CH208132A - Process for the production of a new, nitrogen-containing organic compound. - Google Patents
Process for the production of a new, nitrogen-containing organic compound.Info
- Publication number
- CH208132A CH208132A CH208132DA CH208132A CH 208132 A CH208132 A CH 208132A CH 208132D A CH208132D A CH 208132DA CH 208132 A CH208132 A CH 208132A
- Authority
- CH
- Switzerland
- Prior art keywords
- new
- production
- nitrogen
- organic compound
- containing organic
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- -1 nitrogen-containing organic compound Chemical class 0.000 title claims description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 239000000975 dye Substances 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 239000004753 textile Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C275/46—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups containing any of the groups, X being a hetero atom, Y being any atom, e.g. acylureas
- C07C275/48—Y being a hydrogen or a carbon atom
- C07C275/50—Y being a hydrogen or an acyclic carbon atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung einer neuen, organischen Verbindung. Die Erfindung bezieht sich auf ein Ver fahren zur Herstellung einer neuen, stickstoff haltigen organischen Verbindung, geeignet, um zelluloseartigen Textilmaterialien Affinität für Säurewollfarbstoffe zu erteilen.
Gemäss der Erfindung wird Allophano- methyldimethyl - cyclohexylammoniumchlorid der Formel
EMI0001.0011
erhalten, indem Chloroaoetylharnstoff ver anlasst wird, sich mit Dimethylcyelohexämin zu verbinden.
Wenn gewünscht, kann die Reaktion in Gegenwart eines Lösungs- oder Verdünnungs mittels, z. B. Alkohol, durchgeführt werden. <I>Beispiel:</I> 20 Teile Ohloroacetylharnstoff, 20 Teile Dymethyleyclohexylamin und 100 Teile Äthanol werden zusammen unter Rückfluss- kühlung während fünf Stunden erhitzt. Es bildet sich eine klare Lösung. Der Alkohol wird hierauf bei Unterdruck abdestilliert. Es verbleibt eine viskose, gelbe, an der Atmo sphäre zerfliessende,- ölige Masse, welche beim Stehen langsam Kristalle niederschlägt.
Es ist dies die neue Verbindung, Allophano- methyldimethyl- cyclohexylammoniumchlorid. Sie ist sehr leicht in Wasser löslich, lösbar in heissem Alkohol und in Äther, Azeton und Benzol unlöslich.
Process for the production of a new, organic compound. The invention relates to a process for the production of a new, nitrogen-containing organic compound, suitable for giving cellulosic textile materials an affinity for acid wool dyes.
According to the invention, allophanomethyldimethyl-cyclohexylammonium chloride is of the formula
EMI0001.0011
obtained by causing chloroaoetylurea ver to combine with dimethylcyelohexaemine.
If desired, the reaction can be carried out in the presence of a solvent or diluent, e.g. B. alcohol. <I> Example: </I> 20 parts of ohloroacetylurea, 20 parts of dymethyleyclohexylamine and 100 parts of ethanol are heated together under reflux for five hours. A clear solution forms. The alcohol is then distilled off under reduced pressure. What remains is a viscous, yellow, oily mass that dissolves in the atmosphere and slowly precipitates crystals when standing.
This is the new compound, allophanomethyldimethylcyclohexylammonium chloride. It is very easily soluble in water, soluble in hot alcohol and insoluble in ether, acetone and benzene.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB207203X | 1937-06-18 | ||
| GB208132X | 1937-06-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH208132A true CH208132A (en) | 1939-12-31 |
Family
ID=33031450
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH207203D CH207203A (en) | 1937-06-18 | 1938-06-17 | Process for the production of a new, nitrogen-containing organic compound. |
| CH208132D CH208132A (en) | 1937-06-18 | 1938-06-17 | Process for the production of a new, nitrogen-containing organic compound. |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH207203D CH207203A (en) | 1937-06-18 | 1938-06-17 | Process for the production of a new, nitrogen-containing organic compound. |
Country Status (1)
| Country | Link |
|---|---|
| CH (2) | CH207203A (en) |
-
1938
- 1938-06-17 CH CH207203D patent/CH207203A/en unknown
- 1938-06-17 CH CH208132D patent/CH208132A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CH207203A (en) | 1939-10-15 |
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