CH200527A - Process for the preparation of an acidic wool azo dye. - Google Patents

Process for the preparation of an acidic wool azo dye.

Info

Publication number
CH200527A
CH200527A CH200527DA CH200527A CH 200527 A CH200527 A CH 200527A CH 200527D A CH200527D A CH 200527DA CH 200527 A CH200527 A CH 200527A
Authority
CH
Switzerland
Prior art keywords
azo dye
wool
preparation
acidic
acidic wool
Prior art date
Application number
Other languages
German (de)
Inventor
I. G. Farbenindustrie Aktiengesellschaft
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH200527A publication Critical patent/CH200527A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/24Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
    • C09B29/28Amino naphthols
    • C09B29/30Amino naphtholsulfonic acid
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/34Monoazo dyes prepared by diazotising and coupling from other coupling components
    • C09B29/36Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds
    • C09B29/3604Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom
    • C09B29/3647Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms
    • C09B29/3652Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles
    • C09B29/366Monoazo dyes prepared by diazotising and coupling from other coupling components from heterocyclic compounds containing only a nitrogen as heteroatom containing a five-membered ring with two nitrogen atoms as heteroatoms containing a 1,2-diazoles or hydrogenated 1,2-diazoles containing hydroxy-1,2-diazoles, e.g. pyrazolone

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Verfahren zur Herstellung eines sauren     Wollazofarbstoffes.       Vorliegendes Patent bezieht sich auf ein  Verfahren zur Herstellung     eines    sauren       W        ollazofarbstoffes,    dadurch gekennzeichnet,  dass. man     diazotiertes        1-(N-Aoetyl-s,ec.-.butyl-          amino)-4-aminobenzol    in     essigsaurem        Me-          dium    mit     2,-Ben7,oylamino-5-naphthol-7=sul-          f        onsäure    kuppelt.  



  Der so erhaltene Farbstoff     bildet    nach  dem Trocknen ein gelbrotes, wasserlösliches       Pulver    und färbt Wolle und     Seide    in     leuch-          tend    orangen Tönen von sehr gutem     E.gadi-          siervermögen    und guten     Echtheitseigen-          schaften.     



  <I>Beispiel:</I>  20,6 Teile     1-(N-Acetyl-sec.-butylamino)-          4-aminobenza1    werden in der üblichen     Weise          diazotiert.    Die erhaltene     Diazolösung    lässt  man in eine mit überschüssigem     Natrium-          aoetat        versetzte    Lösung von 3,6 Teilen       2-Benzoylamino-5-naphthol-7-sulfonsäure    ein-         laufen.    Nach     beendeter        Kupplung        wird        der     Farbstoff abgeschieden und getrocknet.



  Process for the preparation of an acidic wool azo dye. The present patent relates to a process for the production of an acidic wool azo dye, characterized in that diazotized 1- (N-aoetyl-s, ec .-. Butyl-amino) -4-aminobenzene in acetic acid medium with 2, -Ben7, oylamino-5-naphthol-7 = sulphonic acid.



  The dyestuff obtained in this way forms a yellow-red, water-soluble powder after drying and dyes wool and silk in bright orange shades with very good E.gadizability and good fastness properties.



  <I> Example: </I> 20.6 parts of 1- (N-acetyl-sec.-butylamino) -4-aminobenza1 are diazotized in the usual way. The diazo solution obtained is allowed to run into a solution of 3.6 parts of 2-benzoylamino-5-naphthol-7-sulfonic acid to which excess sodium acetate has been added. When the coupling is complete, the dye is deposited and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines sauren Wollazofarbstoffes, dadurch gekennzeichnet, ,dass@ man idiazotiertes 1-(N-Aoetyl-sec.-butyl- amäno)-4-aminobenzol in essigsaurem Me dium mit 2-Benzoylamino-5-naphthol-7-sul- fonsäure kuppelt. PATENT CLAIM: Process for the production of an acidic wool azo dye, characterized in that @ one idiazotized 1- (N-aoetyl-sec.-butyl-amano) -4-aminobenzene in acetic acid medium with 2-benzoylamino-5-naphthol-7- sulphonic acid couples. Der so erhaltene Farbstoff bildet nach dem Trocknen ein gelbrotes, wasserlösliches Pulver und färbt Wolle und Seide in leuch tend orangen Tönen von sehr gutem EgaJs- siervermögen und guten Echtheitseigen- schaften. The dye obtained in this way forms a yellow-red, water-soluble powder after drying and dyes wool and silk in bright orange shades with very good gasifying power and good fastness properties.
CH200527D 1935-10-02 1936-09-17 Process for the preparation of an acidic wool azo dye. CH200527A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE200527X 1935-10-02
CH195654T 1936-09-17

Publications (1)

Publication Number Publication Date
CH200527A true CH200527A (en) 1938-10-15

Family

ID=25722777

Family Applications (1)

Application Number Title Priority Date Filing Date
CH200527D CH200527A (en) 1935-10-02 1936-09-17 Process for the preparation of an acidic wool azo dye.

Country Status (1)

Country Link
CH (1) CH200527A (en)

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