CH140914A - Process for the preparation of 4- (di- (oxyethyl)) - amino-1-oxybenzene-2-carboxylic acid. - Google Patents

Process for the preparation of 4- (di- (oxyethyl)) - amino-1-oxybenzene-2-carboxylic acid.

Info

Publication number
CH140914A
CH140914A CH140914DA CH140914A CH 140914 A CH140914 A CH 140914A CH 140914D A CH140914D A CH 140914DA CH 140914 A CH140914 A CH 140914A
Authority
CH
Switzerland
Prior art keywords
oxybenzene
amino
carboxylic acid
preparation
oxyethyl
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH140914A publication Critical patent/CH140914A/en

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Darstellung von     4-[Di-(ogyäthyl)]-amino-l-ogybenzol-2-earbonsänre.       Nach dem Verfahren des Zusatzpatentes  <B>139366</B> gewinnt man     4-[Di-(oxyäthyl)]-amitio-          1-oxybenzol-2-oarbonsäure    durch Kondensation  von     4-Amino-l-oxybenzol-2-carbonsäure    mit  einem     Halogenhydrin    des     Glykols.     



  Wie gefunden wurde, erhält man die  gleiche Verbindung, wenn man 1     Mol.        4-          Amino-l-oxybenzol-2-carbonsäure    mit 2     Mol.          Athylenoxyd    umsetzt.  



  <I>Beispiel:</I>  In eine Aufschlämmung von 153 Teilen       4-Amino-l-oxybenzol-2-carbonsäure    in 1000  Teilen Wasser und 50 Teilen einer     10-          normalen        Natriumhydroxydlösung    leitet man         Äthylenoxyd    ein, bis die     4-[Di-(oxyäthyl)]-          amino-l-oxybenzol-2-carbonsäure    gebildet ist.  Die Aufarbeitung erfolgt in der in der Patent  schrift     139366    beschriebenen Weise.



  Process for the preparation of 4- [di- (ogyäthyl)] - amino-l-ogybenzene-2-earbonsänre. According to the process of the additional patent <B> 139366 </B>, 4- [di- (oxyethyl)] -amitio- 1-oxybenzene-2-carboxylic acid is obtained by condensation of 4-amino-1-oxybenzene-2-carboxylic acid with a Glycol halohydrin.



  It has been found that the same compound is obtained if 1 mole of 4-amino-1-oxybenzene-2-carboxylic acid is reacted with 2 moles of ethylene oxide.



  <I> Example: </I> Ethylene oxide is introduced into a slurry of 153 parts of 4-amino-1-oxybenzene-2-carboxylic acid in 1000 parts of water and 50 parts of a 10 normal sodium hydroxide solution until the 4- [di- (oxyäthyl)] - amino-1-oxybenzene-2-carboxylic acid is formed. The work-up is carried out in the manner described in Patent 139366.

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung von 4-[Di-(oxy- äthyl)j-amino-l-oxybenzol-2-carbonsäure, da durch gekennzeichnet, dass man 1 Mol. 4 Amino-l-oxybenzol-2-carbonsäure mit 2 112o1. Äthylenoxyd umsetzt. PATENT CLAIM: Process for the preparation of 4- [di- (oxy-ethyl) j-amino-1-oxybenzene-2-carboxylic acid, characterized in that 1 mol. 4 amino-1-oxybenzene-2-carboxylic acid with 2 112o1 . Ethylene oxide converts.
CH140914D 1927-11-12 1928-09-27 Process for the preparation of 4- (di- (oxyethyl)) - amino-1-oxybenzene-2-carboxylic acid. CH140914A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE140914X 1927-11-12
CH136381T 1928-05-08

Publications (1)

Publication Number Publication Date
CH140914A true CH140914A (en) 1930-06-30

Family

ID=25712688

Family Applications (1)

Application Number Title Priority Date Filing Date
CH140914D CH140914A (en) 1927-11-12 1928-09-27 Process for the preparation of 4- (di- (oxyethyl)) - amino-1-oxybenzene-2-carboxylic acid.

Country Status (1)

Country Link
CH (1) CH140914A (en)

Similar Documents

Publication Publication Date Title
CH140915A (en) Process for the preparation of 4- (oxyethyl) -amino-1-oxybenzene-2-carboxylic acid.
DE938614C (en) Process for the production of methyltrimethylolmethane
AT123851B (en) Process for the preparation of monooxy-ω-alkylaminoacetophenones.
CH140917A (en) Process for the preparation of 4- (oxyethyl) -amino-3-methyl-1-oxybenzene.
AT88646B (en) Process for the production of tanning substances.
AT155802B (en) Process for the preparation of formaldehyde sodium sulfoxylates from arsenobenzene compounds.
AT128869B (en) Process for the preparation of oxyacylaminoarsenobenzenes.
DE1029820B (en) Process for the production of water-soluble stable condensation products from urea, thiourea or their derivatives and formaldehyde
CH162658A (en) Process for the preparation of the sodium salt of an arsenic complex compound of catechinaric acid.
CH139990A (en) Process for the preparation of 2-chloro-4- (oxyethyl) -amino-1-oxybenzene.
CH236163A (en) Process for the production of a polyether.
CH133686A (en) Process for the preparation of 2-oxynaphthalene-3-carboxylic acid-4&#39;-chlorophenylamide.
CH204701A (en) Process for the production of a condensation product.
CH212352A (en) Process for the preparation of 3- (bis-dioxypropyl) -amino-4-oxy-3&#39;-amino-4&#39;-oxy-arsenobenzene-monoformaldehyde-sodium sulfoxylate.
CH212567A (en) Process for the preparation of a new pyridinium compound.
CH180883A (en) Method of creating a therapeutically valuable compound.
CH192068A (en) Process for the preparation of a 3- (dioxypropyl-oxyethyl) -amino-4-oxy-3&#39;-amino-4&#39;-oxyarsenobenzene sulfoxylate.
CH193467A (en) Process for the preparation of 3- (bis-dioxypropyl) -amino-4-oxy-5-acetylamino-3&#39;-dioxypropylamino-4&#39;-oxyarsenobenzene-formaldehyde sulfoxylate sodium.
CH139367A (en) Process for the preparation of 4- (oxyethyl) -amino-1-oxybenzene-2-carboxylic acid.
CH187362A (en) Process for the production of symm. Cyanuric acid di (2-methyl-4-aminoquinolyl-6) diamide.
CH135161A (en) Process for the preparation of isobutylallylbarbituric acid.
CH217133A (en) Process for the production of a water-soluble, higher molecular weight, α-substituted benzylamine derivative.
CH168725A (en) Process for the preparation of a new ester acid.
CH139366A (en) Process for the preparation of 4-di (oxyethyl) -amino-1-oxybenzene-2-carboxylic acid.
CH194876A (en) Process for the preparation of 2 (3 &#39;, 5&#39;-Diiodo-2&#39;-B-oxethyl-4&#39;-oxypheny) - 6-iodoquinoline-4-carboxylic acid.