CH308806A - Process for the production of a vat dye. - Google Patents
Process for the production of a vat dye.Info
- Publication number
- CH308806A CH308806A CH308806DA CH308806A CH 308806 A CH308806 A CH 308806A CH 308806D A CH308806D A CH 308806DA CH 308806 A CH308806 A CH 308806A
- Authority
- CH
- Switzerland
- Prior art keywords
- red
- production
- vat
- dye
- vat dye
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 239000000984 vat dye Substances 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 5
- LULAYUGMBFYYEX-UHFFFAOYSA-N 3-chlorobenzoic acid Chemical compound OC(=O)C1=CC=CC(Cl)=C1 LULAYUGMBFYYEX-UHFFFAOYSA-N 0.000 claims description 4
- 229920000742 Cotton Polymers 0.000 claims description 2
- 239000013078 crystal Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
- 239000011593 sulfur Substances 0.000 claims 1
- RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- CELCMWUXMBTJRP-UHFFFAOYSA-N chlorobenzene;hydrochloride Chemical compound Cl.ClC1=CC=CC=C1 CELCMWUXMBTJRP-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B5/00—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings
- C09B5/24—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic rings being only condensed with an anthraquinone nucleus in 1-2 or 2-3 position
- C09B5/34—Anthraquinone acridones or thioxanthrones
- C09B5/36—Amino acridones
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines Küpenfarbstoffes. Gegenstand des vorliegenden Patentes ist ein Verfahren zur Herstellung eines Küpen- farbstoffes, dadurch gekennzeichnet, dass man 4-Amino-2,1- anthr achinon-4'- chlorbenzacridon mit Metachlorbenzoesäure bzw. deren funktio nellen Derivaten kondensiert.
Der neue Farbstoff stellt ein dunkelblaues Kristallpulver dar, das sich in konz. Schwefel säure mit rotstichig oranger Farbe löst und Baumwolle aus roter Küpe in klaren, vollen, sehr rotstichig blauen Tönen von hervorra genden Echtheitseigenschaften färbt. Beispiel: Ein Gemisch aus 350 Teilen o-Dichlorben- zol, 18,7 Teilen 4-Amino-2,1-anthrachinon-4'- chlorbenzacridon und 17,5 Teilen m-Chl.or- benzovlchlorid wird 12 Stunden auf 160 er hitzt.
Nach dem Erkalten wird der gebildete Farbstoff abgesaugt und zunächst mit o-Di- chlorbenzol und dann mit Methanol ausge- wasehen und getrocknet.
Process for the production of a vat dye. The subject of the present patent is a process for the production of a vat dye, characterized in that 4-amino-2,1-anthracinone-4'-chlorobenzacridone is condensed with metachlorobenzoic acid or its functional derivatives.
The new dye is a dark blue crystal powder that is in conc. Sulfuric acid dissolves with a red-tinged orange color and dyes cotton from a red vat in clear, full, very red-tinged blue tones with excellent fastness properties. Example: A mixture of 350 parts of o-dichlorobenzene, 18.7 parts of 4-amino-2,1-anthraquinone-4'-chlorobenzacridone and 17.5 parts of m-chlorobenzene chloride is heated to 160 for 12 hours .
After cooling, the dye formed is filtered off with suction and washed first with o-dichlorobenzene and then with methanol and dried.
Claims (1)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE308806X | 1951-07-30 | ||
| DE101051X | 1951-10-10 | ||
| CH306386T | 1952-07-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH308806A true CH308806A (en) | 1955-07-31 |
Family
ID=27178301
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH308806D CH308806A (en) | 1951-07-30 | 1952-07-28 | Process for the production of a vat dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH308806A (en) |
-
1952
- 1952-07-28 CH CH308806D patent/CH308806A/en unknown
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