CN1030445C - 分解氯化铵水溶液的方法 - Google Patents

分解氯化铵水溶液的方法 Download PDF

Info

Publication number: CN1030445C
Authority: CN; China
Prior art keywords: lime; milk; fraction; ammonium chloride; coarse grain
Prior art date: 1990-10-10
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CN 91110654

Other languages

English (en)

Chinese (zh)

Other versions

CN1061760A (zh

Inventor

C·布尔温

P·德米利

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Solvay SA

Original Assignee

Solvay SA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1990-10-10

Filing date

1991-10-10

Publication date

1995-12-06

1991-10-10 Application filed by Solvay SA filed Critical Solvay SA

1992-06-10 Publication of CN1061760A publication Critical patent/CN1061760A/zh

1995-12-06 Application granted granted Critical

1995-12-06 Publication of CN1030445C publication Critical patent/CN1030445C/zh

2006-10-10 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 title claims abstract description 65
238000000034 method Methods 0.000 title claims abstract description 41
235000019270 ammonium chloride Nutrition 0.000 title claims abstract description 35
239000007864 aqueous solution Substances 0.000 title description 9
235000011116 calcium hydroxide Nutrition 0.000 claims abstract description 42
239000000920 calcium hydroxide Substances 0.000 claims abstract description 41
235000019738 Limestone Nutrition 0.000 claims abstract description 7
239000006028 limestone Substances 0.000 claims abstract description 7
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 24
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
239000000243 solution Substances 0.000 claims description 15
239000012452 mother liquor Substances 0.000 claims description 12
235000017557 sodium bicarbonate Nutrition 0.000 claims description 12
229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 12
238000000354 decomposition reaction Methods 0.000 claims description 8
239000000377 silicon dioxide Substances 0.000 claims description 8
238000006243 chemical reaction Methods 0.000 claims description 7
235000012239 silicon dioxide Nutrition 0.000 claims description 7
229960001866 silicon dioxide Drugs 0.000 claims description 7
239000012267 brine Substances 0.000 claims description 6
HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 claims description 6
239000000725 suspension Substances 0.000 claims description 5
SONHSLRCJYJHQE-UHFFFAOYSA-N calcium;silicic acid Chemical compound [Ca].[Ca].O[Si](O)(O)O SONHSLRCJYJHQE-UHFFFAOYSA-N 0.000 claims description 4
239000012429 reaction media Substances 0.000 claims description 4
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims 2
239000001569 carbon dioxide Substances 0.000 claims 1
229910002092 carbon dioxide Inorganic materials 0.000 claims 1
238000005259 measurement Methods 0.000 claims 1
238000000247 postprecipitation Methods 0.000 claims 1
238000004519 manufacturing process Methods 0.000 abstract description 6
239000003513 alkali Substances 0.000 abstract 1
JHLNERQLKQQLRZ-UHFFFAOYSA-N calcium silicate Chemical compound [Ca+2].[Ca+2].[O-][Si]([O-])([O-])[O-] JHLNERQLKQQLRZ-UHFFFAOYSA-N 0.000 abstract 1
229910052918 calcium silicate Inorganic materials 0.000 abstract 1
235000012241 calcium silicate Nutrition 0.000 abstract 1
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 27
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 15
ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 13
229910021529 ammonia Inorganic materials 0.000 description 13
235000008733 Citrus aurantifolia Nutrition 0.000 description 10
240000006909 Tilia x europaea Species 0.000 description 10
235000011941 Tilia x europaea Nutrition 0.000 description 10
239000004571 lime Substances 0.000 description 10
239000000292 calcium oxide Substances 0.000 description 7
235000012255 calcium oxide Nutrition 0.000 description 7
235000017550 sodium carbonate Nutrition 0.000 description 7
229910000029 sodium carbonate Inorganic materials 0.000 description 7
235000019739 Dicalciumphosphate Nutrition 0.000 description 6
239000001506 calcium phosphate Substances 0.000 description 6
NEFBYIFKOOEVPA-UHFFFAOYSA-K dicalcium phosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])([O-])=O NEFBYIFKOOEVPA-UHFFFAOYSA-K 0.000 description 6
229940038472 dicalcium phosphate Drugs 0.000 description 6
229910000390 dicalcium phosphate Inorganic materials 0.000 description 6
239000007789 gas Substances 0.000 description 6
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 4
238000004821 distillation Methods 0.000 description 4
239000000843 powder Substances 0.000 description 4
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
238000010521 absorption reaction Methods 0.000 description 3
239000000908 ammonium hydroxide Substances 0.000 description 3
238000001354 calcination Methods 0.000 description 3
239000011575 calcium Substances 0.000 description 3
229910052791 calcium Inorganic materials 0.000 description 3
239000012535 impurity Substances 0.000 description 3
229910052710 silicon Inorganic materials 0.000 description 3
239000010703 silicon Substances 0.000 description 3
239000007787 solid Substances 0.000 description 3
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
230000002378 acidificating effect Effects 0.000 description 2
238000003763 carbonization Methods 0.000 description 2
238000002425 crystallisation Methods 0.000 description 2
230000008025 crystallization Effects 0.000 description 2
230000007812 deficiency Effects 0.000 description 2
238000010586 diagram Methods 0.000 description 2
230000036571 hydration Effects 0.000 description 2
238000006703 hydration reaction Methods 0.000 description 2
NAPPWIFDUAHTRY-XYDRQXHOSA-N (8r,9s,10r,13s,14s,17r)-17-ethynyl-17-hydroxy-13-methyl-1,2,6,7,8,9,10,11,12,14,15,16-dodecahydrocyclopenta[a]phenanthren-3-one;(8r,9s,13s,14s,17r)-17-ethynyl-13-methyl-7,8,9,11,12,14,15,16-octahydro-6h-cyclopenta[a]phenanthrene-3,17-diol Chemical compound O=C1CC[C@@H]2[C@H]3CC[C@](C)([C@](CC4)(O)C#C)[C@@H]4[C@@H]3CCC2=C1.OC1=CC=C2[C@H]3CC[C@](C)([C@](CC4)(O)C#C)[C@@H]4[C@@H]3CCC2=C1 NAPPWIFDUAHTRY-XYDRQXHOSA-N 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
244000287680 Garcinia dulcis Species 0.000 description 1
UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
238000009621 Solvay process Methods 0.000 description 1
DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 description 1
QWFQQZSXLXELLM-UHFFFAOYSA-N [Na].[Cl].C(O)(O)=O Chemical compound [Na].[Cl].C(O)(O)=O QWFQQZSXLXELLM-UHFFFAOYSA-N 0.000 description 1
239000002253 acid Substances 0.000 description 1
KHPLPBHMTCTCHA-UHFFFAOYSA-N ammonium chlorate Chemical compound N.OCl(=O)=O KHPLPBHMTCTCHA-UHFFFAOYSA-N 0.000 description 1
239000007900 aqueous suspension Substances 0.000 description 1
230000033228 biological regulation Effects 0.000 description 1
239000000571 coke Substances 0.000 description 1
239000012141 concentrate Substances 0.000 description 1
230000007423 decrease Effects 0.000 description 1
230000000694 effects Effects 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
230000035611 feeding Effects 0.000 description 1
239000012065 filter cake Substances 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
-1 hydrogen calcium oxide Chemical class 0.000 description 1
239000007788 liquid Substances 0.000 description 1
239000000203 mixture Substances 0.000 description 1
238000011084 recovery Methods 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000011780 sodium chloride Substances 0.000 description 1
238000001149 thermolysis Methods 0.000 description 1
238000011144 upstream manufacturing Methods 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Images

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/10—Separation of ammonia from ammonia liquors, e.g. gas liquors
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/18—Preparation by the ammonia-soda process

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Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Analytical Chemistry (AREA)
Dairy Products (AREA)
Gas Separation By Absorption (AREA)

CN 91110654 1990-10-10 1991-10-10 分解氯化铵水溶液的方法 Expired - Fee Related CN1030445C (zh)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
BE9000955A BE1004600A3 (fr)	1990-10-10	1990-10-10	Procede pour la decomposition d'une solution aqueuse de chlorure d'ammonium et procede de fabrication de carbonate de sodium.
BE9000955		1990-10-10

Publications (2)

Publication Number	Publication Date
CN1061760A CN1061760A (zh)	1992-06-10
CN1030445C true CN1030445C (zh)	1995-12-06

Family

ID=3884962

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CN 91110654 Expired - Fee Related CN1030445C (zh)	1990-10-10	1991-10-10	分解氯化铵水溶液的方法

Country Status (2)

Country	Link
CN (1)	CN1030445C (fr)
BE (1)	BE1004600A3 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN102351216A (zh) *	2011-07-12	2012-02-15	湖南恒光科技股份有限公司	一种联产白炭黑的纯碱制备工艺
EP3006400B1 (fr) *	2014-10-09	2017-12-13	Solvay SA	Procédé de production d'ammoniac

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
BE561500A (fr) *
US4294812A (en) *	1978-05-25	1981-10-13	General Electric Company	Recovery of ammonia from aqueous streams
JPS58172229A (ja) *	1982-04-02	1983-10-11	Asahi Glass Co Ltd	塩化アンモニウムの蒸留方法

1990
- 1990-10-10 BE BE9000955A patent/BE1004600A3/fr not_active IP Right Cessation
1991
- 1991-10-10 CN CN 91110654 patent/CN1030445C/zh not_active Expired - Fee Related

Also Published As

Publication number	Publication date
CN1061760A (zh)	1992-06-10
BE1004600A3 (fr)	1992-12-22

Legal Events

Date	Code	Title
1992-06-10	C06	Publication
1992-06-10	PB01	Publication
1994-01-12	C10	Entry into substantive examination
1994-01-12	SE01	Entry into force of request for substantive examination
1995-12-06	C14	Grant of patent or utility model
1995-12-06	GR01	Patent grant
1999-12-01	C19	Lapse of patent right due to non-payment of the annual fee
1999-12-01	CF01	Termination of patent right due to non-payment of annual fee

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