CH233345A - Process for the preparation of a higher molecular weight, water-soluble condensation product. - Google Patents

Process for the preparation of a higher molecular weight, water-soluble condensation product.

Info

Publication number
CH233345A
CH233345A CH233345DA CH233345A CH 233345 A CH233345 A CH 233345A CH 233345D A CH233345D A CH 233345DA CH 233345 A CH233345 A CH 233345A
Authority
CH
Switzerland
Prior art keywords
condensation product
water
higher molecular
preparation
molecular weight
Prior art date
Application number
Other languages
German (de)
Inventor
Ag J R Geigy
Original Assignee
Ag J R Geigy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ag J R Geigy filed Critical Ag J R Geigy
Publication of CH233345A publication Critical patent/CH233345A/en

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Description

  

  <B>Zusatzpatent</B> zum Hauptpatent Nr. 230904.    Verfahren zur Darstellung eines     höhermolekularen,    wasserlöslichen  Kondensationsproduktes.    Gegenstand vorliegenden Zusatzpatentes  ist ein Verfahren zur Herstellung eines höher  molekularen     Kondensations.p.roduktes,    wel  ches dadurch gekennzeichnet ist,     dass    man       Stearoylaminomethyl-cyanguanidim    mit     einem     Gemisch aus Mono- und     Diäthanodamin    (1:     \?)     kondensiert und das     Kondensationsprodukt     erschöpfend     methyliert.     



  Die     quaternäre    Verbindung, eine bräun  liche Masse, eignet sich zum Weichmacken  von Textilien.  



       Beispiel:     An 37 Teile     (Stearoylaminomethyl)-cyan-          guanidin    wird ein     Gemisch    von Mono- und       Diäthanolamin    (1:2) durch     12stündiges    Rüh  ren bei 130-140  angelagert und die  Schmelze zirka 6 Stunden noch unter     Rühren     auf 190-210  erhitzt, wodurch eine nach  dem Erkalten     gelbstickige,        feste        Masse    erhal  ten wird.  



  44 Teile der so     dargestellten        Guanamin-          verbindung    werden in 300 Teilen Chlorben  zol gelöst,     mit    37 Teilen     Dimethylsulfat    und    35 Teilen Soda versetzt und während 6 Stun  den auf 100-110  erhitzt. Nach Entfernung  der anorganischen Salze und     Vertreiben    des       Lösungsmittels        hinterbleibt    eine braune, in  Säuren     lösliche        Masse.     



  44 Teile der     methylierten    Verbindung  werden in Form der Base mit 8 Teilen     Di-          methylsulfat    auf dem Wasserbad bis zur       urasserlöslichkeit    erhitzt. Die     quaterxiäre     Verbindung eignet sich vorzüglich zum  Weichmacken von Textilien.



  <B> Additional patent </B> to main patent no. 230904. Process for the preparation of a higher molecular weight, water-soluble condensation product. The subject of the present additional patent is a process for the production of a higher molecular condensation product, which is characterized in that stearoylaminomethyl-cyanguanidime is condensed with a mixture of mono- and diethanodamine (1: \?) And the condensation product is exhaustively methylated.



  The quaternary compound, a brownish mass, is suitable for softening textiles.



       Example: A mixture of mono- and diethanolamine (1: 2) is added to 37 parts of (stearoylaminomethyl) cyanoguanidine by stirring for 12 hours at 130-140 and the melt is heated to 190-210 for about 6 hours while stirring a yellow, sticky mass is obtained after cooling.



  44 parts of the guanamine compound thus prepared are dissolved in 300 parts of chlorobenzene, 37 parts of dimethyl sulfate and 35 parts of soda are added and the mixture is heated to 100-110 for 6 hours. After removing the inorganic salts and driving off the solvent, a brown mass which is soluble in acids remains.



  44 parts of the methylated compound are heated in the form of the base with 8 parts of dimethyl sulfate on a water bath until they are water-soluble. The quaterxial connection is ideally suited to softening textiles.

Claims (1)

<B>PATENTANSPRUCH:</B> Verfahren zur Herstellung eines .höher molekularen; wasserlöslichen Kondensations produktes.; welches dadurch gekennzeichnet ist, @dass man Stearoy lami@nomethyl-cyangu- anidin mit einem Gemisch aus Mono- und Di- äthanolamin (1: 2) kondensiert und das Kon densationsprodukt erschöpfend methyliert. Die quaternäre Verbindung, eine bräun liche Masse, eignet sich zum Weichmacken von Textilien. <B> PATENT CLAIM: </B> Process for producing a .higher molecular; water-soluble condensation product .; which is characterized by condensing Stearoy lami @ nomethyl-cyanguanidine with a mixture of mono- and diethanolamine (1: 2) and methylating the condensation product exhaustively. The quaternary compound, a brownish mass, is suitable for softening textiles.
CH233345D 1942-05-28 1942-05-28 Process for the preparation of a higher molecular weight, water-soluble condensation product. CH233345A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH230904T 1942-05-28
CH233345T 1942-05-28

Publications (1)

Publication Number Publication Date
CH233345A true CH233345A (en) 1944-07-15

Family

ID=25727508

Family Applications (1)

Application Number Title Priority Date Filing Date
CH233345D CH233345A (en) 1942-05-28 1942-05-28 Process for the preparation of a higher molecular weight, water-soluble condensation product.

Country Status (1)

Country Link
CH (1) CH233345A (en)

Similar Documents

Publication Publication Date Title
CH233345A (en) Process for the preparation of a higher molecular weight, water-soluble condensation product.
CH235190A (en) Process for the preparation of a water-soluble, higher molecular weight acyl biguanide.
DE832892C (en) Process for the preparation of condensation products of rutin
DE388794C (en) Process for the preparation of condensation products from phenols and aldehydes
AT160858B (en) Process for the production of bodies containing sulfuric acid residues
DE851065C (en) Process for the production of valuable condensation products
CH235441A (en) Process for the preparation of a monoaryl substitution product of melamine.
CH186464A (en) Process for the preparation of an acridinium compound.
CH252071A (en) Process for the preparation of a new amide derivative.
CH235442A (en) Process for the preparation of a monoaryl substitution product of melamine.
CH195838A (en) Process for the preparation of a salt of N-chloroethylhexahydroaniline.
CH311082A (en) Process for the preparation of an isonicotinic acid derivative.
CH124078A (en) Process for the preparation of an organic rhodane compound.
CH138194A (en) Process for the preparation of a condensation product from cyclohexanone.
CH293939A (en) Process for the preparation of a quaternary ammonium compound of a bis-aminoalkoxy-alkane.
CH160094A (en) Process for the preparation of a basic substituted aminoquinoline derivative.
CH239119A (en) Process for the preparation of a new water-soluble derivative of 4,4&#39;-diamino-diphenyl sulfone.
CH184300A (en) Process for the preparation of a condensation product from the a-naphthylamide of 2,3-oxynaphthoic acid and formaldehyde.
CH129785A (en) Process for the preparation of an ammonium compound of a halogenated aromatic amine.
CH293937A (en) Process for the preparation of a quaternary ammonium compound of a bis-aminoalkoxy-alkane.
CH202725A (en) Process for the preparation of a water-soluble derivative of the heterocyclic series.
CH240354A (en) Process for the production of a water-soluble, higher molecular weight guanamine.
CH214790A (en) Process for the preparation of an N-substitution product of melamine.
CH293932A (en) Process for the preparation of a quaternary ammonium compound of a bis-aminoalkoxy-alkane.
CH216304A (en) Process for the preparation of a new derivative of a heterocyclic compound.