CH618946A5 - Process for producing hydrogen peroxide. - Google Patents
Process for producing hydrogen peroxide. Download PDFInfo
- Publication number
- CH618946A5 CH618946A5 CH942076A CH942076A CH618946A5 CH 618946 A5 CH618946 A5 CH 618946A5 CH 942076 A CH942076 A CH 942076A CH 942076 A CH942076 A CH 942076A CH 618946 A5 CH618946 A5 CH 618946A5
- Authority
- CH
- Switzerland
- Prior art keywords
- hydrogen peroxide
- mixture
- working solution
- solvents
- parts
- Prior art date
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims description 76
- 238000000034 method Methods 0.000 title claims description 21
- 239000000203 mixture Substances 0.000 claims description 30
- 239000012224 working solution Substances 0.000 claims description 24
- 239000002904 solvent Substances 0.000 claims description 22
- 239000000243 solution Substances 0.000 claims description 17
- YEVQZPWSVWZAOB-UHFFFAOYSA-N 2-(bromomethyl)-1-iodo-4-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=C(I)C(CBr)=C1 YEVQZPWSVWZAOB-UHFFFAOYSA-N 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 10
- KXGCGPZBOPCNDE-UHFFFAOYSA-N 1,1-dibutyl-3,3-diethylurea Chemical compound CCCCN(CCCC)C(=O)N(CC)CC KXGCGPZBOPCNDE-UHFFFAOYSA-N 0.000 claims description 8
- 238000005984 hydrogenation reaction Methods 0.000 claims description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000011877 solvent mixture Substances 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 3
- 238000002474 experimental method Methods 0.000 claims description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims 12
- 235000013877 carbamide Nutrition 0.000 claims 9
- 238000009826 distribution Methods 0.000 claims 9
- 150000003672 ureas Chemical class 0.000 claims 8
- 229930195733 hydrocarbon Natural products 0.000 claims 6
- 150000002430 hydrocarbons Chemical class 0.000 claims 6
- 230000003647 oxidation Effects 0.000 claims 6
- 238000007254 oxidation reaction Methods 0.000 claims 6
- -1 phosphoric acid triesters Chemical class 0.000 claims 6
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 4
- 238000000605 extraction Methods 0.000 claims 4
- 239000012074 organic phase Substances 0.000 claims 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Substances OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 4
- 239000004215 Carbon black (E152) Substances 0.000 claims 3
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims 3
- 150000004056 anthraquinones Chemical class 0.000 claims 3
- 239000004202 carbamide Substances 0.000 claims 3
- 239000008346 aqueous phase Substances 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 claims 2
- 238000006243 chemical reaction Methods 0.000 claims 2
- 238000000354 decomposition reaction Methods 0.000 claims 2
- 239000002360 explosive Substances 0.000 claims 2
- 230000002349 favourable effect Effects 0.000 claims 2
- 239000012071 phase Substances 0.000 claims 2
- 239000000047 product Substances 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- AQSQFWLMFCKKMG-UHFFFAOYSA-N 1,3-dibutylurea Chemical compound CCCCNC(=O)NCCCC AQSQFWLMFCKKMG-UHFFFAOYSA-N 0.000 claims 1
- HXQPUEQDBSPXTE-UHFFFAOYSA-N Diisobutylcarbinol Chemical compound CC(C)CC(O)CC(C)C HXQPUEQDBSPXTE-UHFFFAOYSA-N 0.000 claims 1
- 206010016275 Fear Diseases 0.000 claims 1
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 239000006227 byproduct Substances 0.000 claims 1
- 238000005474 detonation Methods 0.000 claims 1
- 238000004090 dissolution Methods 0.000 claims 1
- 230000007257 malfunction Effects 0.000 claims 1
- IMXBRVLCKXGWSS-UHFFFAOYSA-N methyl 2-cyclohexylacetate Chemical compound COC(=O)CC1CCCCC1 IMXBRVLCKXGWSS-UHFFFAOYSA-N 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
- 239000010452 phosphate Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 238000004064 recycling Methods 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- UOHMMEJUHBCKEE-UHFFFAOYSA-N prehnitene Chemical compound CC1=CC=C(C)C(C)=C1C UOHMMEJUHBCKEE-UHFFFAOYSA-N 0.000 description 10
- SJEBAWHUJDUKQK-UHFFFAOYSA-N 2-ethylanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(CC)=CC=C3C(=O)C2=C1 SJEBAWHUJDUKQK-UHFFFAOYSA-N 0.000 description 7
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 4
- KTZJYNVXLDZRMV-UHFFFAOYSA-N 2-ethyl-1,2,3,4,4a,5,6,7,9a,10a-decahydroanthracene-9,10-dione Chemical compound C1CCC2C(=O)C3CCC(CC)CC3C(=O)C2=C1 KTZJYNVXLDZRMV-UHFFFAOYSA-N 0.000 description 3
- JORLUGVBYJSSAW-UHFFFAOYSA-N 2-ethyl-1,2,3,4-tetrahydroanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1CC(CC)CC2 JORLUGVBYJSSAW-UHFFFAOYSA-N 0.000 description 3
- PCKKNFLLFBDNPA-UHFFFAOYSA-N 1,1-dibutylurea Chemical compound CCCCN(C(N)=O)CCCC PCKKNFLLFBDNPA-UHFFFAOYSA-N 0.000 description 1
- YIZOOZLBTNDTMU-UHFFFAOYSA-N 1,3-dibutyl-1,3-diethylurea Chemical compound CCCCN(CC)C(=O)N(CC)CCCC YIZOOZLBTNDTMU-UHFFFAOYSA-N 0.000 description 1
- RKMPHYRYSONWOL-UHFFFAOYSA-N 1-ethyl-1,2,3,4-tetrahydroanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C(CC)CCC2 RKMPHYRYSONWOL-UHFFFAOYSA-N 0.000 description 1
- HSKPJQYAHCKJQC-UHFFFAOYSA-N 1-ethylanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2CC HSKPJQYAHCKJQC-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 1
- CNWSQCLBDWYLAN-UHFFFAOYSA-N butylurea Chemical compound CCCCNC(N)=O CNWSQCLBDWYLAN-UHFFFAOYSA-N 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752532819 DE2532819C3 (de) | 1975-07-23 | 1975-07-23 | Verfahren zur Herstellung von Wasserstoffperoxid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH618946A5 true CH618946A5 (en) | 1980-08-29 |
Family
ID=5952180
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH942076A CH618946A5 (en) | 1975-07-23 | 1976-07-22 | Process for producing hydrogen peroxide. |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS5231998A (fr) |
| AR (1) | AR217242A1 (fr) |
| AT (1) | AT354976B (fr) |
| BE (1) | BE844424A (fr) |
| BR (1) | BR7604689A (fr) |
| CA (1) | CA1089631A (fr) |
| CH (1) | CH618946A5 (fr) |
| DE (1) | DE2532819C3 (fr) |
| FR (1) | FR2318820A1 (fr) |
| GB (1) | GB1524883A (fr) |
| IT (1) | IT1063139B (fr) |
| NL (1) | NL184942B (fr) |
| SE (1) | SE418489B (fr) |
| SU (1) | SU676158A3 (fr) |
| TR (1) | TR19375A (fr) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3027253C2 (de) * | 1980-07-18 | 1982-11-04 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von Wasserstoffperoxid |
| SE459919C (sv) * | 1987-03-27 | 1991-03-25 | Eka Nobel Ab | Foerfarande foer framstaellning av vaeteperoxid genom reduktion och oxidation av en antrakinon |
| SE508111C2 (sv) * | 1996-12-23 | 1998-08-31 | Kvaerner Process Systems As | Förfarande för framställning av väteperoxid genom hydrering av en kinonlösning samt anordning för utövande av förfarandet |
| DE60140939D1 (de) | 2000-06-19 | 2010-02-11 | Akzo Nobel Nv | Nd darin verwendete zusammensetzung |
| CZ299805B6 (cs) * | 2000-06-19 | 2008-12-03 | Akzo Nobel N. V. | Zpusob výroby peroxidu vodíku a kompozice použitelná pro provádení tohoto zpusobu |
| CN117509553A (zh) * | 2022-07-29 | 2024-02-06 | 中国石油化工股份有限公司 | 蒽醌法生产过氧化氢的工作液和过氧化氢的生产方法 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4046868A (en) * | 1973-09-26 | 1977-09-06 | E. I. Du Pont De Nemours And Company | Production of hydrogen peroxide |
-
1975
- 1975-07-23 DE DE19752532819 patent/DE2532819C3/de not_active Expired
-
1976
- 1976-06-15 NL NL7606456A patent/NL184942B/xx not_active IP Right Cessation
- 1976-07-05 IT IT6867276A patent/IT1063139B/it active
- 1976-07-07 TR TR1937576A patent/TR19375A/xx unknown
- 1976-07-15 SU SU762381095A patent/SU676158A3/ru active
- 1976-07-15 AR AR26396076A patent/AR217242A1/es active
- 1976-07-19 BR BR7604689A patent/BR7604689A/pt unknown
- 1976-07-20 GB GB3012076A patent/GB1524883A/en not_active Expired
- 1976-07-21 FR FR7622302A patent/FR2318820A1/fr active Granted
- 1976-07-22 CH CH942076A patent/CH618946A5/de not_active IP Right Cessation
- 1976-07-22 CA CA257,531A patent/CA1089631A/fr not_active Expired
- 1976-07-22 JP JP8770876A patent/JPS5231998A/ja active Pending
- 1976-07-22 SE SE7608379A patent/SE418489B/xx not_active IP Right Cessation
- 1976-07-22 BE BE6045617A patent/BE844424A/fr not_active IP Right Cessation
- 1976-07-22 AT AT540276A patent/AT354976B/de active
Also Published As
| Publication number | Publication date |
|---|---|
| IT1063139B (it) | 1985-02-11 |
| SE7608379L (sv) | 1977-01-24 |
| DE2532819A1 (de) | 1977-01-27 |
| FR2318820A1 (fr) | 1977-02-18 |
| JPS5231998A (en) | 1977-03-10 |
| DE2532819B2 (de) | 1978-01-26 |
| NL7606456A (nl) | 1977-01-25 |
| DE2532819C3 (de) | 1978-10-05 |
| FR2318820B1 (fr) | 1980-06-27 |
| TR19375A (tr) | 1979-02-20 |
| CA1089631A (fr) | 1980-11-18 |
| SE418489B (sv) | 1981-06-09 |
| BR7604689A (pt) | 1977-08-02 |
| SU676158A3 (ru) | 1979-07-25 |
| AT354976B (de) | 1980-02-11 |
| GB1524883A (en) | 1978-09-13 |
| NL184942B (nl) | 1989-07-17 |
| BE844424A (fr) | 1977-01-24 |
| ATA540276A (de) | 1979-07-15 |
| AR217242A1 (es) | 1980-03-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE69203181T2 (de) | Verfahren zur Gewinnung von wässrigen Wasserstoff-Peroxidlösungen. | |
| DE69913883T2 (de) | Verfahren und Anlage zur Herstellung einer wässerigen Wasserstoffperoxydlösung und wässerige Wasserstoffperoxydlösung | |
| DE60025143T2 (de) | Verfahren und Zusammensetzung zur Herstellung von Wasserstoffperoxid | |
| WO1999052819A1 (fr) | Procede pour preparer du peroxyde d'hydrogene et support de reaction utilise pour le mettre en oeuvre | |
| DE1241935B (de) | Verfahren zum Entfernen von Schwefelwasserstoff aus Gasen | |
| DE69314445T2 (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| DE3027253C2 (de) | Verfahren zur Herstellung von Wasserstoffperoxid | |
| CH618946A5 (en) | Process for producing hydrogen peroxide. | |
| DE1567640C3 (de) | Verfahren zur Herstellung von Wasserstoffperoxid | |
| DE69905847T2 (de) | Herstellung von Wasserstoffperoxid nach einem zyklischen Anthrachinonverfahren | |
| DE1467122A1 (de) | Verfahren und Herstellung von Wasserstoffsuperoxyd | |
| DE602004005212T2 (de) | Verfahren zur herstellung von wasserstoffperoxyd nach dem zyklischen anthrachinonverfahren | |
| EP1274651A1 (fr) | Procede de production de peroxyde d'hydrogene | |
| DE2018686C3 (de) | Verfahren zur Herstellung von Was serstoffperoxid | |
| DE2419534C2 (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| DE953790C (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| DE1112051B (de) | Kreislaufverfahren zur Herstellung von Wasserstoffperoxyd | |
| DE958917C (de) | Verfahren zur Herstellung von Wasserstoffperoxyd durch Hydrierung und Oxydierung von Anthrachinonen | |
| DE892747C (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| CH476633A (de) | Verfahren zur Herstellung von Wasserstoffsuperoxyd | |
| AT237570B (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| AT211790B (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| EP0038969A1 (fr) | Procédé pour traiter une solution aqueuse alcaline de sels d'acide anthraquinone-disulfonique | |
| DE1195279B (de) | Verfahren zur Herstellung von Wasserstoff-peroxyd im Kreislauf | |
| DE1055513B (de) | Verfahren zum Reaktivieren des bei der Herstellung von Wasserstoffperoyxd ueber organische Verbindungen verwendeten Katalysators |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PL | Patent ceased |