CH116276A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH116276A CH116276A CH116276DA CH116276A CH 116276 A CH116276 A CH 116276A CH 116276D A CH116276D A CH 116276DA CH 116276 A CH116276 A CH 116276A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- azo dye
- dye
- dianotized
- naphthylamide
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims description 3
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 claims description 3
- 229920000742 Cotton Polymers 0.000 claims description 2
- 235000005811 Viola adunca Nutrition 0.000 claims description 2
- 240000009038 Viola odorata Species 0.000 claims description 2
- 235000013487 Viola odorata Nutrition 0.000 claims description 2
- 235000002254 Viola papilionacea Nutrition 0.000 claims description 2
- 239000000975 dye Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 239000012670 alkaline solution Substances 0.000 description 1
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 1
- 229910052601 baryte Inorganic materials 0.000 description 1
- 239000010428 baryte Substances 0.000 description 1
- -1 for example Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung eines Azofarbstoffesr Gegenstand dieses Zusatzpatentes ist ein Verfahren zur Darstellung eines Azofarb- stoffes, dadurch gekennzeichnet, dass man 2-Amirio-4-benzoylamino-l-anisol dianotiert und die Diazolösung mit 2 # 3-Oxynaphthoe- säure-p-naphthylamid kuppelt.
Der Farbstoff lässt sich sowohl in Sub stanz wie auf Substraten erzeugen. Er bildet ein dunkelrotes Pulver, das sich mit blau violetter Farbe in konzentrierter Schwefel säure löst. Auf Baumwolle erzeugt entsteht eine schöne bordeauxrote Färbung von aus gezeichneten Echtheitseigenschaften.
Beispiel: 242 Gewichtsteile 2-Amino-4-benzoylamino- 1-anisol werden mit 70 Gewichtsteilen Na triumnitrit in üblicher Weise dianotiert und die Diazolösung reit einer alkalischen Auf lösung von 313 Gewichtsteilen 2 # 3-Oxy- rraphthoesä(ire-ss-naphthylamid mit oder ohne Zusatz eines Substrates wie z. B. Schwerspat gekuppelt. Der bordeauxrote Niederschlag kann abfiltriert, gewaschen und getrocknet werden.
Process for the preparation of an azo dye The subject of this additional patent is a process for the preparation of an azo dye, characterized in that 2-amirio-4-benzoylamino-1-anisole is dianotized and the diazo solution with 2 # 3-oxynaphthoic acid-p-naphthylamide clutch.
The dye can be produced both in substance and on substrates. It forms a dark red powder that dissolves in concentrated sulfuric acid with a blue-violet color. Produced on cotton, a beautiful burgundy color with excellent fastness properties is created.
Example: 242 parts by weight of 2-amino-4-benzoylamino-1-anisole are dianotized with 70 parts by weight of sodium nitrite in the usual way and the diazo solution is an alkaline solution of 313 parts by weight of 2 # 3-oxyrraphthoesä (ire-ss-naphthylamide with or coupled without the addition of a substrate such as, for example, barite The burgundy precipitate can be filtered off, washed and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE116276X | 1924-03-29 | ||
| CH114916T | 1925-03-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH116276A true CH116276A (en) | 1926-08-16 |
Family
ID=29402936
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH116276D CH116276A (en) | 1924-03-29 | 1925-03-24 | Process for the preparation of an azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH116276A (en) |
-
1925
- 1925-03-24 CH CH116276D patent/CH116276A/en unknown
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