CN101805995A - Fabric finishing agent and fabric finishing method - Google Patents
Fabric finishing agent and fabric finishing method Download PDFInfo
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- CN101805995A CN101805995A CN 201010130711 CN201010130711A CN101805995A CN 101805995 A CN101805995 A CN 101805995A CN 201010130711 CN201010130711 CN 201010130711 CN 201010130711 A CN201010130711 A CN 201010130711A CN 101805995 A CN101805995 A CN 101805995A
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- finishing agent
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- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 31
- 239000000675 fabric finishing Substances 0.000 title claims abstract description 25
- 238000009962 finishing (textile) Methods 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims description 12
- 239000004744 fabric Substances 0.000 claims abstract description 34
- 239000005871 repellent Substances 0.000 claims abstract description 19
- 229910010413 TiO 2 Inorganic materials 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 36
- 239000003921 oil Substances 0.000 claims description 30
- 239000002689 soil Substances 0.000 claims description 18
- 230000002940 repellent Effects 0.000 claims description 13
- 239000007788 liquid Substances 0.000 claims description 12
- 239000000853 adhesive Substances 0.000 claims description 9
- 230000001070 adhesive effect Effects 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 3
- 238000006424 Flood reaction Methods 0.000 claims description 2
- 230000003373 anti-fouling effect Effects 0.000 abstract description 9
- 230000035699 permeability Effects 0.000 abstract description 4
- 239000011230 binding agent Substances 0.000 abstract 1
- 240000002853 Nelumbo nucifera Species 0.000 description 9
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 9
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 9
- 229920000742 Cotton Polymers 0.000 description 7
- 239000004753 textile Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000002086 nanomaterial Substances 0.000 description 5
- 238000011160 research Methods 0.000 description 5
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 229910052731 fluorine Inorganic materials 0.000 description 4
- 239000011737 fluorine Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 230000006378 damage Effects 0.000 description 3
- 239000002270 dispersing agent Substances 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 230000002045 lasting effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000004045 reactive dyeing Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- 238000001727 in vivo Methods 0.000 description 2
- 210000001161 mammalian embryo Anatomy 0.000 description 2
- 210000001595 mastoid Anatomy 0.000 description 2
- SNGREZUHAYWORS-UHFFFAOYSA-N perfluorooctanoic acid Chemical compound OC(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F SNGREZUHAYWORS-UHFFFAOYSA-N 0.000 description 2
- 230000002085 persistent effect Effects 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- -1 polytetrafluoroethylene Polymers 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 206010019851 Hepatotoxicity Diseases 0.000 description 1
- 206010029350 Neurotoxicity Diseases 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 206010044221 Toxic encephalopathy Diseases 0.000 description 1
- 229920000800 acrylic rubber Polymers 0.000 description 1
- 239000002519 antifouling agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 231100000060 cardiovascular toxicity Toxicity 0.000 description 1
- 230000007681 cardiovascular toxicity Effects 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 231100000025 genetic toxicology Toxicity 0.000 description 1
- 230000001738 genotoxic effect Effects 0.000 description 1
- 231100000304 hepatotoxicity Toxicity 0.000 description 1
- 230000007686 hepatotoxicity Effects 0.000 description 1
- 231100000386 immunotoxicity Toxicity 0.000 description 1
- 230000007688 immunotoxicity Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 231100000228 neurotoxicity Toxicity 0.000 description 1
- 230000007135 neurotoxicity Effects 0.000 description 1
- 239000008041 oiling agent Substances 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000003075 superhydrophobic effect Effects 0.000 description 1
- 238000009988 textile finishing Methods 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
一种织物整理剂，包括0.5-5wt％纳米TiO2、2-10wt％粘合剂DS-5125和2-10wt％柔软剂JM-801。织物使用本发明的整理剂，经拒水、拒油和防污整理、浸轧、二次拒水、拒油和防污整理、二次浸轧、预烘和烘焙等步骤整理后，织物具有持久的拒水、拒油和防污功能，耐磨、耐水洗，并且具有良好的强力、透气性等物理机械性能。A fabric finishing agent, comprising 0.5-5wt% nano TiO 2 , 2-10wt% binder DS-5125 and 2-10wt% softener JM-801. The fabric uses the finishing agent of the present invention, and after finishing through steps such as water-repellent, oil-repellent and antifouling finishing, padding, secondary water-repellent, oil-repellent and antifouling finishing, secondary padding, pre-baking and baking, the fabric has Durable water-repellent, oil-repellent and anti-fouling functions, wear-resistant, washable, and has good physical and mechanical properties such as strength and air permeability.
Description
Technical field
The present invention relates to a kind of finishing agent of functional fabric, relate in particular to a kind of fabric finishing agent, and this finishing agent is used for the method for textile finishing, fabric has after arrangement lasting to be refused water, refuses oil and anti-pollution function.
Background technology
Water, oil are fabrics such as garment material common pollutants in daily life and work of people, particularly at the employed fabric of some particular surroundings, and the easier contamination that is subjected to water, oil.This has just proposed new performance requirement to textiles.And refuse water, refuse the contamination that oil and antifouling textile product can prevent oiliness pollutant and aqueous stain, and the textiles after arrangement changes the style of original textiles hardly, do not produce fabric damage and spot.And at occurring in nature, the structural property of super-hydrophobicity plant has caused their self-purification capacity, and this ability is claimed " lotus leaf effect ".In the research of chemical simulation living things system, super hydrophobic surface is one of relatively more active in recent years field.
It is with a long history that the fabric water, oil and soil repellent is put in order, and China is just existing water repellent finish product when Wei, Shanxi, the Six Dynasties.Nineteen fifty, U.S. DuPont (Du Pont) company takes the lead in refusing water, refusing oil and anti-soil agent as fabric with the polytetrafluoroethylene (PTFE) emulsion, and has applied for patent.Minnesota Mining and Manufacturing Company successfully synthesizes fluorine-containing alkyl acrylate copolymer subsequently, is used for the arrangement of fabric water, oil and soil repellent.The competition in market makes and refuses water, refuses oil and anti-soil agent becomes better and approaching perfection day by day.These fluorochemical repellent water, refuse oil and anti-fouling agent is main active component with PFO sulfonyl compound (PFOS); existing water repellency has the oil repellent energy again; and do not influence the original style of fiber, in a very long time, all be acknowledged as and top qualityly refuse water, refuse oil and anti-soil agent.Show according to investigation, research and develop successfully less than six months, just captured almost whole relevant market at fluorine-containing water and oil repellant anti-soil agent.
Along with the development of society and the enhancing of human environmental consciousness, particularly when ozone layer is subjected to showing great attention to of the mankind, to the also raising gradually of environmental requirement of water, oil and soil repellent finishing agent.Fluorine allows the people worry the destruction of ozone layer and the toxicity of itself to user's harm.2002 OECD (EU Economy Cooperacao e Desenvolvimento) initiated an assessment of risks, this assessment report is classified PFOS as a kind of PBT material (difficult decompose the material that can accumulate in vivo).Experimental results demonstrate that PFOS has hepatotoxicity, neurotoxicity, Cardiovascular Toxicity, genotoxicity, immunotoxicity, genetoxic and carcinogenic etc., and have persistence and height cumulative bad in vivo.Organism is taken in PFOS and can be distributed in blood and the liver, because its stability is strong, thereby is difficult to decompose by the metabolism of biology.Subsequently, U.S. environment food and agricultural sector (DEFRA) have also carried out the assessment of PBT to PFOS, and the conclusion that draws with OECD is consistent.European Parliament passed through to the bill of limiting the quantity of of PFOS, and to require each member state to include them state's laws of various countries in to the sale of PFOS and the proposal of use on October 25th, 2006.At present, U.S. EPA has proposed PFOAstewardship plan (PFOA independently cuts down plan), promptly reduces 95%, 2015 year to PFOA discharging in 2010 and reduces 100%, i.e. zero-emission.
The ecological problem of fluorine-containing water and oil repellant anti-soil agent has caused the upsurge to ecological water, oil and soil repellent arrangement research.Botanist Barthlott of Univ Bonn Germany and Neinhuis find that in the research of lotus leaf being refused the self-cleaning function of water this function is because the mastoid process and the surperficial wax of the micro nano structure of lotus leaf rough surface cause jointly.And with lotus leaf surface because nanoparticle structure arranged, and can make water, oil form smooth little ball on the surface, and the effect of not stain is referred to as " lotus leaf effect ", along with the rapid emergence of nanosecond science and technology, also make " lotus leaf effect " to become the direction of a hot topic in the water, oil and soil repellent arrangement research.
Give with the back finishing technique that weaving face fabric is functional a ubiquitous problem and be: the persistent problem of function, promptly functional fabric water-fast wash, wear-resisting problem.If can not anchor at nano material on the lining effectively, in dress or washing process, nano material just might take off from lining, make functional can not be lasting, simultaneously in the wandering and environment of nano material, easily cause environmental pollution.So give weaving face fabric functional while with the back finishing technique, keep the persistent problem of its original physical and mechanical properties and function, be that can this technology widely used key issue.
Summary of the invention
An object of the present invention is to provide a kind of fabric finishing agent, solve common fabric behind functional treatment, gas permeability descends, its functional unendurable problem.
Another object of the present invention provides a kind of fabric finishing method, improves fabric and has and refuse water, refuse oil and antifouling ability, simplifies preparation process, enlarges the scope of application.
A kind of fabric finishing agent of the present invention mainly comprises the 0.5-5wt% nano-TiO
2, 2-10wt% adhesive DS-5125 (polyacrylate, Guangdong Demei Fine Chemical Co., Ltd. provides) and 2-10wt% softener JM-801 (hydrophilic silicon oil finishing agent, Zhejiang Jiamin Plastic Co provides).
Preferred fabric finishing agent mainly comprises the 1.5wt% nano-TiO
2, 5wt% adhesive DS-5125 and 5wt% softener JM-801.For guaranteeing nano-TiO
2Good dispersion can add an amount of dispersant.
At first put into required nano-TiO in the unscrambled containers
2, add an amount of absolute ethyl alcohol then and (make its submergence nano-TiO
2Powder), magnetic agitation 30min, ultrasonic again dispersion 30min then adds adhesive DS-5125, softener JM-801 respectively successively, adds the required water yield again, adds a spot of dispersant simultaneously, is stirred well to form uniform nano-TiO
2Colloid obtains fabric finishing agent of the present invention.
Former cloth of the present invention is cotton embryo cloth or conventional reactive dyeing cotton.
A kind of fabric finishing method of the present invention, its preparation method is as follows:
I. refuse water, refuse oil and soil resistant finish: former cloth floods 30min at 70 ℃ in the fabric finishing agent of pH value 4.5-5.5, and former cloth and dressing liquid bath raio are 1: 30;
II. pad: normal temperature pads, pick-up rate 60-80%;
III. secondary is refused water, is refused oil and soil resistant finish: in 70 ℃, flood 30min in the fabric finishing agent of pH value 4.5-5.5;
IV. secondary pads: normal temperature pads, pick-up rate 60-80%;
V. preliminary drying: 100-120 ℃, 15-60min;
VI. cure: 150-200 ℃, 1-10min.
Fabric after fabric finishing agent arrangement of the present invention, its contact angle is more than 150 °, and refusing the water grade is more than the level Four, and it is good to refuse oil and antifouling property.
The beneficial effect that the present invention realizes:
A kind of fabric finishing agent of the present invention utilizes nano-TiO
2Property, based on " lotus leaf effect ", with the imitative Nanosurface of the imitated textiles of the mastoid process of lotus leaf micro nano structure, finely disseminated nano-TiO
2Equably attached to fabric face, make textiles have the structure of similar lotus leaf surface at random, reach and refuse water, refuse oil and anti-fouling functions.And, by the use of adhesive DS-5125 and softener JM-801, fabric after the arrangement had lasting refuse water, refuse oil and anti-pollution function, wear-resisting, water-fast washing, and have physical and mechanical propertiess such as good brute force, gas permeability.Solved common fabric behind functional treatment, gas permeability descends, its functional unendurable problem.
Finishing agent used in the present invention is a solvent with water all, and process is pollution-free, and finishing agent is reusable, helps realizing cleaning producing and environmental protection.
A kind of fabric finishing method of the present invention improves fabric and has and refuse water, refuse oil and antifouling ability, simplifies preparation process, enlarges the scope of application.The clothes of preparation or bedding etc. not only have the function of water, oil and soil repellent, and physical and mechanical properties such as brute force descends less.
The specific embodiment
Below describe technical scheme of the present invention in detail.Only for the explanation concrete grammar, the scale of this method is not subjected to the restriction of embodiment to the embodiment of the invention.
The embodiment pure cotton fabric
The base cloth specification: Gram Mass is 150.3g/m
2Through the weft yarn raw material is 25Tex * 28Tex cotton yarn; Through filling density is 360.5 * 228/10 centimetres; Former cloth is 2/1 drillipg through reactive dyeing.
The processing technology step is as follows:
(1) water, oil and soil repellent dressing liquid prescription:
Nano-TiO
2Content 1.5wt% (dressing liquid)
Adhesive DS-5125 content 5wt% (dressing liquid)
Softener JM-801 content 5wt% (dressing liquid)
Take by weighing cloth specimen earlier, calculate dressing liquid weight at 1: 30 with bath raio, according to nano-TiO
2Content, adhesive DS-5125 content, softener JM-801 content are prepared each composition.
At first put into required nano-TiO in the unscrambled containers
2, add an amount of absolute ethyl alcohol then and (make its submergence nano-TiO
2Powder), magnetic agitation 20min, ultrasonic again dispersion 20min then adds adhesive DS-5125, softener JM-801 respectively successively, adds the required water yield again, adds a spot of dispersant simultaneously, is stirred well to form uniform nano-TiO
2Colloid obtains dressing liquid.The arrangement process is as follows:
I. water, oil and soil repellent dressing liquid arrangement: former cloth is cotton embryo cloth or conventional reactive dyeing cotton, 70 ℃ of dipping 30min, dressing liquid pH value 4.5-5.5.
II. roll: normal temperature pads, pick-up rate 60-80%.
III. secondary water, oil and soil repellent dressing liquid arrangement: 70 ℃ of dipping 30min, dressing liquid pH value 4.5-5.5.
IV. secondary pads: normal temperature pads, pick-up rate 60-80%.
V. preliminary drying: 110 ℃, 30min.
VI. cure: 170 ℃, 4min.
The performance of the fabric after the fabric finishing agent arrangement sees Table 1
Table 1 refuses water, refuse the pure cotton fabric performance after oil and the antifouling processing
Claims (5)
1. a fabric finishing agent mainly comprises the 0.5-5wt% nano-TiO
2, 2-10wt% adhesive DS-5125 and 2-10wt%JM-801.
2. fabric finishing agent according to claim 1 is characterized in that described nano-TiO
2Consumption is 1.5wt%.
3. fabric finishing agent according to claim 1 is characterized in that described adhesive DS-5125 consumption is 5wt%.
4. fabric finishing agent according to claim 1 is characterized in that described softener JM-801 consumption is 5wt%.
5. fabric finishing method, its step is as follows:
I. water, oil and soil repellent arrangement: former cloth floods 30min at 70 ℃ in the described fabric finishing agent of one of claim 1-4 of pH value 4.5-5.5, and former cloth and dressing liquid bath raio are 1: 30;
II. pad: normal temperature pads, pick-up rate 60-80%;
III. secondary is refused water, is refused oil and soil resistant finish: in 70 ℃, flood 30min in the described fabric finishing agent of one of claim 1-4 of pH value 4.5-5.5;
IV. secondary pads: normal temperature pads, pick-up rate 60-80%;
V. preliminary drying: 100-120 ℃, 15-60min;
VI. cure: 150-200 ℃, 1-10min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010130711 CN101805995A (en) | 2010-03-23 | 2010-03-23 | Fabric finishing agent and fabric finishing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010130711 CN101805995A (en) | 2010-03-23 | 2010-03-23 | Fabric finishing agent and fabric finishing method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101805995A true CN101805995A (en) | 2010-08-18 |
Family
ID=42607942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201010130711 Pending CN101805995A (en) | 2010-03-23 | 2010-03-23 | Fabric finishing agent and fabric finishing method |
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| CN (1) | CN101805995A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102251407A (en) * | 2011-06-09 | 2011-11-23 | 泰安市金飞虹织造有限公司 | Treatment method for alginate fiber fabric |
| CN102454108A (en) * | 2010-10-19 | 2012-05-16 | 现代自动车株式会社 | Method for preventing stains in fabrics |
| CN102943397A (en) * | 2012-11-12 | 2013-02-27 | 王洪福 | Efficient heat-insulated uvioresistant breathable light textile garment material printing and dyeing paint and preparation method thereof |
| CN103469545A (en) * | 2013-08-21 | 2013-12-25 | 昆山铁牛衬衫厂 | Manufacturing method of easy-to-clean shirt |
| CN105951443A (en) * | 2016-06-01 | 2016-09-21 | 欣龙控股（集团）股份有限公司 | Washing resistance finishing liquid and method for producing washing resistance wood pulp composite spunlace through same |
| CN106283664A (en) * | 2016-08-26 | 2017-01-04 | 南通纺织丝绸产业技术研究院 | Hydrophobic performance can the preparation method of water-fastness fabric of selfreparing |
| CN106381701A (en) * | 2016-09-28 | 2017-02-08 | 鲁泰纺织股份有限公司 | Method suitable for treating light or white pure cotton fabric |
| CN106758140A (en) * | 2017-01-20 | 2017-05-31 | 青岛瑞诚铭机械设计有限公司 | Outer barrel making cloth is protected in a kind of elbow protector for sports |
| CN109295734A (en) * | 2018-10-10 | 2019-02-01 | 五邑大学 | Water- and oil-repellent fabric finishing agent, preparation method of water- and oil-repellent fabric, water- and oil-repellent fabric and application thereof |
| CN115075015A (en) * | 2022-06-07 | 2022-09-20 | 郑州渡森服饰有限公司 | Shrinkage-proof men trousers and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1560353A (en) * | 2004-02-24 | 2005-01-05 | 西安华捷科技发展有限责任公司 | Nano sun-resisting finishing agent and its preparation method and finishing method for textile |
-
2010
- 2010-03-23 CN CN 201010130711 patent/CN101805995A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1560353A (en) * | 2004-02-24 | 2005-01-05 | 西安华捷科技发展有限责任公司 | Nano sun-resisting finishing agent and its preparation method and finishing method for textile |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102454108A (en) * | 2010-10-19 | 2012-05-16 | 现代自动车株式会社 | Method for preventing stains in fabrics |
| CN102454108B (en) * | 2010-10-19 | 2015-11-25 | 现代自动车株式会社 | The anti-fouling method of fabric |
| CN102251407A (en) * | 2011-06-09 | 2011-11-23 | 泰安市金飞虹织造有限公司 | Treatment method for alginate fiber fabric |
| CN102251407B (en) * | 2011-06-09 | 2013-01-30 | 泰安市金飞虹织造有限公司 | Treatment method for alginate fiber fabric |
| CN102943397A (en) * | 2012-11-12 | 2013-02-27 | 王洪福 | Efficient heat-insulated uvioresistant breathable light textile garment material printing and dyeing paint and preparation method thereof |
| CN103469545A (en) * | 2013-08-21 | 2013-12-25 | 昆山铁牛衬衫厂 | Manufacturing method of easy-to-clean shirt |
| CN105951443A (en) * | 2016-06-01 | 2016-09-21 | 欣龙控股（集团）股份有限公司 | Washing resistance finishing liquid and method for producing washing resistance wood pulp composite spunlace through same |
| CN105951443B (en) * | 2016-06-01 | 2019-10-29 | 欣龙控股（集团）股份有限公司 | Water-fastness finishing fluid and its method for producing water-fastness wood pulp composite spun-laced fabric |
| CN106283664A (en) * | 2016-08-26 | 2017-01-04 | 南通纺织丝绸产业技术研究院 | Hydrophobic performance can the preparation method of water-fastness fabric of selfreparing |
| CN106283664B (en) * | 2016-08-26 | 2018-07-13 | 南通纺织丝绸产业技术研究院 | Hydrophobic performance can selfreparing water-fastness fabric preparation method |
| CN106381701A (en) * | 2016-09-28 | 2017-02-08 | 鲁泰纺织股份有限公司 | Method suitable for treating light or white pure cotton fabric |
| CN106758140A (en) * | 2017-01-20 | 2017-05-31 | 青岛瑞诚铭机械设计有限公司 | Outer barrel making cloth is protected in a kind of elbow protector for sports |
| CN109295734A (en) * | 2018-10-10 | 2019-02-01 | 五邑大学 | Water- and oil-repellent fabric finishing agent, preparation method of water- and oil-repellent fabric, water- and oil-repellent fabric and application thereof |
| CN109295734B (en) * | 2018-10-10 | 2021-06-08 | 五邑大学 | Water- and oil-repellent fabric finishing agent, preparation method of water- and oil-repellent fabric, water- and oil-repellent fabric and application thereof |
| CN115075015A (en) * | 2022-06-07 | 2022-09-20 | 郑州渡森服饰有限公司 | Shrinkage-proof men trousers and preparation method thereof |
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Application publication date: 20100818 |