CH191424A - Process for the preparation of a monoazo dye. - Google Patents
Process for the preparation of a monoazo dye.Info
- Publication number
- CH191424A CH191424A CH191424DA CH191424A CH 191424 A CH191424 A CH 191424A CH 191424D A CH191424D A CH 191424DA CH 191424 A CH191424 A CH 191424A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- monoazo dye
- acetylamino
- dye
- new
- Prior art date
Links
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 title 1
- 239000000975 dye Substances 0.000 claims description 4
- 239000000987 azo dye Substances 0.000 claims description 2
- 239000004305 biphenyl Substances 0.000 claims description 2
- 239000000835 fiber Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 125000004494 ethyl ester group Chemical group 0.000 claims 1
- TWLLPUMZVVGILS-UHFFFAOYSA-N Ethyl 2-aminobenzoate Chemical compound CCOC(=O)C1=CC=CC=C1N TWLLPUMZVVGILS-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- XONPDZSGENTBNJ-UHFFFAOYSA-N molecular hydrogen;sodium Chemical compound [Na].[H][H] XONPDZSGENTBNJ-UHFFFAOYSA-N 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/32—Monoazo dyes prepared by diazotising and coupling from coupling components containing a reactive methylene group
- C09B29/33—Aceto- or benzoylacetylarylides
- C09B29/335—Aceto- or benzoylacetylarylides free of acid groups
- C09B29/337—Carbocyclic arylides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines Honoazofarbstoffes. Es wurde gefunden, dass man einen neuen Azofarbstoff erhält, wenn man diazotierten 1- Aminobenzol-2-carbonsäure-äthylester mit 4- Acetylamino-4'- acetoacetylamino - 3 . 3'- dime- thyl-diphenyl vereinigt. Der neue Farbstoff bildet ein gelbes Pulver. Auf der Faser oder andern Substraten hergestellt, färbt er diese in reinen grüngelben Tönen an.
<I>Beispiel:</I> 16,5 Teile 1-Aminobenzol-2-carbonsäure- äthylester werden wie üblich diazotiert und in eine Lösung von 33,8 Teilen 4-Acetyl- amino-4'- acetoacetylamino.3 . 3'- dimethyl -di- phenyl, 100 Teilen Natriumhydrogydlösung, 15 Teilen Soda und 2000 Teilen Wasser ein- getragen. Der gebildete Farbstoff fällt sofort aus. Er wird filtriert und getrocknet.
Process for the preparation of a honoazo dye. It has been found that a new azo dye is obtained if diazotized 1-aminobenzene-2-carboxylic acid ethyl ester with 4-acetylamino-4'-acetoacetylamino-3. 3'-dimethyl-diphenyl combined. The new dye forms a yellow powder. Produced on the fiber or other substrates, he stains them in pure green-yellow tones.
<I> Example: </I> 16.5 parts of 1-aminobenzene-2-carboxylic acid ethyl ester are diazotized as usual and converted into a solution of 33.8 parts of 4-acetylamino-4'-acetoacetylamino. 3. 3'-dimethyldiphenyl, 100 parts of sodium hydrogen solution, 15 parts of soda and 2000 parts of water are introduced. The dye formed precipitates immediately. It is filtered and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH187691T | 1934-07-21 | ||
| CH191424T | 1934-07-21 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH191424A true CH191424A (en) | 1937-06-15 |
Family
ID=25721563
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH191424D CH191424A (en) | 1934-07-21 | 1934-07-21 | Process for the preparation of a monoazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH191424A (en) |
-
1934
- 1934-07-21 CH CH191424D patent/CH191424A/en unknown
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