CH263540A - Process for the production of a new condensation product. - Google Patents
Process for the production of a new condensation product.Info
- Publication number
- CH263540A CH263540A CH263540DA CH263540A CH 263540 A CH263540 A CH 263540A CH 263540D A CH263540D A CH 263540DA CH 263540 A CH263540 A CH 263540A
- Authority
- CH
- Switzerland
- Prior art keywords
- condensation product
- production
- new condensation
- new
- violet color
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 5
- 239000007859 condensation product Substances 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title description 3
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 235000005811 Viola adunca Nutrition 0.000 claims description 2
- 240000009038 Viola odorata Species 0.000 claims description 2
- 235000013487 Viola odorata Nutrition 0.000 claims description 2
- 235000002254 Viola papilionacea Nutrition 0.000 claims description 2
- 238000004043 dyeing Methods 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B13/00—Oxyketone dyes
- C09B13/02—Oxyketone dyes of the naphthalene series, e.g. naphthazarin
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines neuen Kondensationsproduktes. Die vorliecende Erfindung betrifft ein <B>M</B> Verfahren zur Herstellung eines neuen Kon- clensationsproduktes und ist dadurch gekenn- zeielniet, dass man das nach dem Verfahren der Patentsehrift Nr. <B>251646</B> erhältliche bro- mierte Naphtliochinonimid mit Anilin kon densiert.
<I>Beispiel:</I> <B><I>10</I> g</B> bromiertes Naplitlioehiiionimicl (er- lialten naeli dein Beispiel der Patentschrift. Nr. <B>251646)</B> werden mit<B>100 g</B> Anilin und <B>0,5 g</B> Borsäure unter gutem Rühren während 24 Stunden auf<B>50</B> bis<B>600</B> erwärmt.
Der An satz wird nun in übersehüssige 109,lige Salz säure gegossen und der Niederschlag abfil- triert, neutral gewaschen und getroeknet. Man erhält eine harzartige, brüchige Masse, die sieh leicht pulverisieren lässt und in<B>Al-</B> kohol mit blauvioletter und in ELSO, mit rötiiehvioletter Farbe löslieh ist. Die neue Verbindung soll als Farbstoff für Aeetatseide erwendet werden.
Process for the production of a new condensation product. The present invention relates to a <B> M </B> process for the production of a new condensation product and is characterized by the fact that the brominated one obtainable according to the process of patent document no. 251646 </B> is used Naphthioquinonimide condensed with aniline.
<I> Example: </I> <B> <I> 10 </I> g </B> brominated Naplitlioehiiionimicl (naeli your example achieved the patent. No. <B> 251646) </B> are with <B> 100 g </B> aniline and <B> 0.5 g </B> boric acid heated to <B> 50 </B> to <B> 600 </B> for 24 hours with thorough stirring.
The batch is then poured into excess 10% hydrochloric acid and the precipitate is filtered off, washed neutral and dried. A resin-like, brittle mass is obtained, which can be easily pulverized and is soluble in <B> Al </B> alcohol with a blue-violet color and in ELSO with a reddish-violet color. The new compound will be used as a dye for acetate silk.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH263540T | 1946-04-26 | ||
| CH258588T | 1948-12-15 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH263540A true CH263540A (en) | 1949-08-31 |
Family
ID=25730190
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH263540D CH263540A (en) | 1946-04-26 | 1946-04-26 | Process for the production of a new condensation product. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH263540A (en) |
-
1946
- 1946-04-26 CH CH263540D patent/CH263540A/en unknown
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