CH96342A - Process for removing carbon from metals with a high melting temperature. - Google Patents

Process for removing carbon from metals with a high melting temperature.

Info

Publication number
CH96342A
CH96342A CH96342DA CH96342A CH 96342 A CH96342 A CH 96342A CH 96342D A CH96342D A CH 96342DA CH 96342 A CH96342 A CH 96342A
Authority
CH
Switzerland
Prior art keywords
carbon
metals
melting temperature
high melting
removing carbon
Prior art date
Application number
Other languages
German (de)
Inventor
Lohmann-Metall G M B H
Original Assignee
Lohmann Metall G M B H
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lohmann Metall G M B H filed Critical Lohmann Metall G M B H
Publication of CH96342A publication Critical patent/CH96342A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Carbon And Carbon Compounds (AREA)

Description

  

  Verfahren zur Entfernung des     Kohlenstoffes    aus     IVIetallen    von hoher Schmelztemperatur.    Die Entfernung von Kohlenstoff aus  manchen Metallen, wie z. B. Eisen, die durch  einen     Schmelzprozess    im     Kohletiegel    Kohlen  stoff aufgenommen haben, kann durch das  sogenannte Tempern erfolgen.

   Dieses Verfah  ren versagt aber bei Metallen von hoher  Schmelztemperatur, da die zum     Tempern    er  forderlichen sauerstoffhaltigen     Einhüllungen     nur niedrige Temperaturen vertragen, bei  hohen Temperaturen jedoch sehr stark     zusam-          mensintern    und dann den Kohlenstoff     nicht     in der beim Tempern von Eisen erkennbaren  Weise entfernen, sondern eine neue Oxyda  tion des Werkmaterials herbeiführen.  



  Das vorliegende Verfahren beruht auf der  Erkenntnis, dass der Kohlenstoff aus hoch  schmelzenden Metallen, wie Wolfram, Tau  tal,     Molybdän,    Uran, Titan und Bor, in Gas  form entweicht, wenn die zu bearbeitenden  Werkstücke einer Erhitzung bis dicht an den  Schmelzpunkt der Metalle unterworfen wer  den.     Wolfram-Metall    schmilzt beispielsweise  bei<B>2990';</B> eine merkliche     Entweichung    von  Kohlenstoff     kann    schon bei ca.     2300-2400'     beobachtet werden, ohne dass ein oxydieren-    des Reagenz, wie ein Oxyd, Sauerstoff und  dergleichen, vorhanden wäre.  



  Das Verfahren     wird    so ausgeführt, dass  das kohlenstoffhaltige Metall in einem luft  dicht geschlossenen Behälter hoch erhitzt  wird, und dass der dadurch verdampfende  Kohlenstoff durch Absaugen     mittelst        einer     Vakuumpumpe, sowie eines keinen Kohlen  stoff enthaltenden indifferenten Gases ent  fernt wird, ohne dass das Metall in den.  schmelzflüssigen Zustand übergeführt     wird.  



  Process for removing the carbon from high melting temperature metals. The removal of carbon from some metals, such as B. Iron, which have taken up carbon through a melting process in the carbon crucible, can be done by so-called annealing.

   However, this process fails in the case of metals with a high melting temperature, since the oxygen-containing envelopes required for tempering can only tolerate low temperatures, but at high temperatures they are very strongly sintered and then do not remove the carbon in the manner recognizable when iron is tempered, but rather one bring about new oxidation of the material.



  The present process is based on the knowledge that the carbon from high-melting metals such as tungsten, tau tal, molybdenum, uranium, titanium and boron escapes in gaseous form when the workpieces to be processed are subjected to heating close to the melting point of the metals will. Tungsten metal melts, for example, at <B> 2990 '; </B> a noticeable escape of carbon can already be observed at approx. 2300-2400' without an oxidizing reagent such as an oxide, oxygen and the like being present would.



  The method is carried out in such a way that the carbon-containing metal is heated to a high temperature in an airtight container, and that the carbon that evaporates as a result is removed by suction using a vacuum pump and a non-carbon-containing inert gas without the metal entering the . molten state is transferred.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Entfernung des Kohlen stoffes aus Metallei. von hoher Schmelztem peratur, wie Wolfram, Tantal, Molybdän. Uran, Titan und Bor, dadurch gekennzeich net, dass das kohlenstoffhaltige Metall in einem luftdicht geschlossenen Behälter hoch erhitzt wird und dass der dadurch verdamp fende Kohlenstoff durch Absaugen mittelst einer Vakuumpumpe, sowie eines keinen Kohlenstoff enthaltenden .indifferenten Ga ses entfernt wird, ohne dass das Metall in den schmelzflüssigen Zustand übergeführt wird. PATENT CLAIM: Process for removing the carbon from Metalllei. of high melting temperature, such as tungsten, tantalum, molybdenum. Uranium, titanium and boron, characterized in that the carbon-containing metal is heated up in an airtight container and that the carbon that evaporates as a result is removed by suction using a vacuum pump and an indifferent gas that does not contain carbon, without this Metal is converted into the molten state.
CH96342D 1919-01-13 1921-03-30 Process for removing carbon from metals with a high melting temperature. CH96342A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE157780X 1919-01-13

Publications (1)

Publication Number Publication Date
CH96342A true CH96342A (en) 1922-10-02

Family

ID=5679006

Family Applications (1)

Application Number Title Priority Date Filing Date
CH96342D CH96342A (en) 1919-01-13 1921-03-30 Process for removing carbon from metals with a high melting temperature.

Country Status (4)

Country Link
AT (1) AT95311B (en)
CH (1) CH96342A (en)
GB (1) GB157780A (en)
NL (1) NL14373C (en)

Also Published As

Publication number Publication date
AT95311B (en) 1923-12-27
GB157780A (en) 1922-03-09
NL14373C (en) 1926-07-15

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