CH146183A - Process for the preparation of a new monoazo dye. - Google Patents
Process for the preparation of a new monoazo dye.Info
- Publication number
- CH146183A CH146183A CH146183DA CH146183A CH 146183 A CH146183 A CH 146183A CH 146183D A CH146183D A CH 146183DA CH 146183 A CH146183 A CH 146183A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- red
- new
- monoazo dye
- dye
- Prior art date
Links
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 3
- 238000002360 preparation method Methods 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 3
- 210000002268 wool Anatomy 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- IIZVTIZJNOPLQM-UHFFFAOYSA-N CC(C1(N)OC2(C(C3=CC=CC=C3)=CC=CC2C)N)C=CC=C1C1=CC=CC=C1 Chemical compound CC(C1(N)OC2(C(C3=CC=CC=C3)=CC=CC2C)N)C=CC=C1C1=CC=CC=C1 IIZVTIZJNOPLQM-UHFFFAOYSA-N 0.000 claims 1
- 239000000243 solution Substances 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Coloring (AREA)
Description
Verfahren zur Darstellung eines neuen Monoazofarbstoffes. Es wurde gefunden, dass man einen neuen wertvollen Monoazofarbstoff erhält, -wenn man diazotierten o-Aminophenyl-o-tolylätlier mit p-Toluolsulfo-l-amino,8-naplitol-3,6-di- sulfosäure kombiniert, Der neue Farbstoff stellt *ein rotes Pulver dar, welches in Was ser mit blauroter, in konzentrierter Schwefel säure mit violetter Farbe löslich ist. Er färbt auf Wolle und Seide ein sehr klares Blaurot von sehr guter Licht- und Walkechtheit.
<I>Beispiel:</I> Die aus<B>19,9 kg</B> o-Aminophenyl-o-toly!- ätlier auf gewöhnlichem Wege erhaltene Diazolösung lässt man in eine wässerige Lö- sung von---4Z,3 <B>kg</B> p-Toluolsulfo-l-amino-8- naphtol-3,.6-disulf6eure.und <B>30 kg</B> Natrium- aeetat bei<B>0</B> bis<B>5'</B> einlauf'eü--Du:
#ch Zugabe von Sodalösung wird allmählich neutr-ali-ner-t- Nach <B>6</B> bis 8stündigein Rühren ist die Kupp- lung beendet. Es wird aufgewärmt, ausgesal- zen, filtriert und getrocknet. Der erhaltene Farbstoff bildet ein rotes Pulver, das in Schwefelsäure mit violetter Farbe löslich ist. Er färbt auf Wolle und Seide ein sehr klares Blaurot von sehr guter Licht- und Walkecht- heit.
Process for the preparation of a new monoazo dye. It has been found that a new valuable monoazo dye is obtained -if one combines diazotized o-aminophenyl-o-tolylätlier with p-toluenesulfo-l-amino, 8-naplitol-3,6-disulfonic acid, The new dye provides * a red powder, which is soluble in water with a blue-red color, in concentrated sulfuric acid with a purple color. It dyes wool and silk a very clear blue-red with very good light and milled fastness.
<I> Example: </I> The diazo solution obtained in the usual way from <B> 19.9 kg </B> o-aminophenyl-o-toly! - is immersed in an aqueous solution of --- 4Z , 3 <B> kg </B> p-toluenesulfo-1-amino-8-naphthol-3, 6-disulf6eure. And <B> 30 kg </B> sodium acetate at <B> 0 </ B > to <B> 5 '</B> einlauf'eü - you:
#ch addition of soda solution gradually becomes neutral-ali-ner-after <B> 6 </B> to 8 hours of stirring, the coupling is ended. It is warmed up, salted out, filtered and dried. The dye obtained forms a red powder which is soluble in sulfuric acid with a purple color. It dyes wool and silk a very clear blue-red with very good lightfastness and millfastness.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR146183X | 1928-10-15 | ||
| CH143989T | 1929-09-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH146183A true CH146183A (en) | 1931-03-31 |
Family
ID=25714385
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH146183D CH146183A (en) | 1928-10-15 | 1929-09-13 | Process for the preparation of a new monoazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH146183A (en) |
-
1929
- 1929-09-13 CH CH146183D patent/CH146183A/en unknown
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