CN103142425A - Mineral mud nutritional emulsion and preparation method thereof - Google Patents
Mineral mud nutritional emulsion and preparation method thereof Download PDFInfo
- Publication number
- CN103142425A CN103142425A CN2013101128652A CN201310112865A CN103142425A CN 103142425 A CN103142425 A CN 103142425A CN 2013101128652 A CN2013101128652 A CN 2013101128652A CN 201310112865 A CN201310112865 A CN 201310112865A CN 103142425 A CN103142425 A CN 103142425A
- Authority
- CN
- China
- Prior art keywords
- sludge
- water
- condition
- moisture content
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052500 inorganic mineral Inorganic materials 0.000 title claims abstract description 73
- 239000011707 mineral Substances 0.000 title claims abstract description 73
- 239000000839 emulsion Substances 0.000 title claims abstract description 47
- 235000016709 nutrition Nutrition 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 42
- 238000004945 emulsification Methods 0.000 title abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 112
- 239000000203 mixture Substances 0.000 claims abstract description 67
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 42
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 42
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims abstract description 28
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims abstract description 28
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims abstract description 15
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 14
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 14
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 14
- -1 alkyl phosphate Chemical compound 0.000 claims abstract description 14
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 14
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 claims abstract description 14
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 14
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000010452 phosphate Substances 0.000 claims abstract description 14
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 claims abstract description 14
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 claims abstract description 14
- 229960003415 propylparaben Drugs 0.000 claims abstract description 14
- 239000008117 stearic acid Substances 0.000 claims abstract description 14
- 239000010802 sludge Substances 0.000 claims description 140
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 68
- 238000003756 stirring Methods 0.000 claims description 64
- 239000003921 oil Substances 0.000 claims description 41
- 238000000605 extraction Methods 0.000 claims description 40
- 239000000843 powder Substances 0.000 claims description 38
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 34
- 229940032094 squalane Drugs 0.000 claims description 34
- 239000007788 liquid Substances 0.000 claims description 23
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 14
- 229910052710 silicon Inorganic materials 0.000 claims description 14
- 239000010703 silicon Substances 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 12
- 230000035764 nutrition Effects 0.000 abstract description 4
- 239000008367 deionised water Substances 0.000 abstract description 3
- 229910021641 deionized water Inorganic materials 0.000 abstract description 3
- 239000004166 Lanolin Substances 0.000 abstract 1
- 239000000686 essence Substances 0.000 abstract 1
- 229960005150 glycerol Drugs 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 229940039717 lanolin Drugs 0.000 abstract 1
- 235000019388 lanolin Nutrition 0.000 abstract 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 abstract 1
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 abstract 1
- 229960002216 methylparaben Drugs 0.000 abstract 1
- 229960004063 propylene glycol Drugs 0.000 abstract 1
- 235000013772 propylene glycol Nutrition 0.000 abstract 1
- 229920002545 silicone oil Polymers 0.000 abstract 1
- 229960004418 trolamine Drugs 0.000 abstract 1
- 238000005303 weighing Methods 0.000 abstract 1
- 235000010755 mineral Nutrition 0.000 description 48
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 description 12
- 238000012360 testing method Methods 0.000 description 9
- 238000001914 filtration Methods 0.000 description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 239000012982 microporous membrane Substances 0.000 description 6
- 238000004659 sterilization and disinfection Methods 0.000 description 6
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 4
- 238000002372 labelling Methods 0.000 description 4
- 239000011572 manganese Substances 0.000 description 4
- 229910052748 manganese Inorganic materials 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 239000011573 trace mineral Substances 0.000 description 4
- 235000013619 trace mineral Nutrition 0.000 description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000010998 test method Methods 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- CCEKAJIANROZEO-UHFFFAOYSA-N sulfluramid Chemical group CCNS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F CCEKAJIANROZEO-UHFFFAOYSA-N 0.000 description 2
- 238000012795 verification Methods 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 102000001554 Hemoglobins Human genes 0.000 description 1
- 108010054147 Hemoglobins Proteins 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 206010061291 Mineral deficiency Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 210000000709 aorta Anatomy 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 235000020682 bottled natural mineral water Nutrition 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 210000002808 connective tissue Anatomy 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 210000000981 epithelium Anatomy 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000007952 growth promoter Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000003862 health status Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000003859 lipid peroxidation Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000021332 multicellular organism growth Effects 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 230000001835 salubrious effect Effects 0.000 description 1
- 238000013077 scoring method Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 230000037394 skin elasticity Effects 0.000 description 1
- 230000037204 skin physiology Effects 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Landscapes
- Edible Oils And Fats (AREA)
Abstract
A mineral mud nutrition emulsion and a preparation method thereof relate to an emulsion and a preparation method thereof. The invention aims to solve the problem that the existing emulsion can not provide more nutrition because the water for preparing the emulsion is deionized water. The invention relates to a mineral mud nutritional emulsion which is prepared by emulsifying stearic acid, octadecanol, monoglyceride, isopropyl palmitate, lanolin, water-soluble silicone oil, mineral mud oil-soluble extracting solution, alkyl phosphate, triethanolamine, propylene glycol, glycerol, propylparaben, methylparaben, essence and mineral mud water-soluble extracting solution. The preparation method comprises the following steps: firstly, weighing each component; secondly, preparing an oil phase mixture; thirdly, preparing a water phase mixture; fourthly, emulsification; obtaining the mineral mud nutritional emulsion. The invention can be used for preparing the mineral mud nutritional emulsion.
Description
Technical field
The present invention relates to a kind of emulsion and preparation method thereof.
Background technology
The formation of Wudalianchi Volcanic sludge is very long, and since 300,000 years, the old and new are repeatedly broken out in the phase volcano constantly volcano particle matter deposition, and is formed by the underground mineral water soaking.Forming process is through high temperature, high pressure, calmness is natural volcanic slurry naturally, contain various trace elements and organic acid, has higher medical function and health care value, after testing, containing calcium, magnesium, potassium, zinc, ferrum, copper etc. multiple to human body beneficial element and mineral etc., is that the desirable mineral of human body replenishes the source.
Contain higher metasilicic acid in Wudalianchi Volcanic sludge, mineral water, salinity is also higher, element silicon in metasilicic acid is mainly to be distributed on the aorta wall of human vas, it is the necessary trace element of human body, can participate in the biosynthesis of human connective tissue, epithelial tissue, osseous tissue, ossein, promote the human body growth promoter, can strengthen the permeability of blood vessel wall and elasticity, raising skin elasticity, play the effect of beauty and skin care; Zinc is indispensable trace element in body, it participates in the various physiological activities of human body, and in the trace element of skin, the content of zinc is the highest, it is determining the smooth and extent of elasticity of skin, participation melanin is synthetic, prevents and treats acne, keeps gloss and the slickness of skin, lipoid peroxidization resistant is arranged, remove interior free yl, make skin avoid lipid peroxidation injury, make skin soft, lubricious, smooth away wrinkles; Ferrum is the main component that consists of hemoglobin in blood, the ruddy blood that needs to supply with abundance of the gloss of skin, and complexion changed ruddy gloss in opposite is very useful; Copper is relevant with the metabolism of protein, nucleic acid, can make that skin is fine and smooth, hair is shiny black, makes the people full of vigour, keeps vigorous and graceful.The normal human can pass through the various meals of balance, obtain the good complement of mineral, but due to a variety of causes, some people also mineral deficiency can occur, and mineral can not synthesize in vivo, can only drink water by food, breathing or skin obtains.Emulsion is the product that the protection skin is the most basic, consumption is maximum, and the preparation water of most emulsions is deionized water, and more nutrition can not be provided.
Summary of the invention
The present invention is that will to solve the preparation water of existing emulsion be deionized water, more polyauxotrophic problem can not be provided, and a kind of sludge nutritional emulsions and preparation method thereof is provided.
a kind of sludge nutritional emulsions of the present invention is by mass percentage by 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 2%～4% lanoline, 5%～7% water-soluble silicon oil, 5%～7% sludge oil-soluble extracting solution, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben, 0.1%～0.3% methyl hydroxybenzoate, 0.01%～0.05% essence and surplus are that the sludge water-soluble extracting liquid forms through emulsifying.
The preparation method of above-mentioned sludge nutritional emulsions, carry out according to the following steps:
one, take each component: take by mass percentage 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 2%～4% lanoline, 5%～7% water-soluble silicon oil, 5%～7% sludge oil-soluble extracting solution, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben, 0.1%～0.3% methyl hydroxybenzoate, 0.01%～0.05% essence and surplus are the sludge water-soluble extracting liquid, two, preparation oil mixture: low whipping speed is under the condition of 80r/min～100r/min, 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 0.1%～0.3% methyl hydroxybenzoate, 2%～4% lanoline, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine and 5%～7% sludge oil-soluble extracting solution mixing and stirring that step 1 is taken also is heated to 70 ℃～85 ℃ from room temperature, obtains oil mixture, three, preparation aqueous mixture: low whipping speed is under the condition of 100r/min～150r/min, 5%～7% water-soluble silicon oil, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben and surplus that step 1 is taken are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 ℃～90 ℃ from room temperature, then continue to stir 20min～30min, obtain aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained joins in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 5min～10min under the condition of 2500r/min～3000r/min in speed, be cooled to 30 ℃～50 ℃, obtain the water oil mixture, then 0.01%～0.05% essence that step 1 is taken joins in the water oil mixture, continue to stir 10min～20min, be cooled to room temperature, namely obtain the sludge nutritional emulsions.
Advantage of the present invention: one, utilize Wudalianchi Volcanic sludge extracting solution and Wudalianchi natural mineral water to make the sludge nutritional emulsions, can provide abundant nutritional labeling to skin, make skin gloss, softness, high resilience; Two, the sludge nutritional emulsions of the present invention's preparation can satisfy people's demand at aspects such as delay skin aging, alleviation outside stimulus, climate change, environmental effects; Three, the preparation method technique of sludge nutritional emulsions of the present invention is simple, easy to operate; Four, the present invention's sludge extracting solution that will have a looks improving and the skin nourishing effect is applied in product emulsion, by the comprehensive function of various beneficial elements, promotes skin to the absorption of nutritional labeling, and effectively pins moisture, makes skin obtain basic nursing.
The specific embodiment
the specific embodiment one: a kind of sludge nutritional emulsions of present embodiment is by mass percentage by 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 2%～4% lanoline, 5%～7% water-soluble silicon oil, 5%～7% sludge oil-soluble extracting solution, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben, 0.1%～0.3% methyl hydroxybenzoate, 0.01%～0.05% essence and surplus are that the sludge water-soluble extracting liquid forms through emulsifying.
The described sludge nutritional emulsions of present embodiment can provide abundant nutritional labeling to skin, makes skin gloss, softness, high resilience.
the specific embodiment two: present embodiment is different from the specific embodiment one: described sludge water-soluble extracting liquid is to prepare according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min～50r/min, be that 10:1 joins mineral water in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of mineral water and moisture content＜1%, the mud mixture that obtains stirring, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mud mixture that stirs, obtain clear liquor and deposit, then with the deposit that obtains take mineral water as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain the sludge water-soluble extracting liquid, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins mineral water in deposit by mineral water and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other is identical with the specific embodiment one.
The described mineral water of present embodiment is through the pipeline disinfection by ultraviolet light, by the Wudalianchi metasilicic acid mineral water that the filtering with microporous membrane device filters, does not contain ferrum, the manganese of easy oxidation in the metasilicic acid mineral water of Wudalianchi.
the specific embodiment three: present embodiment is different from the specific embodiment one or two: described sludge oil-soluble extracting solution is to prepare according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min～30r/min, be that 5:1 joins squalane in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of squalane and moisture content＜1%, the mud that obtains stirring and the mixture of squalane, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mixture of the mud that stirs and squalane, obtain clear liquor and deposit, then with the deposit that obtains take squalane as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain sludge oil-soluble extracting solution, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins squalane in deposit by squalane and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other is identical with the specific embodiment one or two.
The described mineral water of present embodiment is through the pipeline disinfection by ultraviolet light, by the Wudalianchi metasilicic acid mineral water that the filtering with microporous membrane device filters, does not contain ferrum, the manganese of easy oxidation in the metasilicic acid mineral water of Wudalianchi.
The specific embodiment four: the preparation method of a kind of sludge nutritional emulsions of present embodiment, carry out according to the following steps:
one, take each component: take by mass percentage 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 2%～4% lanoline, 5%～7% water-soluble silicon oil, 5%～7% sludge oil-soluble extracting solution, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben, 0.1%～0.3% methyl hydroxybenzoate, 0.01%～0.05% essence and surplus are the sludge water-soluble extracting liquid, two, preparation oil mixture: low whipping speed is under the condition of 80r/min～100r/min, 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 0.1%～0.3% methyl hydroxybenzoate, 2%～4% lanoline, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine and 5%～7% sludge oil-soluble extracting solution mixing and stirring that step 1 is taken also is heated to 70 ℃～85 ℃ from room temperature, obtains oil mixture, three, preparation aqueous mixture: low whipping speed is under the condition of 100r/min～150r/min, 5%～7% water-soluble silicon oil, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben and surplus that step 1 is taken are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 ℃～90 ℃ from room temperature, then continue to stir 20min～30min, obtain aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained joins in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 5min～10min under the condition of 2500r/min～3000r/min in speed, be cooled to 30 ℃～50 ℃, obtain the water oil mixture, then 0.01%～0.05% essence that step 1 is taken joins in the water oil mixture, continue to stir 10min～20min, be cooled to room temperature, namely obtain the sludge nutritional emulsions.
The sludge nutritional emulsions of present embodiment preparation can provide abundant nutritional labeling to skin, makes skin gloss, softness, high resilience.
The preparation method technique of present embodiment is simple, easy to operate.
the specific embodiment five: what present embodiment was different from the specific embodiment four is: the sludge water-soluble extracting liquid described in step 1 prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min～50r/min, be that 10:1 joins mineral water in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of mineral water and moisture content＜1%, the mud mixture that obtains stirring, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mud mixture that stirs, obtain clear liquor and deposit, then with the deposit that obtains take mineral water as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain the sludge water-soluble extracting liquid, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins mineral water in deposit by mineral water and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other and the specific embodiment four.
The described mineral water of present embodiment is through the pipeline disinfection by ultraviolet light, by the Wudalianchi metasilicic acid mineral water that the filtering with microporous membrane device filters, does not contain ferrum, the manganese of easy oxidation in the metasilicic acid mineral water of Wudalianchi.
the specific embodiment six: what present embodiment was different from the specific embodiment four or five is: the sludge oil-soluble extracting solution described in step 1 prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min～30r/min, be that 5:1 joins squalane in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of squalane and moisture content＜1%, the mud that obtains stirring and the mixture of squalane, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mixture of the mud that stirs and squalane, obtain clear liquor and deposit, then with the deposit that obtains take squalane as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain sludge oil-soluble extracting solution, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins squalane in deposit by squalane and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.Other is identical with the specific embodiment four or five.
The described mineral water of present embodiment is through the pipeline disinfection by ultraviolet light, by the Wudalianchi metasilicic acid mineral water that the filtering with microporous membrane device filters, does not contain ferrum, the manganese of easy oxidation in the metasilicic acid mineral water of Wudalianchi.
The specific embodiment seven: what present embodiment was different from one of specific embodiment four to six is: in step 2, low whipping speed is under the condition of 90r/min～100r/min, 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 0.1%～0.3% methyl hydroxybenzoate, 2%～4% lanoline, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine and 5%～7% sludge oil-soluble extracting solution mixing and stirring that step 1 is taken also is heated to 75 ℃～80 ℃ from room temperature, obtains oil mixture.Other is identical with one of specific embodiment four to six.
The specific embodiment eight: what present embodiment was different from one of specific embodiment four to seven is: in step 3, low whipping speed is under the condition of 100r/min～150r/min, 5%～7% water-soluble silicon oil, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben and surplus that step 1 is taken are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 ℃～85 ℃ from room temperature, then continue to stir 25min～30min, obtain aqueous mixture.Other is identical with one of specific embodiment four to seven.
The specific embodiment nine: what present embodiment was different from one of specific embodiment four to eight is: the oil mixture that in step 4, step 2 is obtained joins in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 10min under the condition of 3000r/min in speed, be cooled to 30 ℃, obtain the water oil mixture, then 0.01%～0.05% essence that step 1 is taken joins in the water oil mixture, continue to stir 20min, be cooled to room temperature, namely obtain the sludge nutritional emulsions.Other is identical with one of specific embodiment four to eight.
Adopt following verification experimental verification effect of the present invention:
Test one: a kind of preparation method of sludge nutritional emulsions, carry out according to the following steps:
One, take each component: take 3.2g stearic acid, 4g octadecanol, 3g monoglyceride, 4g isopropyl palmitate, 3g lanoline, 6g water-soluble silicon oil, 5g sludge oil-soluble extracting solution, 4.5g alkyl phosphate, 1.5g triethanolamine, 5g propylene glycol, 9g glycerol, 0.2g propylparaben, 0.2g methyl hydroxybenzoate, 0.02g essence and 51.38g sludge water-soluble extracting liquid; Two, preparation oil mixture: low whipping speed is under the condition of 100r/min, 3.2g stearic acid, 4g octadecanol, 3g monoglyceride, 4g isopropyl palmitate, 0.2g methyl hydroxybenzoate, 3g lanoline, 4.5g alkyl phosphate, 1.5g triethanolamine and the 5g sludge oil-soluble extracting solution mixing and stirring that step 1 is taken also is heated to 80 ℃ from room temperature, obtains oil mixture; Three, preparation aqueous mixture: low whipping speed is under the condition of 150r/min, 6g water-soluble silicon oil, 5g propylene glycol, 9g glycerol, 0.2g propylparaben and the 51.38g sludge water-soluble extracting liquid mixing and stirring that step 1 is taken also is heated to 85 ℃ from room temperature, then continue to stir 30min, obtain aqueous mixture; Four, emulsifying: the oil mixture that step 2 is obtained joins in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 10min under the condition of 2500r/min in speed, be cooled to 40 ℃, obtain the water oil mixture, then the 0.02g essence that step 1 is taken joins in the water oil mixture, continue to stir 20min, be cooled to room temperature, namely obtain the sludge nutritional emulsions.
sludge water-soluble extracting liquid described in this test procedure one prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 40r/min, to be 1:3 join moisture content with mineral water by the moisture content mass ratio that is 30% Wudalianchi Volcanic sludge and mineral water is to stir in 30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 20 days, pulverized at last 600 mesh sieves, obtain moisture content and be 0.3% sludge powder, two, Centrifugical extraction: low whipping speed is under the condition of 50r/min, it is to stir 24h in 0.3% sludge powder that the 300g mineral water is joined the 30g moisture content, the mud mixture that obtains stirring, then be centrifugal 10min under the condition of 4000r/min at rotating speed with the mud mixture that stirs, obtain clear liquor and deposit, then with the deposit that obtains take mineral water as the extractant Centrifugical extraction 3 times again, merge the clear liquor of gained, namely obtain the sludge water-soluble extracting liquid, deposit Centrifugical extraction described in step 2 carries out according to the following steps: being that 3:1 joins mineral water in deposit by mineral water and sedimental mass ratio, is centrifugal 10min under the condition of 4000r/min at rotating speed, namely completes sedimental Centrifugical extraction, wherein said mineral water is through the pipeline disinfection by ultraviolet light, by the Wudalianchi metasilicic acid mineral water of filtering with microporous membrane device filtration.
sludge oil-soluble extracting solution described in this test procedure one prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 40r/min, to be 1:3 join moisture content with mineral water by the moisture content mass ratio that is 30% Wudalianchi Volcanic sludge and mineral water is to stir in 30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 20 days, pulverized at last 600 mesh sieves, obtain moisture content and be 0.3% sludge powder, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min, it is to stir 24h in 0.3% sludge powder that the 150g squalane is joined the 30g moisture content, the mud that obtains stirring and the mixture of squalane, then be centrifugal 10min under the condition of 4000r/min at rotating speed with the mixture of the mud that stirs and squalane, obtain clear liquor and deposit, then with the deposit that obtains take squalane as the extractant Centrifugical extraction 3 times again, merge the clear liquor of gained, namely obtain sludge oil-soluble extracting solution, deposit Centrifugical extraction described in step 2 carries out according to the following steps: being that 3:1 joins squalane in deposit by squalane and sedimental mass ratio, is centrifugal 10min under the condition of 4000r/min at rotating speed, namely completes sedimental Centrifugical extraction, wherein said mineral water is through the pipeline disinfection by ultraviolet light, by the Wudalianchi metasilicic acid mineral water of filtering with microporous membrane device filtration.
Test two: to testing the sludge nutritional emulsions test of a preparation, method of testing is carried out according to the following steps:
Emulsion is the articles for use that are applied directly to skin, so easy to use and comfortable use sense is arranged is to determine that value of the product and consumer welcome the key factor of degree to this product.Sensory evaluation is during emulsion is used and the subjective assessment after using, and carries out overall merit in conjunction with skin physiology characteristic, permeability principle.
Test result: in evaluation, adopt the scoring method of inspection to carry out the sense organ evaluation and test, set up 8 organoleptic indicators, each organoleptic indicator carries out ten point system marking and estimates, and sense organ group comprises 10 group members.Test result is as shown in table 1:
Table 1
From the test result of use, sludge nutritional emulsions viscosity is low, non-greasy, easy to apply, ductility good and fine and smooth, be conducive to skin absorbing from dividing sludge nutritional emulsions abundant nutrition composition, the moist degree of product and salubrious degree are higher, and, after using, skin is glossy, is conducive to skin and recovers nature, resilient health status.
Claims (9)
1. a sludge nutritional emulsions, is characterized in that the sludge nutritional emulsions is that the sludge water-soluble extracting liquid forms through emulsifying by 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 2%～4% lanoline, 5%～7% water-soluble silicon oil, 5%～7% sludge oil-soluble extracting solution, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben, 0.1%～0.3% methyl hydroxybenzoate, 0.01%～0.05% essence and surplus by mass percentage.
2. a kind of sludge nutritional emulsions according to claim 1, it is characterized in that described sludge water-soluble extracting liquid prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min～50r/min, be that 10:1 joins mineral water in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of mineral water and moisture content＜1%, the mud mixture that obtains stirring, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mud mixture that stirs, obtain clear liquor and deposit, then with the deposit that obtains take mineral water as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain the sludge water-soluble extracting liquid, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins mineral water in deposit by mineral water and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.
3. a kind of sludge nutritional emulsions according to claim 1, it is characterized in that described sludge oil-soluble extracting solution prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min～30r/min, be that 5:1 joins squalane in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of squalane and moisture content＜1%, the mud that obtains stirring and the mixture of squalane, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mixture of the mud that stirs and squalane, obtain clear liquor and deposit, then with the deposit that obtains take squalane as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain sludge oil-soluble extracting solution, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins squalane in deposit by squalane and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.
4. the preparation method of a kind of sludge nutritional emulsions as claimed in claim 1 is characterized in that the preparation method of sludge nutritional emulsions is carried out according to the following steps:
one, take each component: take by mass percentage 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 2%～4% lanoline, 5%～7% water-soluble silicon oil, 5%～7% sludge oil-soluble extracting solution, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben, 0.1%～0.3% methyl hydroxybenzoate, 0.01%～0.05% essence and surplus are the sludge water-soluble extracting liquid, two, preparation oil mixture: low whipping speed is under the condition of 80r/min～100r/min, 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 0.1%～0.3% methyl hydroxybenzoate, 2%～4% lanoline, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine and 5%～7% sludge oil-soluble extracting solution mixing and stirring that step 1 is taken also is heated to 70 ℃～85 ℃ from room temperature, obtains oil mixture, three, preparation aqueous mixture: low whipping speed is under the condition of 100r/min～150r/min, 5%～7% water-soluble silicon oil, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben and surplus that step 1 is taken are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 ℃～90 ℃ from room temperature, then continue to stir 20min～30min, obtain aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained joins in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 5min～10min under the condition of 2500r/min～3000r/min in speed, be cooled to 30 ℃～50 ℃, obtain the water oil mixture, then 0.01%～0.05% essence that step 1 is taken joins in the water oil mixture, continue to stir 10min～20min, be cooled to room temperature, namely obtain the sludge nutritional emulsions.
5. the preparation method of a kind of sludge nutritional emulsions according to claim 4, it is characterized in that the sludge water-soluble extracting liquid described in step 1 prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 20r/min～50r/min, be that 10:1 joins mineral water in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of mineral water and moisture content＜1%, the mud mixture that obtains stirring, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mud mixture that stirs, obtain clear liquor and deposit, then with the deposit that obtains take mineral water as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain the sludge water-soluble extracting liquid, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins mineral water in deposit by mineral water and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.
6. the preparation method of according to claim 4 or 5 described a kind of sludge nutritional emulsions, it is characterized in that the sludge oil-soluble extracting solution described in step 1 prepares according to the following steps: one, preparation sludge powder: low whipping speed is under the condition of 20r/min～50r/min, being that 25%～30% Wudalianchi Volcanic sludge and the mass ratio of mineral water are 1:(2～3.5 by moisture content) mineral water is joined moisture content is to stir in 25%～30% Wudalianchi Volcanic sludge, obtain slime water, at room temperature, the slime water that obtains is crossed 700 mesh sieves, the slime water of volcanic pisolite and root system of plant is removed, then at room temperature dry 15 days～20 days, pulverized at last 600 mesh sieves, obtain the sludge powder of moisture content＜1%, two, Centrifugical extraction: low whipping speed is under the condition of 10r/min～30r/min, be that 5:1 joins squalane in the sludge powder of moisture content＜1% and stirs 24h～30h by the mass ratio of the sludge powder of squalane and moisture content＜1%, the mud that obtains stirring and the mixture of squalane, then be centrifugal 10min～15min under the condition of 3000r/min～4000r/min at rotating speed with the mixture of the mud that stirs and squalane, obtain clear liquor and deposit, then with the deposit that obtains take squalane as the extractant Centrifugical extraction 2 times～3 times again, the clear liquor that merges gained, namely obtain sludge oil-soluble extracting solution, deposit Centrifugical extraction described in step 2 carries out according to the following steps: be that 3:1 joins squalane in deposit by squalane and sedimental mass ratio, be centrifugal 8min～10min under the condition of 3000r/min～4000r/min at rotating speed, namely complete sedimental Centrifugical extraction.
7. the preparation method of a kind of sludge nutritional emulsions according to claim 6, it is characterized in that in step 2, low whipping speed is under the condition of 90r/min～100r/min, 3%～3.5% stearic acid, 4%～5% octadecanol, 2%～3% monoglyceride, 3%～5% isopropyl palmitate, 0.1%～0.3% methyl hydroxybenzoate, 2%～4% lanoline, 4%～5% alkyl phosphate, 1.5%～2.5% triethanolamine and 5%～7% sludge oil-soluble extracting solution mixing and stirring that step 1 is taken also is heated to 75 ℃～80 ℃ from room temperature, obtains oil mixture.
8. the preparation method of a kind of sludge nutritional emulsions according to claim 4, it is characterized in that in step 3, low whipping speed is under the condition of 100r/min～150r/min, 5%～7% water-soluble silicon oil, 1%～3% propylene glycol, 8%～9% glycerol, 0.1%～0.3% propylparaben and surplus that step 1 is taken are sludge water-soluble extracting liquid mixing and stirring and are heated to 80 ℃～85 ℃ from room temperature, then continue to stir 25min～30min, obtain aqueous mixture.
9. the preparation method of a kind of sludge nutritional emulsions according to claim 4, it is characterized in that the oil mixture that in step 4, step 2 is obtained joins in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 10min under the condition of 3000r/min in speed, be cooled to 30 ℃, obtain the water oil mixture, 0.01%～0.05% essence that then step 1 is taken joins in the water oil mixture, continues to stir 20min, be cooled to room temperature, namely obtain the sludge nutritional emulsions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310112865.2A CN103142425B (en) | 2013-04-02 | 2013-04-02 | Mineral mud nutritional emulsion and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310112865.2A CN103142425B (en) | 2013-04-02 | 2013-04-02 | Mineral mud nutritional emulsion and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103142425A true CN103142425A (en) | 2013-06-12 |
| CN103142425B CN103142425B (en) | 2014-12-17 |
Family
ID=48540945
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310112865.2A Expired - Fee Related CN103142425B (en) | 2013-04-02 | 2013-04-02 | Mineral mud nutritional emulsion and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103142425B (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104666128A (en) * | 2015-03-16 | 2015-06-03 | 黑龙江省科学院火山与矿泉研究所 | Volcanic mud essence spray mask and preparation method thereof |
| CN105078770A (en) * | 2014-05-20 | 2015-11-25 | 李复兴 | Method for making mineral cleaning and maintaining lozenge |
| CN105232369A (en) * | 2015-09-28 | 2016-01-13 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof |
| CN106074855A (en) * | 2016-07-25 | 2016-11-09 | 王波林 | A kind of absorption sludge |
| CN106074231A (en) * | 2016-08-03 | 2016-11-09 | 黑龙江省科学院火山与矿泉研究所 | Slime skin-cleaning gel and preparation method thereof |
| CN107080724A (en) * | 2017-04-19 | 2017-08-22 | 北海蓝晖环保科技有限公司 | Nti-freckle anti-wrinkle cream |
| CN107137302A (en) * | 2017-04-19 | 2017-09-08 | 北海蓝晖环保科技有限公司 | Compound face cream |
| CN110101613A (en) * | 2019-06-24 | 2019-08-09 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified oil-in-water emulsion and preparation method thereof |
| CN110179699A (en) * | 2019-06-24 | 2019-08-30 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified water-in-oil emulsion and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1252266A (en) * | 1998-10-28 | 2000-05-10 | 黑龙江省科学院火山矿泉资源研究所 | Mineral slime beauty cream and preparation method thereof |
| CN102068389A (en) * | 2010-09-06 | 2011-05-25 | 厦门澳丽尔日化有限公司 | Micro-emulsified environmentally-friendly facial treatment milk and preparation method thereof |
| CN102935056A (en) * | 2012-12-06 | 2013-02-20 | 黑龙江省科学院火山与矿泉研究所 | Slime sun screen and preparation method thereof |
-
2013
- 2013-04-02 CN CN201310112865.2A patent/CN103142425B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1252266A (en) * | 1998-10-28 | 2000-05-10 | 黑龙江省科学院火山矿泉资源研究所 | Mineral slime beauty cream and preparation method thereof |
| CN102068389A (en) * | 2010-09-06 | 2011-05-25 | 厦门澳丽尔日化有限公司 | Micro-emulsified environmentally-friendly facial treatment milk and preparation method thereof |
| CN102935056A (en) * | 2012-12-06 | 2013-02-20 | 黑龙江省科学院火山与矿泉研究所 | Slime sun screen and preparation method thereof |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105078770A (en) * | 2014-05-20 | 2015-11-25 | 李复兴 | Method for making mineral cleaning and maintaining lozenge |
| CN104666128A (en) * | 2015-03-16 | 2015-06-03 | 黑龙江省科学院火山与矿泉研究所 | Volcanic mud essence spray mask and preparation method thereof |
| CN104666128B (en) * | 2015-03-16 | 2017-07-18 | 黑龙江省科学院火山与矿泉研究所 | Volcanic mud essence spray mask |
| CN105232369B (en) * | 2015-09-28 | 2018-09-28 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof |
| CN105232369A (en) * | 2015-09-28 | 2016-01-13 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof |
| CN106074855A (en) * | 2016-07-25 | 2016-11-09 | 王波林 | A kind of absorption sludge |
| CN106074231B (en) * | 2016-08-03 | 2019-04-02 | 黑龙江省科学院火山与矿泉研究所 | Slime skin-cleaning gel and preparation method thereof |
| CN106074231A (en) * | 2016-08-03 | 2016-11-09 | 黑龙江省科学院火山与矿泉研究所 | Slime skin-cleaning gel and preparation method thereof |
| CN107137302A (en) * | 2017-04-19 | 2017-09-08 | 北海蓝晖环保科技有限公司 | Compound face cream |
| CN107080724A (en) * | 2017-04-19 | 2017-08-22 | 北海蓝晖环保科技有限公司 | Nti-freckle anti-wrinkle cream |
| CN110101613A (en) * | 2019-06-24 | 2019-08-09 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified oil-in-water emulsion and preparation method thereof |
| CN110179699A (en) * | 2019-06-24 | 2019-08-30 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified water-in-oil emulsion and preparation method thereof |
| CN110179699B (en) * | 2019-06-24 | 2022-03-22 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified water-in-oil emulsion and preparation method thereof |
| CN110101613B (en) * | 2019-06-24 | 2022-03-22 | 黑龙江省科学院火山与矿泉研究所 | Natural skin-care volcanic mud particle emulsified oil-in-water emulsion and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103142425B (en) | 2014-12-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103142425B (en) | Mineral mud nutritional emulsion and preparation method thereof | |
| CN106137916A (en) | The cosmetic composition of a kind of removing acnes and controlling oil whitening and application thereof | |
| CN106176556A (en) | A kind of removing acnes and controlling oil whitening cream | |
| CN103340817A (en) | Radix puerariae whitening facial mask | |
| CN103381136B (en) | A kind of edible cosmetics and preparation method thereof | |
| CN106798722A (en) | A kind of anti-ageing moisturizing maintenance creams of not silicate-containing oil and preparation method thereof | |
| CN106551398A (en) | A kind of anti-aging cream taste and preparation method thereof | |
| CN108261367A (en) | A kind of anti-aging moisturizing essence and preparation method thereof | |
| CN106177921A (en) | A kind of breast augmentation and health alimentation composition | |
| CN103735457A (en) | Toner containing herbal components and preparation method thereof | |
| CN104473286A (en) | Solid (functional) beverage synthesized from hibiacus esculengtus, fungi and alga and preparation method thereof | |
| CN105123960A (en) | Soybean milk capable of tonifying blood, caring skin and beautifying face | |
| CN103893101A (en) | Ganoderma lucidum and pollen anti-aging cream | |
| CN105055773A (en) | Foot bath health-preserving rehabilitation health product, preparation method and application thereof | |
| CN103860430B (en) | A kind of beauty mask and preparation method thereof | |
| CN101278967B (en) | Health care capsules for overall regulating immunity of organism and preparation technique | |
| CN102488637A (en) | Environment-friendly and carrier-free food-grade cosmetic membrane | |
| CN106234924A (en) | A kind of brain-strengthening dumplings and preparation method thereof | |
| CN105168067A (en) | A kind of active freckle essence and its preparation method | |
| CN100381060C (en) | Method for preparing liver-benefiting, face-beautifying yoghout with micron pine pollen, pearl powder for women | |
| CN104432305A (en) | Beverage with dietary therapy function and preparation method thereof | |
| KR20090050930A (en) | Camellia leaf tea composition and preparation method thereof | |
| CN100352358C (en) | Method for preparing liver-benefiting, face-beautifying milk liquid with micron pine pollen, pearl powder for women | |
| CN104982924A (en) | Coix seed composition | |
| CN100360043C (en) | Method for preparing liver-benefiting, face-beautifying milk powder with micron pine pollen, pearl powder for women |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141217 Termination date: 20200402 |