CH410396A - Verfahren zur Herstellung schwer entflammbarer Phenolharz-Schaumstoffe - Google Patents

Verfahren zur Herstellung schwer entflammbarer Phenolharz-Schaumstoffe

Info

Publication number: CH410396A
Authority: CH; Switzerland
Prior art keywords: flame; phenolic resin; foam; resin foams; production
Prior art date: 1961-04-18

Application number

CH387462A

Other languages

German (de)

English (en)

Inventor

Pinten Peter Ing Dr

Nat Weissenfels Franz Dr Rer

Original Assignee

Dynamit Nobel Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1961-04-18

Filing date

1962-03-30

Publication date

1966-03-31

1962-03-30 Application filed by Dynamit Nobel Ag filed Critical Dynamit Nobel Ag

1966-03-31 Publication of CH410396A publication Critical patent/CH410396A/de

Links

239000006260 foam Substances 0.000 title claims description 26
239000003063 flame retardant Substances 0.000 title claims description 10
RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims description 9
229920001568 phenolic resin Polymers 0.000 title claims description 7
KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 title claims description 6
239000005011 phenolic resin Substances 0.000 title claims description 6
238000000034 method Methods 0.000 title claims description 5
238000004519 manufacturing process Methods 0.000 title description 2
150000001639 boron compounds Chemical class 0.000 claims description 6
239000007787 solid Substances 0.000 claims description 6
239000007859 condensation product Substances 0.000 claims description 5
239000007788 liquid Substances 0.000 claims description 5
150000002989 phenols Chemical class 0.000 claims description 5
238000005187 foaming Methods 0.000 claims description 4
125000002485 formyl group Chemical class [H]C(*)=O 0.000 claims 1
239000000203 mixture Substances 0.000 description 15
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 8
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 7
235000010338 boric acid Nutrition 0.000 description 6
229920005989 resin Polymers 0.000 description 6
239000011347 resin Substances 0.000 description 6
KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 5
239000004327 boric acid Substances 0.000 description 5
238000010438 heat treatment Methods 0.000 description 5
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
150000001875 compounds Chemical class 0.000 description 4
238000009833 condensation Methods 0.000 description 4
230000005494 condensation Effects 0.000 description 4
VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 description 4
238000003756 stirring Methods 0.000 description 4
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
150000001299 aldehydes Chemical class 0.000 description 3
239000008187 granular material Substances 0.000 description 3
238000000465 moulding Methods 0.000 description 3
229920003987 resole Polymers 0.000 description 3
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
229930040373 Paraformaldehyde Natural products 0.000 description 2
OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
238000009835 boiling Methods 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 2
239000004312 hexamethylene tetramine Substances 0.000 description 2
235000010299 hexamethylene tetramine Nutrition 0.000 description 2
WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
229920002866 paraformaldehyde Polymers 0.000 description 2
GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 1
ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
239000002253 acid Substances 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
239000001099 ammonium carbonate Substances 0.000 description 1
235000012501 ammonium carbonate Nutrition 0.000 description 1
150000003863 ammonium salts Chemical class 0.000 description 1
238000007664 blowing Methods 0.000 description 1
229910021538 borax Inorganic materials 0.000 description 1
125000005619 boric acid group Chemical class 0.000 description 1
229910052796 boron Inorganic materials 0.000 description 1
235000013877 carbamide Nutrition 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
239000000571 coke Substances 0.000 description 1
229930003836 cresol Natural products 0.000 description 1
MIHINWMALJZIBX-UHFFFAOYSA-N cyclohexa-2,4-dien-1-ol Chemical class OC1CC=CC=C1 MIHINWMALJZIBX-UHFFFAOYSA-N 0.000 description 1
HORRDWBRNSMTIZ-UHFFFAOYSA-N diphenoxyborinic acid Chemical compound C=1C=CC=CC=1OB(O)OC1=CC=CC=C1 HORRDWBRNSMTIZ-UHFFFAOYSA-N 0.000 description 1
UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 description 1
239000000839 emulsion Substances 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
235000019441 ethanol Nutrition 0.000 description 1
230000009970 fire resistant effect Effects 0.000 description 1
235000011187 glycerol Nutrition 0.000 description 1
150000002366 halogen compounds Chemical class 0.000 description 1
230000020169 heat generation Effects 0.000 description 1
239000008240 homogeneous mixture Substances 0.000 description 1
239000012774 insulation material Substances 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
229920003986 novolac Polymers 0.000 description 1
239000003921 oil Substances 0.000 description 1
239000002245 particle Substances 0.000 description 1
239000003208 petroleum Substances 0.000 description 1
235000021317 phosphate Nutrition 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
239000004848 polyfunctional curative Substances 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
239000003380 propellant Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000004328 sodium tetraborate Substances 0.000 description 1
235000010339 sodium tetraborate Nutrition 0.000 description 1
238000007711 solidification Methods 0.000 description 1
230000008023 solidification Effects 0.000 description 1
239000000126 substance Substances 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
150000003672 ureas Chemical class 0.000 description 1
229940099259 vaseline Drugs 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0066—Use of inorganic compounding ingredients
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0014—Use of organic additives
- C08J9/0047—Use of organic additives containing boron
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/38—Boron-containing compounds
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2361/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers
- C08J2361/04—Condensation polymers of aldehydes or ketones with phenols only
- C08J2361/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Inorganic Chemistry (AREA)
Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
Compositions Of Macromolecular Compounds (AREA)

CH387462A 1961-04-18 1962-03-30 Verfahren zur Herstellung schwer entflammbarer Phenolharz-Schaumstoffe CH410396A (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DED35870A DE1230557B (de)	1961-04-18	1961-04-18	Schwer entflammbare Phenolharzschaumstoffe

Publications (1)

Publication Number	Publication Date
CH410396A true CH410396A (de)	1966-03-31

Family

ID=7042837

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH387462A CH410396A (de)	1961-04-18	1962-03-30	Verfahren zur Herstellung schwer entflammbarer Phenolharz-Schaumstoffe

Country Status (8)

Country	Link
AT (1)	AT244599B (fr)
BE (1)	BE616587A (fr)
CH (1)	CH410396A (fr)
DE (1)	DE1230557B (fr)
FR (1)	FR1319889A (fr)
GB (1)	GB973835A (fr)
NL (1)	NL130445C (fr)
OA (1)	OA01653A (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2220366B1 (fr) *	1973-03-05	1976-05-21	Saint Gobain
US4071481A (en) *	1974-02-25	1978-01-31	Saint-Gobain Industries	Manufacture of phenolic foam
GB2343181A (en) *	1998-10-30	2000-05-03	Kingspan Ind Insulation Limite	A phenolic foam
DE102020005288B4 (de)	2020-08-28	2025-07-17	Bakelite Gmbh	Feuerfestes Umhüllungsmaterial für entzündliche und/oder brennbare Materialien eine Schaumharzzusammensetzung auf der Basis von Novolaken enthaltend, Verfahren zur Herstellung und Verwendung

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE537367C (de) *	1928-12-14	1931-11-02	Erich Asser Dr	Verfahren zur Erhoehung des Schmelzpunktes von Novolaken und den daraus mit natuerlichen Harzsaeuren bereiteten oelloeslichen Verbindungen
BE506553A (fr) *	1950-10-21
GB818574A (en) *	1957-04-12	1959-08-19	British Plimber Ltd	Method of producing chip-boards or -panels, and chip-boards or -panels produced by the method

1961
- 1961-04-17 FR FR894782A patent/FR1319889A/fr not_active Expired
- 1961-04-18 DE DED35870A patent/DE1230557B/de active Pending
1962
- 1962-03-30 CH CH387462A patent/CH410396A/de unknown
- 1962-04-02 AT AT266662A patent/AT244599B/de active
- 1962-04-16 NL NL277281A patent/NL130445C/xx active
- 1962-04-16 GB GB14704/62A patent/GB973835A/en not_active Expired
- 1962-04-18 BE BE616587A patent/BE616587A/fr unknown
1964
- 1964-12-31 OA OA51885A patent/OA01653A/fr unknown

Also Published As

Publication number	Publication date
FR1319889A (fr)	1963-03-01
NL277281A (nl)	1964-10-26
AT244599B (de)	1966-01-10
GB973835A (en)	1964-10-28
NL130445C (nl)	1971-01-15
OA01653A (fr)	1969-09-20
BE616587A (fr)	1962-08-16
DE1230557B (de)	1966-12-15

Publication	Publication Date	Title
EP0037470B1 (fr)	1985-06-19	Procédé pour la préparation de mousses élastiques à base d'un produit de condensation du formaldéhyde avec la mélamine
EP0017672B1 (fr)	1983-04-27	Mousse élastique à base d'un produit de condensation mélamine-formaldéhyde et son application
DE1569493B2 (fr)	1976-01-08
DE2717775C3 (de)	1980-07-10	Phenolharz-Schaumstoff
EP0017671B1 (fr)	1983-01-12	Procédé pour la préparation de mousses élastiques à base de résines mélamine-formaldéhyde
DE3244779C1 (de)	1984-04-12	Nicht brennbarer Hartschaum und seine Verwendung als Baustoff
DE19910257A1 (de)	2000-09-21	Flammhemmend ausgerüstete Schaumstoffe auf Basis von Styrolpolymerisaten
DE1236183B (de)	1967-03-09	Verfahren zur Herstellung von Phenolharzschaumstoffen
EP0010714A1 (fr)	1980-05-14	Matières intumescentes résistant à la flamme, procédé pour leur fabrication et leur utilisation
DE69313548T2 (de)	1998-01-15	Verfahren zur Herstellung von hauptsächlich geschlossenzelligem Phenolharzschaum
DE3244523A1 (de)	1984-06-07	Verfahren zur herstellung von wasserglasschaumstoffen aus aerosoldosen
DE1920867C3 (de)	1975-10-02	Verfahren zur Herstellung von Phenolharzschaumstoffen
EP3333216B1 (fr)	2020-05-06	Mousses en matière plastique ignifuges
DE1230557B (de)	1966-12-15	Schwer entflammbare Phenolharzschaumstoffe
DE602004006376T2 (de)	2008-01-10	Phenolharzschaumstoff
DE3007151C2 (de)	1983-10-27	Verfahren zur Herstellung von Aminoharzschaum
CH517142A (de)	1971-12-31	Harz
DE1569490A1 (de)	1970-04-16	Verfahren zur Herstellung von Schaumstoffen
DE1917012A1 (de)	1970-10-15	Phenolharzschaumstoff mit verminderter Schrumpfneigung
DE2453658C3 (de)	1981-01-08	Verwendung von wässrigen Furanharzmischkondensaten in Mischung mit porösen organischen oder anorganischen Stoffen zur Herstellung von brandfesten Isolierstoffen
DE2625811A1 (de)	1976-12-16	Verschaeumbare kunststoffmasse
DE2549219A1 (de)	1977-03-31	Waerme-, schall- und feuer-daemmende leichtbaustoffe und verfahren zu deren herstellung
DE1569491C3 (fr)	1975-10-30
DE2124811B2 (de)	1978-11-16	Feuerfeste Schaumstoffplatte
DE1936848A1 (de)	1971-02-04	Verfahren zur Herstellung von Schaumstoffen auf Aminoplastharzbasis mit verminderter Rissanfaelligkeit