CH374081A - Verfahren zur Herstellung von Polyelektrolyten - Google Patents

Verfahren zur Herstellung von Polyelektrolyten

Info

Publication number: CH374081A
Authority: CH; Switzerland
Prior art keywords: heated; hours; mixture; groups; methyl
Prior art date: 1955-01-22

Application number

CH2907256A

Other languages

German (de)

English (en)

Original Assignee

Leinfelder Hermann

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1955-01-22

Filing date

1956-01-21

Publication date

1963-12-31

1956-01-21 Application filed by Leinfelder Hermann filed Critical Leinfelder Hermann

1963-12-31 Publication of CH374081A publication Critical patent/CH374081A/de

Links

238000000034 method Methods 0.000 title claims description 14
229920000867 polyelectrolyte Polymers 0.000 title description 4
238000004519 manufacturing process Methods 0.000 title description 3
150000003512 tertiary amines Chemical class 0.000 claims description 14
229910052757 nitrogen Inorganic materials 0.000 claims description 10
125000004433 nitrogen atom Chemical group N* 0.000 claims description 8
229920000233 poly(alkylene oxides) Polymers 0.000 claims description 7
125000000217 alkyl group Chemical group 0.000 claims description 4
125000004432 carbon atom Chemical group C* 0.000 claims description 4
125000005843 halogen group Chemical group 0.000 claims description 4
239000003792 electrolyte Substances 0.000 claims description 3
125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 2
125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 claims description 2
150000001733 carboxylic acid esters Chemical class 0.000 claims 1
150000002016 disaccharides Chemical class 0.000 claims 1
150000002772 monosaccharides Chemical class 0.000 claims 1
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 24
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 24
239000000203 mixture Substances 0.000 description 21
GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 21
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
-1 amino, carboxyl Chemical group 0.000 description 17
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 15
239000000243 solution Substances 0.000 description 14
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
239000007864 aqueous solution Substances 0.000 description 11
XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 10
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 9
238000006116 polymerization reaction Methods 0.000 description 9
239000000126 substance Substances 0.000 description 9
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
239000000460 chlorine Substances 0.000 description 8
SJRJJKPEHAURKC-UHFFFAOYSA-N N-Methylmorpholine Chemical compound CN1CCOCC1 SJRJJKPEHAURKC-UHFFFAOYSA-N 0.000 description 7
229910052801 chlorine Inorganic materials 0.000 description 7
239000000047 product Substances 0.000 description 7
PAMIQIKDUOTOBW-UHFFFAOYSA-N 1-methylpiperidine Chemical compound CN1CCCCC1 PAMIQIKDUOTOBW-UHFFFAOYSA-N 0.000 description 6
150000001450 anions Chemical class 0.000 description 6
125000001246 bromo group Chemical group Br* 0.000 description 6
239000007795 chemical reaction product Substances 0.000 description 6
238000000502 dialysis Methods 0.000 description 6
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 6
239000002904 solvent Substances 0.000 description 6
GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical class CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 5
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 5
229910052794 bromium Inorganic materials 0.000 description 5
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 4
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
125000004185 ester group Chemical group 0.000 description 4
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 3
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
238000001816 cooling Methods 0.000 description 3
GKIPXFAANLTWBM-UHFFFAOYSA-N epibromohydrin Chemical compound BrCC1CO1 GKIPXFAANLTWBM-UHFFFAOYSA-N 0.000 description 3
239000000174 gluconic acid Substances 0.000 description 3
235000012208 gluconic acid Nutrition 0.000 description 3
LRZFEBJUJIQVDQ-UHFFFAOYSA-N methyl 2-(dimethylamino)acetate Chemical compound COC(=O)CN(C)C LRZFEBJUJIQVDQ-UHFFFAOYSA-N 0.000 description 3
DILRJUIACXKSQE-UHFFFAOYSA-N n',n'-dimethylethane-1,2-diamine Chemical compound CN(C)CCN DILRJUIACXKSQE-UHFFFAOYSA-N 0.000 description 3
238000006386 neutralization reaction Methods 0.000 description 3
125000001453 quaternary ammonium group Chemical group 0.000 description 3
150000003254 radicals Chemical class 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
150000003839 salts Chemical group 0.000 description 3
125000001424 substituent group Chemical group 0.000 description 3
PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
CFAFEJHONLMPQY-UHFFFAOYSA-N 2-(dimethylazaniumyl)ethanesulfonate Chemical compound CN(C)CCS(O)(=O)=O CFAFEJHONLMPQY-UHFFFAOYSA-N 0.000 description 2
229910015900 BF3 Inorganic materials 0.000 description 2
UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 description 2
239000002253 acid Substances 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
150000001408 amides Chemical class 0.000 description 2
WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 2
GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 description 2
238000009792 diffusion process Methods 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
CRVGTESFCCXCTH-UHFFFAOYSA-N methyl diethanolamine Chemical compound OCCN(C)CCO CRVGTESFCCXCTH-UHFFFAOYSA-N 0.000 description 2
238000001226 reprecipitation Methods 0.000 description 2
229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
235000017557 sodium bicarbonate Nutrition 0.000 description 2
JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 description 2
238000003756 stirring Methods 0.000 description 2
125000000542 sulfonic acid group Chemical group 0.000 description 2
210000001519 tissue Anatomy 0.000 description 2
SZYJELPVAFJOGJ-UHFFFAOYSA-N trimethylamine hydrochloride Chemical group Cl.CN(C)C SZYJELPVAFJOGJ-UHFFFAOYSA-N 0.000 description 2
RBACIKXCRWGCBB-UHFFFAOYSA-N 1,2-Epoxybutane Chemical class CCC1CO1 RBACIKXCRWGCBB-UHFFFAOYSA-N 0.000 description 1
JUXXCHAGQCBNTI-UHFFFAOYSA-N 1-n,1-n,2-n,2-n-tetramethylpropane-1,2-diamine Chemical compound CN(C)C(C)CN(C)C JUXXCHAGQCBNTI-UHFFFAOYSA-N 0.000 description 1
DWGMAIPVJRBOIB-UHFFFAOYSA-N 2-(dimethylamino)-n,n-dimethylacetamide Chemical compound CN(C)CC(=O)N(C)C DWGMAIPVJRBOIB-UHFFFAOYSA-N 0.000 description 1
KNVRBEGQERGQRP-UHFFFAOYSA-N 2-amino-n,n-dimethylacetamide Chemical compound CN(C)C(=O)CN KNVRBEGQERGQRP-UHFFFAOYSA-N 0.000 description 1
TWWCBLSUGOSDIY-UHFFFAOYSA-N 2-ethyl-1,1-dimethylhydrazine Chemical compound CCNN(C)C TWWCBLSUGOSDIY-UHFFFAOYSA-N 0.000 description 1
QCMHUGYTOGXZIW-UHFFFAOYSA-N 3-(dimethylamino)propane-1,2-diol Chemical compound CN(C)CC(O)CO QCMHUGYTOGXZIW-UHFFFAOYSA-N 0.000 description 1
SKWAJBSFADKWHK-UHFFFAOYSA-M 3-(dimethylamino)propyl-trimethylazanium bromide Chemical compound [Br-].CN(CCC[N+](C)(C)C)C SKWAJBSFADKWHK-UHFFFAOYSA-M 0.000 description 1
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical class NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 1
XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
PHOQVHQSTUBQQK-SQOUGZDYSA-N D-glucono-1,5-lactone Chemical compound OC[C@H]1OC(=O)[C@H](O)[C@@H](O)[C@@H]1O PHOQVHQSTUBQQK-SQOUGZDYSA-N 0.000 description 1
108010003272 Hyaluronate lyase Proteins 0.000 description 1
102000001974 Hyaluronidases Human genes 0.000 description 1
DJEQZVQFEPKLOY-UHFFFAOYSA-N N,N-dimethylbutylamine Chemical compound CCCCN(C)C DJEQZVQFEPKLOY-UHFFFAOYSA-N 0.000 description 1
XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
125000002947 alkylene group Chemical class 0.000 description 1
150000003868 ammonium compounds Chemical group 0.000 description 1
210000001557 animal structure Anatomy 0.000 description 1
238000005349 anion exchange Methods 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
239000001110 calcium chloride Substances 0.000 description 1
229910001628 calcium chloride Inorganic materials 0.000 description 1
239000004202 carbamide Substances 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
150000007942 carboxylates Chemical class 0.000 description 1
125000003262 carboxylic acid ester group Chemical group [H]C([H])([*:2])OC(=O)C([H])([H])[*:1] 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
238000004140 cleaning Methods 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000013078 crystal Substances 0.000 description 1
229960002887 deanol Drugs 0.000 description 1
SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Natural products CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
230000000694 effects Effects 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
238000005194 fractionation Methods 0.000 description 1
238000004108 freeze drying Methods 0.000 description 1
229910052736 halogen Inorganic materials 0.000 description 1
150000002367 halogens Chemical class 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
229960002773 hyaluronidase Drugs 0.000 description 1
125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
QDUXDCXILAPLAG-UHFFFAOYSA-N hydron;1-methylpiperidine;chloride Chemical group Cl.CN1CCCCC1 QDUXDCXILAPLAG-UHFFFAOYSA-N 0.000 description 1
238000001802 infusion Methods 0.000 description 1
239000007924 injection Substances 0.000 description 1
238000002347 injection Methods 0.000 description 1
238000005342 ion exchange Methods 0.000 description 1
239000007788 liquid Substances 0.000 description 1
238000002844 melting Methods 0.000 description 1
230000008018 melting Effects 0.000 description 1
WCYWZMWISLQXQU-UHFFFAOYSA-N methyl Chemical compound [CH3] WCYWZMWISLQXQU-UHFFFAOYSA-N 0.000 description 1
OZQUQEWSJJCYPL-UHFFFAOYSA-N methyl 2-(dimethylamino)hexanoate Chemical compound CCCCC(N(C)C)C(=O)OC OZQUQEWSJJCYPL-UHFFFAOYSA-N 0.000 description 1
229940102396 methyl bromide Drugs 0.000 description 1
210000003097 mucus Anatomy 0.000 description 1
OHLICMMXIJECIN-UHFFFAOYSA-N n-[3-(dimethylamino)propyl]acetamide Chemical compound CN(C)CCCNC(C)=O OHLICMMXIJECIN-UHFFFAOYSA-N 0.000 description 1
230000003472 neutralizing effect Effects 0.000 description 1
239000002674 ointment Substances 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
150000003856 quaternary ammonium compounds Chemical class 0.000 description 1
150000003242 quaternary ammonium salts Chemical class 0.000 description 1
238000005956 quaternization reaction Methods 0.000 description 1
238000001953 recrystallisation Methods 0.000 description 1
239000013557 residual solvent Substances 0.000 description 1
210000003296 saliva Anatomy 0.000 description 1
239000007858 starting material Substances 0.000 description 1
238000001256 steam distillation Methods 0.000 description 1
IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical class NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 description 1
210000001179 synovial fluid Anatomy 0.000 description 1
125000001302 tertiary amino group Chemical group 0.000 description 1
238000001291 vacuum drying Methods 0.000 description 1
210000004127 vitreous body Anatomy 0.000 description 1
238000010626 work up procedure Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07K—PEPTIDES
- C07K1/00—General methods for the preparation of peptides, i.e. processes for the organic chemical preparation of peptides or proteins of any length
- C07K1/006—General methods for the preparation of peptides, i.e. processes for the organic chemical preparation of peptides or proteins of any length of peptides containing derivatised side chain amino acids
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
- C08F20/62—Monocarboxylic acids having ten or more carbon atoms; Derivatives thereof
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/02—Alkylation
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/12—Hydrolysis
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/30—Introducing nitrogen atoms or nitrogen-containing groups
- C08F8/32—Introducing nitrogen atoms or nitrogen-containing groups by reaction with amines
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/34—Introducing sulfur atoms or sulfur-containing groups
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
- C08G18/0809—Manufacture of polymers containing ionic or ionogenic groups containing cationic or cationogenic groups
- C08G18/0814—Manufacture of polymers containing ionic or ionogenic groups containing cationic or cationogenic groups containing ammonium groups or groups forming them
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
- C08G18/0833—Manufacture of polymers containing ionic or ionogenic groups containing cationic or cationogenic groups together with anionic or anionogenic groups
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/32—Polymers modified by chemical after-treatment
- C08G65/329—Polymers modified by chemical after-treatment with organic compounds
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/10—Alpha-amino-carboxylic acids
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/48—Polymers modified by chemical after-treatment
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/02—Polyamines
- C08G73/028—Polyamidoamines
- C08G73/0293—Quaternisation of polyamidoamines
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2800/00—Copolymer characterised by the proportions of the comonomers expressed
- C08F2800/10—Copolymer characterised by the proportions of the comonomers expressed as molar percentages
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2800/00—Copolymer characterised by the proportions of the comonomers expressed
- C08F2800/20—Copolymer characterised by the proportions of the comonomers expressed as weight or mass percentages

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Manufacturing & Machinery (AREA)
Engineering & Computer Science (AREA)
Biophysics (AREA)
Proteomics, Peptides & Aminoacids (AREA)
Molecular Biology (AREA)
Genetics & Genomics (AREA)
General Health & Medical Sciences (AREA)
Biochemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Analytical Chemistry (AREA)
Polyamides (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

CH2907256A 1955-01-22 1956-01-21 Verfahren zur Herstellung von Polyelektrolyten CH374081A (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DEM25859A DE1123468B (de)	1955-01-22	1955-01-22	Verfahren zur Herstellung wasserloeslicher, poly-N-quaternaerer, die Diffusion in Geweben erhoehender Substanzen

Publications (1)

Publication Number	Publication Date
CH374081A true CH374081A (de)	1963-12-31

Family

ID=7299665

Family Applications (2)

Application Number	Title	Priority Date	Filing Date
CH2907256A CH374081A (de)	1955-01-22	1956-01-21	Verfahren zur Herstellung von Polyelektrolyten
CH341262A CH412924A (de)	1955-01-22	1956-01-21	Verfahren zur Herstellung wasserlöslicher poly-N-quaternärer Substanzen

Family Applications After (1)

Application Number	Title	Priority Date	Filing Date
CH341262A CH412924A (de)	1955-01-22	1956-01-21	Verfahren zur Herstellung wasserlöslicher poly-N-quaternärer Substanzen

Country Status (4)

Country	Link
BE (1)	BE544607A (fr)
CH (2)	CH374081A (fr)
DE (1)	DE1123468B (fr)
FR (1)	FR1484601A (fr)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3855290A (en) *	1971-03-03	1974-12-17	Dyk & Co Inc Van	Quaternary halides of gluconamides
US3898188A (en) *	1972-08-14	1975-08-05	California Inst Of Techn	Novel polyelectrolytes
CA1059693A (fr) *	1974-09-18	1979-07-31	B.F. Goodrich Company (The)	Epaississeur a base de polyepihalohydrine a liaisons transversales et transformee en derive quaternaire
LU78153A1 (fr) *	1977-09-20	1979-05-25	Oreal	Compositions cosmetiques a base de polymeres polyammonium quaternaires et procede de preparation
DE19503279C2 (de) *	1995-02-02	1998-11-12	Henkel Kgaa	Kation- und/oder Amphooligomere
PE20060426A1 (es)	2004-06-02	2006-06-28	Schering Corp	DERIVADOS DE ACIDO TARTARICO COMO INHIBIDORES DE MMPs, ADAMs, TACE Y TNF-alfa
US7638513B2 (en)	2004-06-02	2009-12-29	Schering Corporation	Compounds for the treatment of inflammatory disorders

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE696780C (de) *	1935-06-23	1940-09-28	I G Farbenindustrie Akt Ges	Verfahren zur Herstellung von technisch wertvollen Kondensationsprodukten
DE714585C (de) *	1935-08-17	1941-12-03	Ig Farbenindustrie Ag	Verfahren zur Herstellung stickstoffhaltiger Produkte
DE907598C (de) *	1942-03-05	1954-03-25	Basf Ag	Verfahren zur Herstellung von polymeren Isothioharnstoffaethern
DE904591C (de) *	1944-01-04	1954-02-22	Cassella Farbwerke Mainkur Ag	Verfahren zur Herstellung von quaternaeren Ammoniumverbindungen
DE880485C (de) *	1944-07-02	1953-06-22	Bayer Ag	Verfahren zur Herstellung von Hochpolymeren
US2483749A (en) *	1948-02-24	1949-10-04	Gen Mills Inc	Quaternary ammonium salts
GB652830A (en) *	1948-10-23	1951-05-02	Reginald Patrick Linstead	Improvements in and relating to insoluble poly-quaternary resins
DE847347C (de) *	1950-06-30	1952-08-21	Basf Ag	Verfahren zur Herstellung von Polymerisaten
GB717305A (en) *	1951-10-05	1954-10-27	Rohm & Haas	Improvements in or relating to the preparation of resinous quaternary ammonium hydroxides and alkoxides

1955
- 1955-01-22 DE DEM25859A patent/DE1123468B/de active Pending
1956
- 1956-01-20 FR FR706808A patent/FR1484601A/fr not_active Expired
- 1956-01-21 BE BE544607A patent/BE544607A/fr unknown
- 1956-01-21 CH CH2907256A patent/CH374081A/de unknown
- 1956-01-21 CH CH341262A patent/CH412924A/de unknown

Also Published As

Publication number	Publication date
CH412924A (de)	1966-05-15
DE1123468B (de)	1962-02-08
FR1484601A (fr)	1967-06-16
BE544607A (fr)	1956-07-23

Publication	Publication Date	Title
CH374081A (de)	1963-12-31	Verfahren zur Herstellung von Polyelektrolyten
DE2118109A1 (de)	1971-12-02	Neue chemische Verbindung
AT213383B (de)	1961-02-10	Verfahren zur Herstellung von neuen, wasserlöslichen poly-N-quaternären Elektrolyten
DE1227893B (de)	1966-11-03	Verfahren zur Herstellung von Glycyrrhetinsaeurederivaten
DE2628042C3 (de)	1979-11-29	3-Amino-tricyclo [5.3.1.0.38I -undecan, dessen Säureadditionssalze und Verfahren zur Herstellung dieser Verbindungen
AT224619B (de)	1962-12-10	Verfahren zur Herstellung von wasserlöslichen, poly-N-quaternären Elektrolyten
CH369759A (de)	1963-06-15	Verfahren zur Herstellung von N-Alkylpiperidin-a-carbonsäureaniliden
DE940828C (de)	1956-03-29	Verfahren zur Herstellung von Estern des Penicillins mit Phenolen und Thiophenolen
DE949471C (de)	1956-09-20	Verfahren zur Herstellung von neuen Estern des Yohimbins
DE855712C (de)	1952-11-17	Verfahren zur Herstellung neuer, in 8-Stellung substituierter 6, 9-Dioxy-2-amino-pteridinderivate
DE1036259B (de)	1958-08-14	Verfahren zur Herstellung von basisch substituierten Alkoxyalkylestern der Phenthiazin-10-carbonsaeure und deren Salzen bzw. quaternaeren Ammoniumverbindungen
DE932675C (de)	1955-09-05	Verfahren zur Herstellung von Estern des Penicillins mit eine sekundaere Aminogruppe aufweisenden Alkoholen und von Salzen dieser Ester
DE1132917B (de)	1962-07-12	Verfahren zur Herstellung von wasserloeslichen und wenig toxischen Tetracyclinderivaten bzw. deren neutralen Komplexverbindungen
DE973048C (de)	1959-11-19	Verfahren zur Herstellung von als Heilmittel geeigneten substituierten Morpholinen
DE1963318C (de)	1972-11-30	Silybinhalbestersauren des Silybins mit 1 und bzw oder 2 Mol Bernsteinsaure und deren Salze mit pharmakologisch ver traglichen anorganischen oder organischen Basen, und Arzneimittel
AT215997B (de)	1961-07-10	Verfahren zur Herstellung neuer Ester der α-Phenyl-α-piperidyl-(2)-essigsäure
AT265265B (de)	1968-10-10	Verfahren zur Herstellung von neuen rechtsdrehenden und linksdrehenden Formen von 1-(β-Hydroxy-äthyl)-diphenylmethyl-piperidinen und ihren Salzen
DE972336C (de)	1959-07-02	Verfahren zur Gewinnung von stabilen, besonders fuer die Oraltherapie geeigneten Penicillinen
DE859518C (de)	1952-12-15	Verfahren zur Herstellung des Natrium- oder Calciumsalzes des Penicillins, gegebenenfalls in aufgeloester Form, aus dem Kaliumsalz
DE2027832C3 (de)	1976-03-25	Verfahren zur Herstellung von Thiamphenicol-glycinat-acetylcysteinat
AT212304B (de)	1960-12-12	Verfahren zur Herstellung von Aminosäureestern von threo-1-(p-Nitrophenyl)-2-dichloracetamidopropan-1, 3-diolen
DE974320C (de)	1960-11-24	Verfahren zur Herstellung eines als Lokalanaestheticum verwendbaren p-Amino-benzoesaeure-polyglykolesters
CH316965A (de)	1956-10-31	Verfahren zur Herstellung neuer, biologisch wirksamer Polykondensationsprodukte aus Gentisinsäure
AT233172B (de)	1964-04-25	Verfahren zur Herstellung neuer Äther
DE1225159B (de)	1966-09-22	Verfahren zur Herstellung von N-(Sulfobenzoyl)-N-desulfoheparinen oder deren Alkalisalzen