CH227744A - Process for the preparation of a solid molecular compound containing mercury. - Google Patents
Process for the preparation of a solid molecular compound containing mercury.Info
- Publication number
- CH227744A CH227744A CH227744DA CH227744A CH 227744 A CH227744 A CH 227744A CH 227744D A CH227744D A CH 227744DA CH 227744 A CH227744 A CH 227744A
- Authority
- CH
- Switzerland
- Prior art keywords
- molecular compound
- solution
- compound
- preparation
- compound containing
- Prior art date
Links
- 150000001875 compounds Chemical class 0.000 title claims description 8
- 239000007787 solid Substances 0.000 title claims description 6
- 238000000034 method Methods 0.000 title claims description 5
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 title claims description 4
- 229910052753 mercury Inorganic materials 0.000 title claims description 4
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 claims description 6
- 239000000243 solution Substances 0.000 claims description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 claims description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 229960001948 caffeine Drugs 0.000 claims description 3
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 3
- 229940100892 mercury compound Drugs 0.000 claims description 3
- 150000002731 mercury compounds Chemical class 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 230000001376 precipitating effect Effects 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 238000002560 therapeutic procedure Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 230000008030 elimination Effects 0.000 claims 1
- 238000003379 elimination reaction Methods 0.000 claims 1
- 238000001556 precipitation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/10—Mercury compounds
- C07F3/12—Aromatic substances containing mercury
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
Torfahren zur Herstellung einer festen quecksilberhaltigen Holekularverbindung. Gegenstand des vorliegenden Zusatz patentes ist ein Verfahren zur Herstellung einer festen quecksilberhaltigen Molekular verbindung, das dadurch gekennzeichnet ist,
dass man .die komplexe Quecksilberverbin dung des salicylallylamid - 0 -essigsauren Natriums der Formel
EMI0001.0011
und Coffein in wässriger Lösung aufein ander einwirken lässt und aus der Lösung die entstandene Molekularverbindung in fester Form ausscheidet, vorzugsweise durch Zusatz geeigneter fällender Lösungsmittel oder durch Eindampfen der Lösung zur Trockne.
Beispiel: 100 cm' einem 10%igen wässrigen Lösung der komplexen Quecksilberverbindung des salicylal3lylami@d-0-essigsauren Natriums der Formel: n
EMI0001.0026
werden mit 5 g Coffein versetzt. Unter Schütteln tritt Lösung ein. Das beim Ein- dampfen im Vakuum hinterbleibende Pro dukt stellt ein weisses körniges Material dar, das die Modekularverbindung ist.
Die erhal tene neue Verbindung stellt ein weisses. Pulver .dar, das sich in Wasser mit curcuma- alkalischer Reaktion löst und in Äther und Aceton unlöslich ist. Sie ist zur Verwendung in der Therapie bestimmt.
Gate driving to produce a solid mercury-containing molecular compound. The subject of the present additional patent is a process for the production of a solid mercury-containing molecular compound, which is characterized by
that one .the complex mercury compound of salicylallylamide - 0 -acetic acid sodium of the formula
EMI0001.0011
and allowing caffeine to act on one another in aqueous solution and the resulting molecular compound is precipitated in solid form from the solution, preferably by adding suitable precipitating solvents or by evaporating the solution to dryness.
Example: 100 cm 'of a 10% aqueous solution of the complex mercury compound of salicylal3lylami @ d-0-acetic acid sodium of the formula: n
EMI0001.0026
5 g of caffeine are added. Solution enters with shaking. The product that remains after evaporation in a vacuum is a white, granular material that is the modular connection.
The new connection obtained is white. Powder .dar that dissolves in water with a curcuma-alkaline reaction and is insoluble in ether and acetone. It is intended for use in therapy.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH219010T | 1938-11-29 | ||
| CH227744T | 1938-11-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH227744A true CH227744A (en) | 1943-06-30 |
Family
ID=25726236
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH227744D CH227744A (en) | 1938-11-29 | 1938-11-29 | Process for the preparation of a solid molecular compound containing mercury. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH227744A (en) |
-
1938
- 1938-11-29 CH CH227744D patent/CH227744A/en unknown
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