant de l'hmf
EP1351949B1 (fr) Procede en continu de production d'acide l-ascorbique
AU2019276047B2 (en) Anolyte fraction-catalyzed hmf production
US20170015642A1 (en) Conversion of fructose-containing feedstocks to hmf-containing product
CN117820263A (zh) 一种5-羟甲基糠醛晶体的制备及提纯方法
WO2019014393A1 (fr) Nouveaux procédés de préparation d'acide 2,5-furandicarboxylique
CA3045541C (fr) Procédé de production de hmf
BR112020024326B1 (pt) Produção de hmf catalisado por mistura de sal e ácido
EA045367B1 (ru) Получение hmf, катализируемое смесью соли и кислоты
WO2019150578A1 (fr) Procédé de préparation de cyclopenténone
WO2026013041A1 (fr) Procédé amélioré pour la synthèse et la purification de hmf

Legal Events

Date Code Title Description
EEER Examination request

Effective date: 20220726

D15 Examination report completed

Free format text: ST27 STATUS EVENT CODE: A-2-2-D10-D15-D126 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: EXAMINER'S REPORT

Effective date: 20240816

P11 Amendment of application requested

Free format text: ST27 STATUS EVENT CODE: A-2-2-P10-P11-P100 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: AMENDMENT RECEIVED - RESPONSE TO EXAMINER'S REQUISITION

Effective date: 20241209

W00 Other event occurred

Free format text: ST27 STATUS EVENT CODE: A-2-2-W10-W00-W111 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: CORRESPONDENT DETERMINED COMPLIANT

Effective date: 20250205

MFA Maintenance fee for application paid

Free format text: FEE DESCRIPTION TEXT: MF (APPLICATION, 6TH ANNIV.) - STANDARD

Year of fee payment: 6

U00 Fee paid

Free format text: ST27 STATUS EVENT CODE: A-2-2-U10-U00-U101 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE REQUEST RECEIVED

Effective date: 20250519

U11 Full renewal or maintenance fee paid

Free format text: ST27 STATUS EVENT CODE: A-2-2-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT PAID IN FULL

Effective date: 20250519

P11 Amendment of application requested

Free format text: ST27 STATUS EVENT CODE: A-2-2-P10-P11-P102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: AMENDMENT DETERMINED COMPLIANT

Effective date: 20250607

P13 Application amended

Free format text: ST27 STATUS EVENT CODE: A-2-2-P10-P13-X000 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: APPLICATION AMENDED

Effective date: 20250607

D15 Examination report completed

Free format text: ST27 STATUS EVENT CODE: A-2-2-D10-D15-D126 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: EXAMINER'S REPORT

Effective date: 20251024

P11 Amendment of application requested

Free format text: ST27 STATUS EVENT CODE: A-2-2-P10-P11-P100 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: AMENDMENT RECEIVED - RESPONSE TO EXAMINER'S REQUISITION

Effective date: 20260220

P11 Amendment of application requested

Free format text: ST27 STATUS EVENT CODE: A-2-2-P10-P11-P102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: AMENDMENT DETERMINED COMPLIANT

Effective date: 20260223

P13 Application amended

Free format text: ST27 STATUS EVENT CODE: A-2-2-P10-P13-X000 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: APPLICATION AMENDED

Effective date: 20260223

W00 Other event occurred

Free format text: ST27 STATUS EVENT CODE: A-2-2-W10-W00-W111 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: CORRESPONDENT DETERMINED COMPLIANT

Effective date: 20260223