CN102701774B - Thermosetting adhesive adhering and curing device - Google Patents

Thermosetting adhesive adhering and curing device Download PDF

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CN102701774B
CN102701774B CN 201210147717 CN201210147717A CN102701774B CN 102701774 B CN102701774 B CN 102701774B CN 201210147717 CN201210147717 CN 201210147717 CN 201210147717 A CN201210147717 A CN 201210147717A CN 102701774 B CN102701774 B CN 102701774B
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gas
elastic plate
inlet pipe
curing
base body
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CN102701774A (en
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金家楣
王亮
杨颖�
张建辉
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Nanjing University of Aeronautics and Astronautics
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Abstract

The invention discloses a thermosetting adhesive adhering and curing device, which comprises a pedestal and an ultrasonic vibration apparatus and a gas liquid mixing apparatus arranged in the pedestal. The ultrasonic vibration apparatus includes an elastic plate and a piezoelectric ceramic sheet, the piezoelectric ceramic sheet is arranged at the lower surface of the elastic plate, a base body support pad is arranged at the upper surface of the elastic plate, and the upper surface of the base body support pad is provided with a base body holding groove. The gas liquid mixing apparatus is arranged on the base body support pad and includes a shell having a gas inlet pipe and a gas outlet pipe, liquid is arranged in the shell, a high temperature gas for raising the temperature of the liquid to the boiling point is introduced into the gas inlet pipe, and a flow control valve is arranged on both the gas inlet pipe and the gas outlet pipe. Compared with prior arts, the inventive device can satisfy the requirements for constant temperature, constant pressure, given duration time and uniform adhering required by adhering and curing between the base bodies through thermosetting adhesive and realize mass production of base body adhering.

Description

热固化胶粘贴固化装置Heat curing adhesive paste curing device

技术领域:Technical field:

本发明涉及一种热固化胶粘贴固化装置,属于热固化胶粘贴技术领域。 The invention relates to a thermosetting adhesive pasting curing device, which belongs to the technical field of thermosetting adhesive pasting.

背景技术:Background technique:

   热固化胶是一种基体之间粘接的粘贴剂。由于热固化胶对金属有很强的粘结力,固化后的胶层具有良好的耐水、耐油、耐温、耐老化性能、不变质、不沉淀结块,可采用烘道或烘炉加温进行粘接,加注方式可采用机注或手工施注,因此广泛被金属、陶瓷等基体作为理想的粘贴剂。两种基体之间通过热固化胶粘接,需要在一定的温度和压力下,持续一段时间进行固化才能达到粘接牢固效果。目前基体粘接后的处理方式主要是通过烘炉或者烘道对热固化胶进行高温固化,同时在烘道或烘炉中对基体施加压力,才能使基体相互粘接牢固。但是烘炉或烘道的温度不易稳定控制,对基体所施加的压力波动和不均匀易导致相互粘接的基体之间的胶层在基体粘贴面分布不均匀,从而影响粘接强度和均匀度。因此,本发明针对此问题,发明一种简单的方法获得基体粘贴固化所需的恒温和恒压,使胶层在基体表面分布均匀,该热固化胶粘贴固化装置可实现热固化粘接零件的批量化生产。  Heat-curing adhesive is an adhesive for bonding between substrates. Because the heat-curing adhesive has strong adhesion to metal, the cured adhesive layer has good water resistance, oil resistance, temperature resistance, aging resistance, no deterioration, no precipitation and agglomeration, and can be heated by drying tunnel or oven For bonding, the injection method can be machine injection or manual injection, so it is widely used as an ideal adhesive for metal, ceramic and other substrates. The two substrates are bonded by heat-curing adhesive, which needs to be cured for a period of time under a certain temperature and pressure to achieve a firm bond. At present, the processing method after substrate bonding is mainly to cure the thermosetting adhesive at high temperature through an oven or oven, and at the same time apply pressure to the substrate in the oven or oven, so that the substrates can be firmly bonded to each other. However, the temperature of the oven or oven is not easy to control stably, and the pressure fluctuation and unevenness applied to the substrate may easily lead to uneven distribution of the adhesive layer between the mutually bonded substrates on the substrate bonding surface, thereby affecting the bonding strength and uniformity. . Therefore, the present invention aims at this problem, and invents a simple method to obtain the constant temperature and constant pressure required for the substrate to be pasted and cured, so that the adhesive layer is evenly distributed on the surface of the substrate. mass production.

发明内容:Invention content:

本发明旨在研发一种热固化胶粘贴固化装置,具有固化所需的恒温、恒压、胶层分布均匀的特点。 The invention aims to develop a thermal curing adhesive paste curing device, which has the characteristics of constant temperature, constant pressure and uniform distribution of adhesive layers required for curing.

本发明的热固化胶粘贴固化装置,包括基座以及设置在基座内的超声振动装置和气液混合装置,其特征在于:所述超声振动装置包括弹性板和压电陶瓷片,所述的压电陶瓷片设置在所述的弹性板的下表面,在所述的弹性板的上表面放置有基体支撑垫,基体支撑垫的上表面设置有基体放置槽;所述的气液混合装置设置在所述的基体支撑垫上,气液混合装置包括具有进气管和出气管的外壳,在外壳内设置有液体,在所述的进气管内通入使所述液体到达沸点的高温气体,在所述的进气管和出气管上均设置有流量控制阀。 The heat-curing adhesive bonding and curing device of the present invention includes a base and an ultrasonic vibration device and a gas-liquid mixing device arranged in the base, and is characterized in that: the ultrasonic vibration device includes an elastic plate and a piezoelectric ceramic sheet, and the The piezoelectric ceramic sheet is arranged on the lower surface of the elastic plate, a substrate support pad is placed on the upper surface of the elastic plate, and the upper surface of the substrate support pad is provided with a substrate placement groove; the gas-liquid mixing device is provided On the base support pad, the gas-liquid mixing device includes a shell with an air inlet pipe and an air outlet pipe, and a liquid is arranged in the shell, and a high-temperature gas that makes the liquid reach the boiling point is introduced into the air inlet pipe, and in the Both the air inlet pipe and the air outlet pipe are provided with flow control valves.

所述的基体支撑垫为橡胶垫。 The base supporting pad is a rubber pad.

所述的外壳的底板为橡胶板。 The bottom plate of the shell is a rubber plate.

所述的弹性板与所述的基座一体成型。 The elastic plate is integrally formed with the base.

本发明装置压电陶瓷粘贴在超声振动装置的弹性板上,外加电压后产生振动使弹性板上表面作均匀、连续的微幅振动,由弹性板、压电陶瓷片组和基座上表面加工形成的凹槽共同构成了超声振动槽;橡胶垫放置于超声振动槽中,由热固化胶粘贴的基体放置在橡胶垫表面加工形成的基体放置凹槽中;由外部蒸汽装置向气液混合装置置的入气管口输入蒸汽,并在气液混合装置内腔内形成气液体混合物,部分蒸汽又从出气管口输出进入外部蒸汽装置循环,经过一定时间的蒸汽冷却和循环,气液混合装置内腔的气液混合物的温度达到液体气化的沸点,并可保持恒定不变;将气液混合装置置在橡胶垫上方,即可对基体施加压力,通过流量调节阀调节蒸汽输入气液混合装置的量可以控制气液混合装置的总重量保持不变,因此可对基体提供恒定的压力,此外根据热固化胶固化所需的温度调节蒸汽中所含杂质的成分,为热固化胶固化提供恒定温度;由于弹性板的持续微幅振动,使得基体之间的胶层在基体的粘贴面分布均匀;根据实际需求增加橡胶垫的凹槽可以实现基体粘胶固化的量产化。 The piezoelectric ceramics of the device of the present invention are pasted on the elastic plate of the ultrasonic vibration device, and the vibration is generated after the voltage is applied to make the upper surface of the elastic plate vibrate uniformly and continuously with a slight amplitude, and the upper surface of the elastic plate, the piezoelectric ceramic sheet group and the base are processed. The formed grooves together constitute the ultrasonic vibration groove; the rubber pad is placed in the ultrasonic vibration groove, and the substrate pasted by the heat-curing glue is placed in the substrate placement groove formed by the surface processing of the rubber pad; the gas-liquid mixing is performed by an external steam device The steam inlet pipe installed in the device inputs steam, and forms a gas-liquid mixture in the inner cavity of the gas-liquid mixing device, and part of the steam is output from the gas outlet pipe and enters the external steam device for circulation. After a certain period of steam cooling and circulation, the gas-liquid mixing device The temperature of the gas-liquid mixture in the inner cavity reaches the boiling point of liquid vaporization and can be kept constant; the gas-liquid mixing device is placed above the rubber pad to apply pressure to the substrate and adjust the steam input gas-liquid mixing through the flow regulating valve The amount of the device can be controlled. The total weight of the gas-liquid mixing device remains constant, so a constant pressure can be provided on the substrate. In addition, the composition of impurities contained in the steam can be adjusted according to the temperature required for the curing of the heat-curing adhesive to provide Constant temperature; due to the continuous slight vibration of the elastic plate, the adhesive layer between the substrates is evenly distributed on the bonding surface of the substrate; increasing the groove of the rubber pad according to actual needs can realize the mass production of the substrate adhesive curing.

附图说明:Description of drawings:

图1是本发明装置的结构示意。 Fig. 1 is a structural representation of the device of the present invention.

图2是本发明基座与弹性板连接示意图。 Fig. 2 is a schematic diagram of the connection between the base and the elastic plate of the present invention.

图3是本发明超声振动装置结构示意图。 Fig. 3 is a schematic diagram of the structure of the ultrasonic vibration device of the present invention.

图4是支撑垫结构示意图。 Fig. 4 is a schematic diagram of the structure of the support pad.

  图5是气液混合装置结构示意图。 Figure 5 is a schematic diagram of the gas-liquid mixing device.

其中: 1.基座,2.超声振动槽,3.弹性板,4.基体支撑垫,5.基体放置槽,6.橡胶外壳, 7.进气管,8.出气管,10.蒸汽泡,11.气液混合物,12.内部空腔。 Among them: 1. Base, 2. Ultrasonic vibration groove, 3. Elastic plate, 4. Substrate support pad, 5. Substrate placement groove, 6. Rubber shell, 7. Inlet pipe, 8. Outlet pipe, 10. Steam bubble, 11. Gas-liquid mixture, 12. Internal cavity.

具体实施方式:Detailed ways:

下面结合附图,对本发明做详细说明,本发明的热固化胶粘贴固化装置,如图1所示,包括基座1和设置在基座1内的超声振动装置和气液混合装置。其中超声振动装置的结构如图3所示,由弹性板3和压电陶瓷片9构成。气液混合装置结构如图5所示,由外壳6、进气管7、出气管8、气液混合物11构成,其中外壳6可以选用橡胶材料。超声振动装置固定在基座1的上端,与基座1的上表面加工形成的凹槽构成超声振动槽2,气液混合装置设置在超声振动槽2内,在基座1的下端加工形成凹槽,凹槽的上表面为弹性板3的下表面,压电陶瓷片9粘贴在弹性板3的下表面上。也可以在弹性板上放置一层基体支撑垫4,基体支撑垫4优选橡胶垫,在橡胶垫的上表面被加工形成若干基体放置槽5。气液混合装置在输入蒸汽后,整个装置的温度、总重达到恒定不变后,放置于已安放在橡胶垫表面槽中的粘胶基体上。 The present invention will be described in detail below in conjunction with the accompanying drawings. The thermosetting adhesive curing device of the present invention, as shown in FIG. The structure of the ultrasonic vibration device is shown in FIG. 3 , which is composed of an elastic plate 3 and a piezoelectric ceramic sheet 9 . The structure of the gas-liquid mixing device is shown in Figure 5, which consists of a casing 6, an air inlet pipe 7, an air outlet pipe 8, and a gas-liquid mixture 11, wherein the casing 6 can be made of rubber. The ultrasonic vibrating device is fixed on the upper end of the base 1, and forms an ultrasonic vibrating groove 2 with the groove formed on the upper surface of the base 1. Groove, the upper surface of the groove is the lower surface of the elastic plate 3, and the piezoelectric ceramic sheet 9 is pasted on the lower surface of the elastic plate 3. It is also possible to place a layer of substrate support pad 4 on the elastic plate. The substrate support pad 4 is preferably a rubber pad, and several substrate placement grooves 5 are formed on the upper surface of the rubber pad. After the gas-liquid mixing device is input with steam, after the temperature and total weight of the whole device are constant, it is placed on the viscose substrate that has been placed in the groove on the surface of the rubber pad.

本发明是利用压电陶瓷的逆压电效应激发超声振动装置中的弹性板进行往复微幅振动,在弹性板上表面形成一个振动平面,并通过橡胶垫将振动平面的微幅振动传递至放置在橡胶垫的凹槽中的粘胶基体,使相互粘胶基体之间的胶层在粘贴面分布均匀;其次利用气液混合装置输入蒸汽的方式为粘胶基体施加恒定的压力,提供热固化胶在基体粘贴过程中所需的持续压力,同时使相互粘胶基体之间的胶层厚度压缩并均匀分布,此外气液混合橡胶装置内腔充满蒸汽、液体的气液混合物,此时内腔温度为液体的沸点,为热固化胶的固化提供恒定的温度;最后,增大固化装置的结构尺寸比例,在橡胶垫的表面加工若干凹槽,可实现基体粘胶的量产化。因此,本发明的提出的热固化胶固化装置具有以下特点: The present invention uses the inverse piezoelectric effect of piezoelectric ceramics to excite the elastic plate in the ultrasonic vibration device to perform reciprocating micro-amplitude vibration, forms a vibration plane on the surface of the elastic plate, and transmits the micro-amplitude vibration of the vibration plane to the place via the rubber pad. The viscose matrix in the groove of the rubber pad makes the adhesive layer between the viscose matrix evenly distributed on the pasting surface; secondly, the steam is input into the gas-liquid mixing device to apply a constant pressure to the viscose matrix to provide thermal curing. The continuous pressure required by the glue in the process of sticking the substrate, and at the same time compress and evenly distribute the thickness of the adhesive layer between the adhesive substrates. In addition, the inner cavity of the gas-liquid mixing rubber device is filled with steam and liquid gas-liquid mixture. At this time, the inner cavity The temperature is the boiling point of the liquid, which provides a constant temperature for the curing of the heat-curing adhesive; finally, increasing the structural size ratio of the curing device and processing several grooves on the surface of the rubber pad can realize the mass production of the base adhesive. Therefore, the thermosetting glue curing device proposed by the present invention has the following characteristics:

(1)为基体粘贴层的热固化胶固化提供恒温,温度的高低由蒸汽冷却后变为液体,再由液体气化的沸点决定,通过在蒸汽或液体中添加杂质可调节温度变化; (1) To provide a constant temperature for the curing of the heat-curing adhesive of the substrate adhesive layer. The temperature is changed from steam to liquid after cooling, and then determined by the boiling point of liquid vaporization. The temperature change can be adjusted by adding impurities to the steam or liquid;

(2)通过调节流量控制阀调节蒸汽输入和输出气液混合橡胶装置的量来控制橡胶装置的总重量,为热固化胶固化提供的恒定外部压力; (2) Control the total weight of the rubber device by adjusting the flow control valve to adjust the amount of steam input and output gas-liquid mixing rubber device, and provide a constant external pressure for the curing of the heat-curing glue;

(3)超声振动槽内的持续微幅振动通过橡胶垫传递给粘胶基体,可使基体粘贴表面的胶层在粘贴面均匀分布,大大降低相互粘接基体之间由于胶层分布不均而脱落的概率; (3) The continuous micro-vibration in the ultrasonic vibration tank is transmitted to the viscose matrix through the rubber pad, which can make the glue layer on the pasting surface of the matrix evenly distributed on the pasting surface, greatly reducing the uneven distribution of the glue layer between the mutually bonded substrates. probability of falling out;

(4)根据实际工况需求,通过增大固化装置的结构设计比例,增加橡胶垫表面的加工凹槽数量,可实现粘胶基体的批量生产。 (4) According to the needs of actual working conditions, by increasing the structural design ratio of the curing device and increasing the number of processing grooves on the surface of the rubber pad, mass production of the adhesive matrix can be realized.

下面以具体实例进行说明。压电振子是一种弹性体材料与压电陶瓷片粘贴一起形成的捕获或耗散能量的器件。众多压电器件的研究都与压电振子有关,如何使压电振子具有较佳的使用性能成为了压电器件技术突破的关键问题之一。其中由于弹性体与压电陶瓷片之间采用热固化胶粘接不佳的问题是造成压电振子性能降低的原因之一。目前采用烘道或者烘炉的方式进行压电振子粘接不可避免的会出现弹性体与压电陶瓷片之间的脱落、胶层过厚、固化效果差等结果,而通过采用本发明提出的固化装置可避免这一现象的出现。超声振动槽的持续微幅振动使弹性体与压电陶瓷之间的粘贴胶层在两者的粘贴面分布均匀,可避免胶层中断、不连续的情况;其次,气液混合橡胶装置为压电振子的粘贴提供恒定的压力和温度,可避免粘接胶层过厚、固化效果差的现象出现;最后,在橡胶垫上加工大量的压电振子放置槽,可大大缩短压电振子批量粘接的总时间,使整批压电器件的生产实现量产化。 The following will be described with specific examples. A piezoelectric vibrator is a device that captures or dissipates energy formed by pasting an elastomer material and a piezoelectric ceramic sheet. Many studies on piezoelectric devices are related to piezoelectric vibrators. How to make piezoelectric vibrators have better performance has become one of the key issues in the breakthrough of piezoelectric device technology. One of the reasons for the performance degradation of the piezoelectric vibrator is the problem of poor bonding between the elastomer and the piezoelectric ceramic sheet using a thermosetting adhesive. At present, the bonding of piezoelectric vibrators in the way of drying tunnels or ovens will inevitably lead to the results of falling off between the elastomer and the piezoelectric ceramic sheet, excessive thickness of the adhesive layer, and poor curing effect. The curing device can avoid this phenomenon. The continuous micro-vibration of the ultrasonic vibration tank makes the adhesive layer between the elastic body and the piezoelectric ceramic evenly distributed on the bonding surface of the two, which can avoid the interruption and discontinuity of the adhesive layer; secondly, the gas-liquid mixing rubber device is a press The sticking of the electric vibrator provides constant pressure and temperature, which can avoid the phenomenon that the adhesive layer is too thick and the curing effect is poor; finally, a large number of piezoelectric vibrator placement slots are processed on the rubber pad, which can greatly shorten the batch bonding of piezoelectric vibrators. The total time of the whole batch of piezoelectric devices can be mass-produced.

Claims (4)

1. a heat-curable glue is pasted solidification equipment, comprise pedestal (1) and be arranged on pedestal (1) interior ultrasonic vibration installation and Liqiud-gas mixing device, it is characterized in that: described ultrasonic vibration installation comprises elastic plate (3) and piezoelectric ceramic piece (9), described piezoelectric ceramic piece (9) is arranged on the lower surface of described elastic plate (3), upper surface at described elastic plate (3) is placed with matrix supporting pad (4), and the upper surface of matrix supporting pad (4) is provided with matrix standing groove (5); Described Liqiud-gas mixing device is arranged on described matrix supporting pad (4), Liqiud-gas mixing device comprises the shell (6) of have inlet pipe (7) and escape pipe (8), be provided with liquid in shell (6), pass into the high-temperature gas that makes described liquid arrive boiling point in described inlet pipe (7), be provided with flowrate control valve on described inlet pipe (7) and escape pipe (8).
2. heat-curable glue according to claim 1 is pasted solidification equipment, and it is characterized in that: described matrix supporting pad is rubber pad.
3. heat-curable glue according to claim 1 and 2 is pasted solidification equipment, and it is characterized in that: the base plate of described shell (6) is rubber plate.
4. heat-curable glue according to claim 3 is pasted solidification equipment, it is characterized in that: described elastic plate (3) is one-body molded with described pedestal (1).
CN 201210147717 2012-05-14 2012-05-14 Thermosetting adhesive adhering and curing device Expired - Fee Related CN102701774B (en)

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CN104505459B (en) * 2014-11-27 2017-06-30 南京航空航天大学 A kind of viscose glue solidification equipment of ring piezoelectric transducer
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