CH116744A - Process for the production of a new dye. - Google Patents

Process for the production of a new dye.

Info

Publication number
CH116744A
CH116744A CH116744DA CH116744A CH 116744 A CH116744 A CH 116744A CH 116744D A CH116744D A CH 116744DA CH 116744 A CH116744 A CH 116744A
Authority
CH
Switzerland
Prior art keywords
new dye
production
acid
brown
nitro
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH116744A publication Critical patent/CH116744A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/06Monoazo dyes prepared by diazotising and coupling from coupling components containing amino as the only directing group
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/06Monoazo dyes prepared by diazotising and coupling from coupling components containing amino as the only directing group
    • C09B29/095Amino naphthalenes
    • C09B29/0955Amino naphthalenes containing water solubilizing groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Heat Sensitive Colour Forming Recording (AREA)
  • Coloring (AREA)
  • Paper (AREA)

Description

  

  Zusatzpatent zum Hauptpatent     Nr.   <B>110287.</B>         Terfaln-en    zur Herstellung eines neuen     Farbstoffes.       Es wurde gefunden,     dass    man einen neuen  Farbstoff erhält, wenn man     diazotierte        6-          Nitro-2-a.mino-l-phenol-4-karbonsä,ure    mit     3-          Aminonaplithalin-1,8-dikarbonsnure    vereinigt.  Der neue Farbstoff bildet ein braunes Pul  ver, das sieh in Wasser und in Schwefelsäure  mit     rotbrauner    Farbe löst.

   Er färbt Wolle  aus saurem Bade in     rötlichbraunen    Tönen,  welche beim     Nachehromieren    nach     gelbolive     umschlagen.  



  <I>Beispiel:</I>  <B>10,7</B> Teile     3-Aminonaplitlia.lin-1,8-dikar-          bonsäureanhydrid    werden mit Hilfe von<B>10</B>  Teilen<B>30</B>     '/oiger    Natronlauge in<B>150</B> Teilen  Wasser heiss gelöst, mit<B>10</B> Teilen Soda ver  setzt, abgekühlt und mit der aus<B>9,9</B> Teilen       6-Nitro-2-amine-l-phene,1-4-karbonsä,ure    her-    gestellten     Diazoverbindung    versetzt. Nach  erfolgter Kupplung wird     der-Farbstoff        aus-          gesalzen,    filtriert und getrocknet



  Additional patent to main patent no. <B> 110287. </B> Terfaln-en for the production of a new dye. It has been found that a new dye is obtained if diazotized 6-nitro-2-a.mino-1-phenol-4-carboxylic acid is combined with 3-aminonaplithalin-1,8-dicarboxylic acid. The new dye forms a brown powder that dissolves in water and sulfuric acid with a red-brown color.

   He dyes wool from an acid bath in reddish-brown tones, which turn to yellow olive when re-homing.



  <I> Example: </I> <B> 10.7 </B> parts of 3-aminonaplitlia.lin-1,8-dicarboxylic acid anhydride are converted into <B> 10 </B> parts <B> 30 </B> '/ above sodium hydroxide solution dissolved in <B> 150 </B> parts of hot water, mixed with <B> 10 </B> parts of soda, cooled and mixed with the <B> 9.9 </ B > Parts of 6-nitro-2-amine-l-phene, 1-4-carboxylic acid, added diazo compound. After coupling has taken place, the dye is salted out, filtered and dried

 

Claims (1)

PATENTANSPRUCH <B>-:</B> Verfahren zur Herstellung eines neuen Farbstoffes, dadurch gekennzeichnet, dass man diazotierte 6-Nitro-2-amino-l-phenol-4- karbonsäure mit 3-Aminonaplithalin-1,8-di- karbonsäure vereinigt. Der neue Farbstoff bildet ein braunes Pulver, das sich in Was ser und in Schwefelsäure mit rotbrauner Farbe löst. Er färbt Wolle aus saurem Bade in rötlichbraunen Tönen, welche beim Nach- chromieren nach gelbolive umschlagen. PATENT CLAIM <B> -: </B> Process for the production of a new dye, characterized in that diazotized 6-nitro-2-amino-1-phenol-4-carboxylic acid is mixed with 3-aminonaplithalin-1,8-dicarboxylic acid united. The new dye forms a brown powder that dissolves in water and sulfuric acid with a red-brown color. It dyes wool from an acid bath in reddish-brown tones, which turn to yellow-olive when chromed.
CH116744D 1923-12-28 1924-08-16 Process for the production of a new dye. CH116744A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH110287T 1923-12-28
CH116744T 1924-08-16

Publications (1)

Publication Number Publication Date
CH116744A true CH116744A (en) 1926-09-16

Family

ID=25707693

Family Applications (1)

Application Number Title Priority Date Filing Date
CH116744D CH116744A (en) 1923-12-28 1924-08-16 Process for the production of a new dye.

Country Status (1)

Country Link
CH (1) CH116744A (en)

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