CH210488A - Process for the preparation of a water-soluble monoazo dye. - Google Patents
Process for the preparation of a water-soluble monoazo dye.Info
- Publication number
- CH210488A CH210488A CH210488DA CH210488A CH 210488 A CH210488 A CH 210488A CH 210488D A CH210488D A CH 210488DA CH 210488 A CH210488 A CH 210488A
- Authority
- CH
- Switzerland
- Prior art keywords
- water
- preparation
- monoazo dye
- soluble monoazo
- dye
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 title claims description 3
- 238000002360 preparation method Methods 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 7
- BHAAPTBBJKJZER-UHFFFAOYSA-N p-anisidine Chemical compound COC1=CC=C(N)C=C1 BHAAPTBBJKJZER-UHFFFAOYSA-N 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
- C09B29/28—Amino naphthols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines wasserlöslichen 1Vlonoazofarbstofies. Gegenstand des vorliegenden Zusatz patentes ist ein Verfahren zur Herstellung eines wasserlöslichen Monoazofarbstoffes, welches dadurch gekennzeichnet ist, dass man diazotiertes 1-Amino-4-methoxybenzol in al kalischem Medium mit 2-Sulfomethylamino- 7-oxynaphthalin kuppelt.
Beispiel: 107 Gewichtsteile 1-Amino-4-methoxy- benzol werden wie üblich diazotiert und in Gegenwart von überschüssigem Natrium- carbonat mit einer wässrigen Lösung von 239 Gewichtsteilen 2-Sulfomethylamino-7-oxy- naphthalin unter Kühlung vereinigt. Der erhaltene Farbstoff wird ausgesalzen und ge trocknet.
Er stellt ein dunkelbraunes Pulver dar, das sich in Wasser mit roter Farbe löst und Wolle unter Kochtemperatur aus saufern Bade in braunroten Tönen gleichmässig durchfärbt.
Process for the preparation of a water-soluble 1-vlonoazo dye. The subject of the present additional patent is a process for the production of a water-soluble monoazo dye, which is characterized in that diazotized 1-amino-4-methoxybenzene is coupled in an alkaline medium with 2-sulfomethylamino-7-oxynaphthalene.
Example: 107 parts by weight of 1-amino-4-methoxybenzene are diazotized as usual and, in the presence of excess sodium carbonate, combined with an aqueous solution of 239 parts by weight of 2-sulfomethylamino-7-oxynaphthalene with cooling. The dye obtained is salted out and dried.
It is a dark brown powder that dissolves in water with a red color and evenly dyes wool from an acidic bath at boiling temperature in brown-red tones.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE210488X | 1937-03-24 | ||
| CH205165T | 1938-03-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH210488A true CH210488A (en) | 1940-07-15 |
Family
ID=25724147
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH210488D CH210488A (en) | 1937-03-24 | 1938-03-17 | Process for the preparation of a water-soluble monoazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH210488A (en) |
-
1938
- 1938-03-17 CH CH210488D patent/CH210488A/en unknown
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