CH200980A - Process for the preparation of a quaternary nitrogen compound. - Google Patents

Process for the preparation of a quaternary nitrogen compound.

Info

Publication number
CH200980A
CH200980A CH200980DA CH200980A CH 200980 A CH200980 A CH 200980A CH 200980D A CH200980D A CH 200980DA CH 200980 A CH200980 A CH 200980A
Authority
CH
Switzerland
Prior art keywords
sep
preparation
nitrogen compound
quaternary nitrogen
mol
Prior art date
Application number
Other languages
German (de)
Inventor
Waldmann Dr Edmund
Chwala Dr August
Original Assignee
Waldmann Dr Edmund
Chwala Dr August
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Waldmann Dr Edmund, Chwala Dr August filed Critical Waldmann Dr Edmund
Publication of CH200980A publication Critical patent/CH200980A/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung einer     quaternären        Stiel;stoffverbindung.       Es wurde gefunden, dass man das bisher  noch nicht bekannte     1,3-Dibenzyl-2-heptade-          cylimidazolinintnehlorid    darstellen kann, wenn  man     Stearinsäure    mit einem Gemisch, be  stehend aus     '/z        Mol    N .     N'-Dibeiizyläthyleii-          diamin    und     1/q        11u1    N .     N'-Dibenzylätliyleti-          diamindihydrochlorid    bei 200-250   C um  setzt.

   Das gebildete Produkt stellt eine in  Wasser lösliche Masse dar; es soll als Tex  tilhilfsmittel     verwendet    werden.  



  <I>Beispiel:</I>  6 g     Stearinsäure,    2,5 g     Dibenzyläthylen-          diamin,    3;5 g     Dibenzylätbylendiamiiiliydi@o-          chlorid    werden innerhalb von etwa 40 Mi  nuten allmählich bis 230   C erhitzt, hierauf  wird die Temperatur in weiteren 10     Minuten     auf 240   C gesteigert und sodann während  30 Minuten auf 240-250   C gehalten.  Hierbei geht das Hydrochlorid in Lösung,    und man erhält das     1,3-Dibenzyl-2-heptade-          cyliinidazoliniumehlorid.     



  Das gebildete Produkt stellt eine in  Wasser lösliche     blasse    dar: es soll als     Teg-          tilltilfsmittel    verwendet werden.



  Method for producing a quaternary stem; fabric connection. It has been found that the hitherto unknown 1,3-dibenzyl-2-heptadecylimidazolinintnehlorid can be represented if stearic acid is mixed with a mixture consisting of '/ z mol N. N'-Dibeiizyläthyleii- diamine and 1 / q 11u1 N. N'-Dibenzylätliyleti- diamindihydrochlorid at 200-250 C to sets.

   The product formed is a mass soluble in water; it is intended to be used as a textile auxiliary.



  <I> Example: </I> 6 g of stearic acid, 2.5 g of dibenzylethylenediamine, 3; 5 g of dibenzylethylenediamiiiliydi @ o-chloride are gradually heated to 230 C over about 40 minutes, after which the temperature is increased for a further 10 Minutes to 240 ° C and then held at 240-250 ° C for 30 minutes. Here, the hydrochloride dissolves, and 1,3-dibenzyl-2-heptadecyliinidazolinium chloride is obtained.



  The product formed is a pale one which is soluble in water: it is intended to be used as a tegill aid.

Claims (1)

EMI0001.0026 PATENTANSPRUCH: <tb> Verfahren <SEP> zur <SEP> Herstellung <SEP> einer <SEP> quater nären <SEP> Stick,;toffverbiiiduiig, <SEP> dadurch <SEP> gekenn zeichnet, <SEP> dar <SEP> man <SEP> Stearinsäure <SEP> mit <SEP> einem <tb> Gemisch <SEP> aus <SEP> '/z <SEP> Mol <SEP> N <SEP> . <SEP> IlT'-Dibettzyläthylen dIamin <SEP> und <SEP> '/z <SEP> Mol <SEP> N <SEP> . <SEP> N'-Dibenzyläthylen diamindihydrochlorid <SEP> bei <SEP> \?00-250 <SEP> <SEP> C <SEP> um setzt. <tb> Das <SEP> gebildete <SEP> 1,3 <SEP> Dibenzyl.2-heptadeeyl imidazoliniumehlorid <SEP> stellt <SEP> eine <SEP> in <SEP> Wasser <tb> lösliche <SEP> Masse <SEP> dar; <SEP> es <SEP> soll <SEP> als <SEP> Teatilhilfs tnittel <SEP> verwendet <SEP> werden. EMI0001.0026 PATENT CLAIM: <tb> Method <SEP> for <SEP> production <SEP> a <SEP> quater när <SEP> stick,; toffverbiiiduiig, <SEP> marked with <SEP>, <SEP> represents <SEP> man <SEP> Stearic acid <SEP> with <SEP> one <tb> Mixture <SEP> from <SEP> '/ z <SEP> mol <SEP> N <SEP>. <SEP> IlT'-Dibettzyläthylendiamine <SEP> and <SEP> '/ z <SEP> Mol <SEP> N <SEP>. <SEP> N'-dibenzylethylene diamine dihydrochloride <SEP> at <SEP> \? 00-250 <SEP> <SEP> C <SEP>. <tb> The <SEP> formed <SEP> 1,3 <SEP> dibenzyl.2-heptadeeyl imidazolinium chloride <SEP> represents <SEP> a <SEP> in <SEP> water <tb> is soluble <SEP> mass <SEP>; <SEP> it <SEP> should <SEP> be used as <SEP> auxiliary device <SEP> <SEP>.
CH200980D 1936-07-29 1937-07-28 Process for the preparation of a quaternary nitrogen compound. CH200980A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AT200980X 1936-07-29

Publications (1)

Publication Number Publication Date
CH200980A true CH200980A (en) 1938-11-15

Family

ID=3669162

Family Applications (1)

Application Number Title Priority Date Filing Date
CH200980D CH200980A (en) 1936-07-29 1937-07-28 Process for the preparation of a quaternary nitrogen compound.

Country Status (1)

Country Link
CH (1) CH200980A (en)

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