CH388981A - Verfahren zur Herstellung von w-Aminodecansäure - Google Patents
Verfahren zur Herstellung von w-AminodecansäureInfo
- Publication number
- CH388981A CH388981A CH483961A CH483961A CH388981A CH 388981 A CH388981 A CH 388981A CH 483961 A CH483961 A CH 483961A CH 483961 A CH483961 A CH 483961A CH 388981 A CH388981 A CH 388981A
- Authority
- CH
- Switzerland
- Prior art keywords
- acid
- aminodecanoic
- sodium salt
- aminodecanoic acid
- cyanopelargonic
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 11
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 24
- 239000002253 acid Substances 0.000 claims description 9
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 claims description 8
- 159000000000 sodium salts Chemical class 0.000 claims description 8
- 150000001413 amino acids Chemical class 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000005984 hydrogenation reaction Methods 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 4
- 238000009903 catalytic hydrogenation reaction Methods 0.000 claims description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 2
- 239000011707 mineral Substances 0.000 claims description 2
- 238000006386 neutralization reaction Methods 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical class OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- HJMZMZRCABDKKV-UHFFFAOYSA-N carbonocyanidic acid Chemical class OC(=O)C#N HJMZMZRCABDKKV-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- JINGUCXQUOKWKH-UHFFFAOYSA-N 2-aminodecanoic acid Chemical compound CCCCCCCCC(N)C(O)=O JINGUCXQUOKWKH-UHFFFAOYSA-N 0.000 description 2
- 239000007868 Raney catalyst Substances 0.000 description 2
- 229910000564 Raney nickel Inorganic materials 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- MLIREBYILWEBDM-UHFFFAOYSA-N cyanoacetic acid Chemical compound OC(=O)CC#N MLIREBYILWEBDM-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- FBUKVWPVBMHYJY-UHFFFAOYSA-N nonanoic acid Chemical compound CCCCCCCCC(O)=O FBUKVWPVBMHYJY-UHFFFAOYSA-N 0.000 description 2
- 159000000001 potassium salts Chemical class 0.000 description 2
- -1 γ-cyan pelargonic acid Chemical compound 0.000 description 2
- CIQRWLRUNXKNTE-UHFFFAOYSA-N 2-cyanononanoic acid Chemical compound CCCCCCCC(C#N)C(O)=O CIQRWLRUNXKNTE-UHFFFAOYSA-N 0.000 description 1
- 239000007832 Na2SO4 Substances 0.000 description 1
- 239000005643 Pelargonic acid Substances 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 125000002560 nitrile group Chemical group 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- BDAWXSQJJCIFIK-UHFFFAOYSA-N potassium methoxide Chemical compound [K+].[O-]C BDAWXSQJJCIFIK-UHFFFAOYSA-N 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- LTOCMXUTASYUOC-UHFFFAOYSA-M sodium;nonanoate Chemical compound [Na+].CCCCCCCCC([O-])=O LTOCMXUTASYUOC-UHFFFAOYSA-M 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH483961A CH388981A (de) | 1961-04-25 | 1961-04-25 | Verfahren zur Herstellung von w-Aminodecansäure |
| GB984762A GB953621A (en) | 1961-04-25 | 1962-03-14 | Process for the manufacture of omega-aminodecanoic acid |
| BE615830A BE615830A (fr) | 1961-04-25 | 1962-03-30 | Procédé de fabrication d l'acide omega -aminodécanoïque |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH483961A CH388981A (de) | 1961-04-25 | 1961-04-25 | Verfahren zur Herstellung von w-Aminodecansäure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH388981A true CH388981A (de) | 1965-03-15 |
Family
ID=4283449
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH483961A CH388981A (de) | 1961-04-25 | 1961-04-25 | Verfahren zur Herstellung von w-Aminodecansäure |
Country Status (3)
| Country | Link |
|---|---|
| BE (1) | BE615830A (fr) |
| CH (1) | CH388981A (fr) |
| GB (1) | GB953621A (fr) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10329242B2 (en) | 2017-08-25 | 2019-06-25 | Vitaworks Ip, Llc | Process for purifying long chain amino acids |
| US10239823B2 (en) | 2017-08-25 | 2019-03-26 | Vitaworks Ip, Llc | Process for purifying long chain amino acids |
| CN116947668A (zh) * | 2023-06-21 | 2023-10-27 | 中国五环工程有限公司 | 11-氨基十一酸的结晶方法 |
-
1961
- 1961-04-25 CH CH483961A patent/CH388981A/de unknown
-
1962
- 1962-03-14 GB GB984762A patent/GB953621A/en not_active Expired
- 1962-03-30 BE BE615830A patent/BE615830A/fr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE615830A (fr) | 1962-07-16 |
| GB953621A (en) | 1964-03-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE1226567B (de) | Verfahren zur Herstellung von trans-Hexahydroterephthalsaeure | |
| CH388981A (de) | Verfahren zur Herstellung von w-Aminodecansäure | |
| DE2026538A1 (de) | Verfahren zur gleichzeitigen Herstellung von 2-Amino-l-butanol und 2-Amino-2-äthyl-l,3-propandiol | |
| DE3936522A1 (de) | 5-((alpha)-d-glucopyranosyloxymethyl)-furan-2-carboxaldehyd und dessen derivate und folgeprodukte sowie verfahren zur herstellung der verbindungen und deren verwendung | |
| DE830951C (de) | Verfahren zur Herstellung mehrwertiger Alkohole | |
| DE1129944B (de) | Verfahren zur Herstellung von Sebacin- oder 3-AEthylkorksaeure oder deren Gemischen | |
| DE2647317A1 (de) | Verfahren zur herstellung von alpha,omega-diaminen | |
| CH495944A (de) | Verfahren zur Herstellung von a-Methyl-polycyclomethylaminen | |
| AT227268B (de) | Verfahren zur Herstellung des neuen 2-Hydroxymethylpiperazins | |
| DE2350668C2 (de) | Verfahren zur Gewinnung von kristallinem, nicht mehr als etwa 0,1 Gew.% Xylose enthaltendem Xylit | |
| DE3839004A1 (de) | Verfahren zur herstellung von 4,4'-dinitrodiphenylamin | |
| AT203476B (de) | Verfahren zur Herstellung von Lactamen | |
| CH378868A (de) | Verfahren zur Herstellung des w-Amino-caprylsäureamids | |
| AT236356B (de) | Verfahren zur Reinigung von rohem Caprolactam | |
| DE929368C (de) | Verfahren zur Herstellung von Acrylsaeure | |
| AT286294B (de) | Verfahren zur herstellung von 2-(4'-thiazolyl)-benzimidazol | |
| AT202556B (de) | Verfahren zur kontinuierlichen Herstellung von Hexamethylendiamin aus Adipinsäuredinitril | |
| DE1067820B (de) | Verfahren zur Herstellung von Piperazin | |
| DE423026C (de) | Verfahren zur Darstellung eines Bz-Tetrahydrooxychinolins | |
| AT208837B (de) | Verfahren zur Herstellung von γ-Aminocaprylsäure und deren Ester | |
| AT338800B (de) | Verfahren zur herstellung von 2,4-diamino-5-(3',4',5'-trimethoxybenzyl)-6-chlorpyrimidin | |
| DE2160674C3 (de) | Verfahren zur Herstellung von 4(5)-Aminoimidazol-5(4)-carboxamid aus 4(5)-Aminoimidazol-5(4)-carbonitril | |
| DE1029820B (de) | Verfahren zur Herstellung wasserloeslicher stabiler Kondensations-produkte aus Harnstoff, Thioharnstoff oder ihren Derivaten und Formaldehyd | |
| CH651044A5 (en) | Process for preparing 2,6-Diaminopurine | |
| DE1011429B (de) | Verfahren zur Herstellung von Aminocarbonsaeuren durch Hydrolyse ihrer Lactame |