CH100933A - Process for evaporating salt solutions. - Google Patents
Process for evaporating salt solutions.Info
- Publication number
- CH100933A CH100933A CH100933DA CH100933A CH 100933 A CH100933 A CH 100933A CH 100933D A CH100933D A CH 100933DA CH 100933 A CH100933 A CH 100933A
- Authority
- CH
- Switzerland
- Prior art keywords
- chamber
- evaporation
- chambers
- unheated
- vapor
- Prior art date
Links
- 238000001704 evaporation Methods 0.000 claims description 16
- 230000008020 evaporation Effects 0.000 claims description 13
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- 150000003839 salts Chemical class 0.000 claims description 5
- 239000013078 crystal Substances 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 230000006835 compression Effects 0.000 claims 2
- 238000007906 compression Methods 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 235000002639 sodium chloride Nutrition 0.000 description 5
- 239000012266 salt solution Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 3
- 206010038743 Restlessness Diseases 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Description
Verfahren zum Eindampfen von Salzlösungen. Es sind Verfahren zum Eindampfen von Salzlösungen bekannt, bei denen letztere nach Durchgang durch eine Heizkammer in eine unter niedrigerem Druck stehende, ungeheizte Verdampfungskamm,er gelangen. In der letzt genannten Verdampfungskammer unterliegt die Salzlösung einer heftigen Verdampfung durch Kochen, wobei entsprechend der Was serabgabe Salz ausgeschieden wird.
Dieses Verfahren ist aber dann nicht an wendbar, wenn es sieh darum handelt, das Salz in grobkristallinischer Form zu erhalten, denn die unruhige, kochende Flüssigkeitsober- fläche lässt es nicht zu, da,ss die Salzkristalle Gelegenheit zum Auswachsen erhalten.
Diese Übelstände sollen durch die vorlie gende Erfindung beseitigt werden, wodurch es gelingt, ein Salz von grobkristallinischer Form, und zwar bei Anwendung von Koch salzlösung in Form .der bekannten Pyramiden kristalle zu erhalten.
Bei dem vorliegenden Verfahren wird die Salzlösung in bekannter Weise nach Durch gang durch eine Heizkammer in eine unter niedrigerem Druck stehende Verdunstungs kammer geleitet. Die dabei zur Anwendung gelangende Neuerung beruht darauf, dass der Dampfdruckunterschied in den beiden Kam mern auf solcher Höhe erhalten wird, dass in der ungeheizten Verdunstungskammer wohl eine Verdunstung der Lösung eintritt, aber das Kochen derselben vermieden wird. Auf diese Weise bilden sich an der Ober fläche der ruhigen Lösung grobe Kristalle, die volle Gelegenheit zum Auswachsen haben.
Der aus den beiden Kammern abziehende Dampf wird zweckmässigerweise zu einem Kompressor geführt, worin er verdichtet und zur Heizung .der Heizkammer verwendet wird.
M.an kann auch einen Verdichter zwi schen idie beiden Kammern derart einschalten, dass er den Dampf aus der Verdunstungskam mer absaugt und in den Brüdendampfraum ,der Heizkammer drängt, wobei die gesamte Dampfmenge hier .durch einen Verdichter .ab gesaugt wird, der sie auf den zur Verwen dung als Heizdampf erforderlichen Druck bringt.
Zur Einstellung des Dampf druckunter- schiedes in den beiden Kammern können zum Beispiel getrennte Absauge - Vorrichtungen verwendet werden; man kann dazu aber auch bestimmte, geeignete Stufen des gleichen Ver dichters verwenden.
Den niedrigeren Dampfdruck in .der un geheizten Verdunstungskammer kann man ferner auch dadurch einstellen, dass man Luft in diese Kammer einführt:
Process for evaporating salt solutions. Processes for evaporating salt solutions are known, in which the latter, after passing through a heating chamber, get into an unheated evaporation comb which is under lower pressure. In the last-mentioned evaporation chamber, the salt solution is subject to vigorous evaporation by boiling, whereby salt is excreted according to the amount of water released.
However, this method cannot be used if the aim is to preserve the salt in a coarsely crystalline form, because the restless, boiling liquid surface does not allow the salt crystals to grow out.
These inconveniences are to be eliminated by the present invention, whereby it is possible to obtain a salt of coarsely crystalline form, namely when using common salt solution in the form of the known pyramid crystals.
In the present method, the salt solution is passed in a known manner after passage through a heating chamber into a lower pressure evaporation chamber. The innovation used here is based on the fact that the vapor pressure difference in the two chambers is maintained at such a level that evaporation of the solution occurs in the unheated evaporation chamber, but cooking of the same is avoided. In this way, coarse crystals form on the surface of the calm solution and have full opportunities to grow out.
The steam drawn off from the two chambers is expediently fed to a compressor, where it is compressed and used to heat the heating chamber.
You can also switch on a compressor between the two chambers in such a way that it sucks the vapor out of the evaporation chamber and pushes it into the vapor space, the heating chamber, whereby the entire amount of vapor is sucked out by a compressor that opens it brings the pressure required for use as heating steam.
For example, separate suction devices can be used to adjust the steam pressure difference in the two chambers; but you can also use certain, suitable stages of the same Ver poet.
The lower vapor pressure in the unheated evaporation chamber can also be adjusted by introducing air into this chamber:
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE100933X | 1921-06-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH100933A true CH100933A (en) | 1923-08-16 |
Family
ID=5648706
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH100933D CH100933A (en) | 1921-06-04 | 1922-05-24 | Process for evaporating salt solutions. |
Country Status (2)
| Country | Link |
|---|---|
| AT (1) | AT96934B (en) |
| CH (1) | CH100933A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2556184A (en) * | 1946-03-25 | 1951-06-12 | Ici Ltd | Anhydrous calcium chloride process |
-
1922
- 1922-05-22 AT AT96934D patent/AT96934B/en active
- 1922-05-24 CH CH100933D patent/CH100933A/en unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2556184A (en) * | 1946-03-25 | 1951-06-12 | Ici Ltd | Anhydrous calcium chloride process |
Also Published As
| Publication number | Publication date |
|---|---|
| AT96934B (en) | 1924-05-10 |
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