CH198317A - Process for the preparation of a monoazo dye. - Google Patents
Process for the preparation of a monoazo dye.Info
- Publication number
- CH198317A CH198317A CH198317DA CH198317A CH 198317 A CH198317 A CH 198317A CH 198317D A CH198317D A CH 198317DA CH 198317 A CH198317 A CH 198317A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- monoazo dye
- chlorobenzoyl
- dye
- amido
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Substances C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
- C09B29/28—Amino naphthols
- C09B29/30—Amino naphtholsulfonic acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. 189141. Verfahren zur Darstellung eines RonoazofarbstoffAs. Das vorliegende Patent betrifft ein Ver fahren zur Darstellung eines Monoazofarb- stoffes und ist dadurch gekennzeichnet, dass man 4-(N-o-Chlorbenzoyl-N-benzyl)-amido-l- amidobenzol dianotiert und mit N-o-Chlor- benzoyl-r-säU-re kuppelt.
<I>Beispiel:</I> 33,7 Teile 4-(N-o-Chlorbenzoyl-N-benzyl)- amido-l-amidobenzol werden mit 6,9 Teilen Nitrit und 25 Teilen Salzsäure dianotiert und in Gegenwart von überschüssigem Natrium acetat mit 37,8 Teilen N-o-Chlorbenzoyl-r- säure gekuppelt. Die Kupplung kann auch in Gegenwart von Natriumbicarbonat oder ähnlich schwachwirkenden Neutralisationsmitteln vor genommen werden.
Der isolierte und getrocknete Farbstoff stellt ein rotes Pulver dar und färbt Wolle und Seide in lebhaften roten Tönen.
Patent amendment to main patent No. 189141. Process for the preparation of a ronoazo dye As. The present patent relates to a method for the preparation of a monoazo dye and is characterized in that 4- (No-chlorobenzoyl-N-benzyl) -amido-l-amidobenzene is dianotated and with No-chlorobenzoyl-r-acid re clutch.
<I> Example: </I> 33.7 parts of 4- (no-chlorobenzoyl-N-benzyl) - amido-l-amidobenzene are dianotized with 6.9 parts of nitrite and 25 parts of hydrochloric acid and in the presence of excess sodium acetate 37.8 parts of no-chlorobenzoyl-acid coupled. The coupling can also be carried out in the presence of sodium bicarbonate or similar weak neutralizing agents.
The isolated and dried dye is a red powder and dyes wool and silk in vivid red tones.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH198317T | 1937-03-18 | ||
| CH189141T | 1937-03-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH198317A true CH198317A (en) | 1938-06-15 |
Family
ID=25721755
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH198317D CH198317A (en) | 1937-03-18 | 1937-03-18 | Process for the preparation of a monoazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH198317A (en) |
-
1937
- 1937-03-18 CH CH198317D patent/CH198317A/en unknown
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