CN100455565C - 磺酰胺阴离子用作nco低聚反应的催化剂 - Google Patents

磺酰胺阴离子用作nco低聚反应的催化剂 Download PDF

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Publication number
CN100455565C
CN100455565C CNB2004800225141A CN200480022514A CN100455565C CN 100455565 C CN100455565 C CN 100455565C CN B2004800225141 A CNB2004800225141 A CN B2004800225141A CN 200480022514 A CN200480022514 A CN 200480022514A CN 100455565 C CN100455565 C CN 100455565C
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CN
China
Prior art keywords
oligomerization
catalyst
isocyanate
mmol
general formula
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Expired - Fee Related
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CNB2004800225141A
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English (en)
Chinese (zh)
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CN1833003A (zh
Inventor
J·科切
R·哈尔帕普
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Covestro Deutschland AG
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Bayer MaterialScience AG
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Publication of CN1833003A publication Critical patent/CN1833003A/zh
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Anticipated expiration legal-status Critical
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/22—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with hetero atoms directly attached to ring nitrogen atoms
    • C07D295/28—Nitrogen atoms
    • C07D295/30—Nitrogen atoms non-acylated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D241/00—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings
    • C07D241/02—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings not condensed with other rings
    • C07D241/10—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D241/14—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D241/20—Nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D261/00—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings
    • C07D261/02—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings
    • C07D261/06—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having two or more double bonds between ring members or between ring members and non-ring members
    • C07D261/10—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having two or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D261/14—Nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D277/00—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
    • C07D277/02—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings
    • C07D277/20—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D277/32—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D277/38—Nitrogen atoms
    • C07D277/50—Nitrogen atoms bound to hetero atoms
    • C07D277/52—Nitrogen atoms bound to hetero atoms to sulfur atoms, e.g. sulfonamides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
    • C08G18/022—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only the polymeric products containing isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
    • C08G18/027—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only the polymeric products containing urethodione groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1883—Catalysts containing secondary or tertiary amines or salts thereof having heteroatoms other than oxygen and nitrogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
CNB2004800225141A 2003-08-07 2004-07-26 磺酰胺阴离子用作nco低聚反应的催化剂 Expired - Fee Related CN100455565C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10336186A DE10336186A1 (de) 2003-08-07 2003-08-07 Sulfonamid-Anionen als Katalysatoren für die NCO-Oligomerisierung
DE10336186.3 2003-08-07

Publications (2)

Publication Number Publication Date
CN1833003A CN1833003A (zh) 2006-09-13
CN100455565C true CN100455565C (zh) 2009-01-28

Family

ID=34111992

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2004800225141A Expired - Fee Related CN100455565C (zh) 2003-08-07 2004-07-26 磺酰胺阴离子用作nco低聚反应的催化剂

Country Status (11)

Country Link
US (1) US7060817B2 (de)
EP (1) EP1654324B1 (de)
JP (1) JP2007501769A (de)
KR (1) KR20060118401A (de)
CN (1) CN100455565C (de)
AT (1) ATE349494T1 (de)
CA (1) CA2534850A1 (de)
DE (2) DE10336186A1 (de)
ES (1) ES2279399T3 (de)
MX (1) MXPA06001441A (de)
WO (1) WO2005017037A1 (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10336184A1 (de) * 2003-08-07 2005-02-24 Bayer Materialscience Ag Neue Katalysatoren für die selektive Isocyanatdimerisierung
DE102004048775A1 (de) * 2004-10-07 2006-04-13 Degussa Ag Hoch reaktive uretdiongruppenhaltige Polyurethanzusammensetzungen
DE102006023262A1 (de) * 2006-05-18 2007-11-22 Bayer Materialscience Ag Neue Katalysatoren für die selektive Isocyanatdimerisierung
US20100198734A1 (en) * 2008-10-31 2010-08-05 The Carlar Group Method and System for Integrating an Entertainment-Based Project with a Method and System from the Financial Protocol of a Financial Institution Via a Communications Network
CN102245665B (zh) * 2008-11-10 2013-11-13 陶氏环球技术有限责任公司 一种异氰酸酯三聚催化剂体系，前体制剂，使异氰酸酯三聚的方法，由其制备的硬质多异氰脲酸酯/聚氨酯泡沫体，和制备这种泡沫体的方法
KR101702704B1 (ko) * 2013-07-23 2017-02-03 제일모직주식회사 포스포늄 이온 함유 화합물, 이를 포함하는 에폭시수지 조성물, 및 이를 사용하여 제조된 장치
CN114112965B (zh) * 2020-08-31 2024-04-09 万华化学集团股份有限公司 一种检测异氰酸酯中痕量水分的方法及其在线监控的应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4324879A (en) * 1978-09-08 1982-04-13 Bayer Aktiengesellschaft Process for the preparation of polyisocyanates containing isocyanurate groups and the use thereof
US4960848A (en) * 1988-04-27 1990-10-02 Bayer Aktiengesellschaft Process for the production of polyisocyanates containing isocyanurate groups and their use
CN1103409A (zh) * 1994-07-22 1995-06-07 广东省肇庆星湖化工企业集团公司 封闭异氰酸酯固化剂的生产方法
US20030013872A1 (en) * 2001-05-14 2003-01-16 Hans-Josef Laas Method of dimerizing isophorone diisocyanate

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE584820A (de) * 1957-09-25
US3619338A (en) * 1968-05-14 1971-11-09 Monsanto Res Corp Glass fabric sheets bonded together with polyisocyanurates prepared from an organic diisocyanate and a monoisocyanate using ionic polymerization catalysts
US4022721A (en) * 1974-09-26 1977-05-10 Mitsubishi Chemical Industries Ltd. Process for producing compounds having an oxazolidone ring using a complex of aluminum halide catalyst
JPS51136622A (en) * 1975-05-21 1976-11-26 Kao Corp Process for preparation of isocyanic acid derivatives
DE3100263A1 (de) * 1981-01-08 1982-08-12 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von isocyanuratgruppen aufweisenden polyisocyanaten und ihre verwendung bei der herstellung von polyurethanen
US4423197A (en) * 1981-12-01 1983-12-27 Minnesota Mining And Manufacturing Company Cyclic perfluoroaliphatic-disulfonic acid anhydrides and sulfonamide derivatives thereof
CA1258337A (en) * 1985-02-14 1989-08-08 Samuel A. Ogoe Ignition resistant carbonate polymer with improved processing stability
DE3806276A1 (de) 1988-02-27 1989-09-07 Bayer Ag Verfahren zur herstellung von isocyanuratgruppen aufweisenden polyisocyanaten und ihre verwendung
US5410073A (en) * 1989-12-29 1995-04-25 E. I. Du Pont De Nemours And Company Manufacture of polyfluoro nitrogen containing organic compounds
US5414111A (en) * 1989-12-29 1995-05-09 E. I. Du Pont De Nemours And Company Polyfluoro nitrogen-containing organic compounds
DE19603245A1 (de) * 1996-01-30 1997-07-31 Bayer Ag Dünnschichtdestillation von Uretdiondiisocyanaten
DE19611849A1 (de) * 1996-03-26 1997-10-02 Bayer Ag Neue Isocyanattrimerisate und Isocyanattrimerisatmischungen, deren Herstellung und Verwendung
JP2000290268A (ja) * 1999-04-02 2000-10-17 Mitsui Chemicals Inc ポリイソシアナートの製造法
DE10336184A1 (de) * 2003-08-07 2005-02-24 Bayer Materialscience Ag Neue Katalysatoren für die selektive Isocyanatdimerisierung

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4324879A (en) * 1978-09-08 1982-04-13 Bayer Aktiengesellschaft Process for the preparation of polyisocyanates containing isocyanurate groups and the use thereof
US4960848A (en) * 1988-04-27 1990-10-02 Bayer Aktiengesellschaft Process for the production of polyisocyanates containing isocyanurate groups and their use
CN1103409A (zh) * 1994-07-22 1995-06-07 广东省肇庆星湖化工企业集团公司 封闭异氰酸酯固化剂的生产方法
US20030013872A1 (en) * 2001-05-14 2003-01-16 Hans-Josef Laas Method of dimerizing isophorone diisocyanate

Also Published As

Publication number Publication date
KR20060118401A (ko) 2006-11-23
HK1091852A1 (zh) 2007-01-26
CN1833003A (zh) 2006-09-13
US7060817B2 (en) 2006-06-13
US20050033005A1 (en) 2005-02-10
DE502004002481D1 (de) 2007-02-08
EP1654324A1 (de) 2006-05-10
JP2007501769A (ja) 2007-02-01
WO2005017037A1 (de) 2005-02-24
EP1654324B1 (de) 2006-12-27
DE10336186A1 (de) 2005-03-03
MXPA06001441A (es) 2006-05-15
ATE349494T1 (de) 2007-01-15
ES2279399T3 (es) 2007-08-16
CA2534850A1 (en) 2005-02-24

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