CH200069A - Process for the production of a condensation product. - Google Patents
Process for the production of a condensation product.Info
- Publication number
- CH200069A CH200069A CH200069DA CH200069A CH 200069 A CH200069 A CH 200069A CH 200069D A CH200069D A CH 200069DA CH 200069 A CH200069 A CH 200069A
- Authority
- CH
- Switzerland
- Prior art keywords
- condensation product
- production
- nitro
- yellow
- aniline
- Prior art date
Links
- 239000007859 condensation product Substances 0.000 title claims description 6
- 238000000034 method Methods 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title description 3
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 3
- 239000013078 crystal Substances 0.000 claims description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 3
- NKJIFDNZPGLLSH-UHFFFAOYSA-N 4-nitrobenzonitrile Chemical compound [O-][N+](=O)C1=CC=C(C#N)C=C1 NKJIFDNZPGLLSH-UHFFFAOYSA-N 0.000 claims 1
- 239000000975 dye Substances 0.000 claims 1
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines Kondensationsproduktes. Es wurde gefunden, dass. man durcli Ko-n- densation von 1-Halagen-2-nitro-4-eyauben- zolen mit aromatisclien Aminen Konden sationsprodukte der Diphenylaminreilie er hält, #die sieh insbasondere zum Färben von Lacken, und zum Färben und Dru-,ken,
von Acetatseide eignen. Man erhält auf Aoetat- seide lebhaft grünstichig-gelbe bis orange Farbtöne von hervorragender Lichtechtheit.
vorliegendes Patent bezieht sieh nun auf eiii Verfahren. zur Herstellung eines Konden sationsproduktes, dadurch gekennzeichnet, .dass man 1-Clilor-2-nitro-4-eyauben#z#ol mit Anilin kondensiert.
Dast, so erhaltene 2-Nitro-4-eyandiplienyl- amin kristallisiert aus Methanel. in gelben Kristallen vom Smp. <B>126</B> 'bis<B>127 '</B> und f #Lrbt und #druckt Acotateei-cle in gelben Tönen von Uervorragünder Liehteahtheit. <I>Beispiel:
</I> <B>18,5</B> Teile l#Chl#o#r-,2#-nitro-4-eyaubenzol werden mit etwa 120 Teilen Alkohol und 20 Teilen Anilin mehrere Stunden. unter Rück- flusskühlung zum Sieden erhitzt. Beim Er halten sssheidet sich das gebildete Konden sationsprodukt in gelben Kristallen aus.
Process for the production of a condensation product. It has been found that condensation products of the diphenylamine range are obtained by co-condensation of 1-Halagen-2-nitro-4-eyaubenzolen with aromatic amines, # which are particularly useful for coloring lacquers, and for dyeing and Printing,
of acetate silk are suitable. Vivid greenish-yellow to orange shades of excellent lightfastness are obtained on acetate silk.
This patent now relates to a process. for the production of a condensation product, characterized in that 1-Clilor-2-nitro-4-eyauben # z # ol is condensed with aniline.
The 2-nitro-4-eyandiplienylamine thus obtained crystallizes from Methanel. in yellow crystals from m.p. <B> 126 </B> 'to <B> 127' </B> and colors and #prints Acotateei-cle in yellow tones by Vorvorvoründer Liehteahtheit <I> example:
</I> <B> 18.5 </B> parts of l # Chl # o # r-, 2 # -nitro-4-eyaubenzol are mixed with about 120 parts of alcohol and 20 parts of aniline for several hours. heated to boiling under reflux cooling. When it is held, the condensation product formed separates out in yellow crystals.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE200069X | 1936-08-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH200069A true CH200069A (en) | 1938-09-30 |
Family
ID=5759226
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH200069D CH200069A (en) | 1936-08-28 | 1937-08-11 | Process for the production of a condensation product. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH200069A (en) |
-
1937
- 1937-08-11 CH CH200069D patent/CH200069A/en unknown
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